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These results have been patented in: DE-P-19623142.6
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Kinetic resolution could be excluded in the derivatization of 2. In the reaction of rac-2 with (S)-1 -phenylethylamine two diatereomers were formed in a ratio of 1:1.
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0343244705
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note
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2=0.120, Flack-parameter=-0.8(4), programs used: SHELXS-86, SHELXL-93, SCHAKAL-92. Other details of the crystal structure analysis can be ordered at the "Fachinformationszentrum Karlsruhe", D-76344 Eggenstein-Leopoldshafen, deposition number CSD-405477.
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