-
1
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-
0003829079
-
-
Academic Press, London
-
Lazlo, P. (ed), 'Preparative Chemistry Using Supported Reagents', Academic Press, London, 1987 ; Smith, K. 'Solid Supports and Catalysts in Organic Synthesis'. Elis Horwood, Chichester, 1992.
-
(1987)
Preparative Chemistry Using Supported Reagents
-
-
Lazlo, P.1
-
2
-
-
0004153643
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-
Elis Horwood, Chichester
-
Lazlo, P. (ed), 'Preparative Chemistry Using Supported Reagents', Academic Press, London, 1987 ; Smith, K. 'Solid Supports and Catalysts in Organic Synthesis'. Elis Horwood, Chichester, 1992.
-
(1992)
Solid Supports and Catalysts in Organic Synthesis
-
-
Smith, K.1
-
3
-
-
0030485144
-
-
Bone, S.; Evans, D.G.; Perriam, J.L; Slade, R.C.T., Angew. Chem. Int. Ed. Engl., 1996, 35, 1850-1852; Lane, R.H.; Callahan, K.P.; Cooksey, R.; Dines, P.M.; Griffith, P.C. Prepr. Am. Chem. Soc., Div. Pet. Chem., 1982, 27, 624-631 (C.A., 101: 130760n) ; Dines, M.B.; DiGiacomo, P.M.; Callahan, K.P. US Pat. 4,384,981, (1981) (C.A., 99: 121445b) ; Callahan, K.P.; Dines, M.B. US Pat. 4,983,564 (1984) (C.A., 115: 51412m)
-
(1996)
Angew. Chem. Int. Ed. Engl.
, vol.35
, pp. 1850-1852
-
-
Bone, S.1
Evans, D.G.2
Perriam, J.L.3
Slade, R.C.T.4
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4
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-
0020179432
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C.A., 101: 130760n
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Bone, S.; Evans, D.G.; Perriam, J.L; Slade, R.C.T., Angew. Chem. Int. Ed. Engl., 1996, 35, 1850-1852; Lane, R.H.; Callahan, K.P.; Cooksey, R.; Dines, P.M.; Griffith, P.C. Prepr. Am. Chem. Soc., Div. Pet. Chem., 1982, 27, 624-631 (C.A., 101: 130760n) ; Dines, M.B.; DiGiacomo, P.M.; Callahan, K.P. US Pat. 4,384,981, (1981) (C.A., 99: 121445b) ; Callahan, K.P.; Dines, M.B. US Pat. 4,983,564 (1984) (C.A., 115: 51412m)
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(1982)
Prepr. Am. Chem. Soc., Div. Pet. Chem.
, vol.27
, pp. 624-631
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Lane, R.H.1
Callahan, K.P.2
Cooksey, R.3
Dines, P.M.4
Griffith, P.C.5
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5
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0343555739
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US Pat. 4,384,981, (1981) (C.A., 99: 121445b)
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Bone, S.; Evans, D.G.; Perriam, J.L; Slade, R.C.T., Angew. Chem. Int. Ed. Engl., 1996, 35, 1850-1852; Lane, R.H.; Callahan, K.P.; Cooksey, R.; Dines, P.M.; Griffith, P.C. Prepr. Am. Chem. Soc., Div. Pet. Chem., 1982, 27, 624-631 (C.A., 101: 130760n) ; Dines, M.B.; DiGiacomo, P.M.; Callahan, K.P. US Pat. 4,384,981, (1981) (C.A., 99: 121445b) ; Callahan, K.P.; Dines, M.B. US Pat. 4,983,564 (1984) (C.A., 115: 51412m)
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Dines, M.B.1
DiGiacomo, P.M.2
Callahan, K.P.3
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6
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0342685527
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US Pat. 4,983,564 (1984) (C.A., 115: 51412m)
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Bone, S.; Evans, D.G.; Perriam, J.L; Slade, R.C.T., Angew. Chem. Int. Ed. Engl., 1996, 35, 1850-1852; Lane, R.H.; Callahan, K.P.; Cooksey, R.; Dines, P.M.; Griffith, P.C. Prepr. Am. Chem. Soc., Div. Pet. Chem., 1982, 27, 624-631 (C.A., 101: 130760n) ; Dines, M.B.; DiGiacomo, P.M.; Callahan, K.P. US Pat. 4,384,981, (1981) (C.A., 99: 121445b) ; Callahan, K.P.; Dines, M.B. US Pat. 4,983,564 (1984) (C.A., 115: 51412m)
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Callahan, K.P.1
Dines, M.B.2
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8
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49349130611
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Alberti, G.; Costantino, U.; Allulli, S.; Tomassini, N. J. Inorg. Nucl. Chem., 1978, 40, 1113-1117
-
(1978)
J. Inorg. Nucl. Chem.
, vol.40
, pp. 1113-1117
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-
Alberti, G.1
Costantino, U.2
Allulli, S.3
Tomassini, N.4
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9
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0001156588
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Schull, T.L.; Fettinger, J.C.; Knight, D.A. Inorg. Chem., 1996, 35, 6717-6723.
-
(1996)
Inorg. Chem.
, vol.35
, pp. 6717-6723
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-
Schull, T.L.1
Fettinger, J.C.2
Knight, D.A.3
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10
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0026607580
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Ravindar, V.; Hemling, H.; Schumann, H.; Blum, J. Synth. Commun., 1992, 22, 841-851.
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(1992)
Synth. Commun.
, vol.22
, pp. 841-851
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-
Ravindar, V.1
Hemling, H.2
Schumann, H.3
Blum, J.4
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11
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0001412847
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Under argon atmosphere, dichlorobis(triphenylphosphine)palladium (0.17 mmol), triethylsilane (0.17 mmol) and 2 ml of toluene were refluxed for 5 min. in order to reduce palladium (II) complex to palladium (0). Phosphine 1 (3.45 mmol), diethylphosphite (3.47 mmol) and triethylamine (3.5 mmol) in solution of toluene (6 mL) of toluene were added. The solution was refluxed for 22 hours, washed and purified by column chromatography to offer the phosphonate 2 with 56 % yield
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Hirao, T.; Masunaga, T.; Yamada, N. Y. Ohshiro, N.Y.; Agawa, T. Bull. Chem. Soc. Jpn., 1982, 55, 909-913. Under argon atmosphere, dichlorobis(triphenylphosphine)palladium (0.17 mmol), triethylsilane (0.17 mmol) and 2 ml of toluene were refluxed for 5 min. in order to reduce palladium (II) complex to palladium (0). Phosphine 1 (3.45 mmol), diethylphosphite (3.47 mmol) and triethylamine (3.5 mmol) in solution of toluene (6 mL) of toluene were added. The solution was refluxed for 22 hours, washed and purified by column chromatography to offer the phosphonate 2 with 56 % yield.
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(1982)
Bull. Chem. Soc. Jpn.
, vol.55
, pp. 909-913
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Hirao, T.1
Masunaga, T.2
Yamada, N.Y.3
Ohshiro, N.Y.4
Agawa, T.5
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12
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15144356086
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McKenna, C.E.; Higa, M.T.; Cheung, N.H.; McKenna, M.C. Tetrahedron Lett., 1977, 155-58.
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(1977)
Tetrahedron Lett.
, pp. 155-158
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McKenna, C.E.1
Higa, M.T.2
Cheung, N.H.3
McKenna, M.C.4
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13
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0343991840
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To a solution of phosphonic acid 3 in 100 mL of DMF under argon atmosphere, we added palladium dichloride (4.7 mmol) and the solution was stirred for 24 h. Evaporation of the solvent under vacuum afforded the palladium complex 4 as a polymeric form in 98% yield ; Roffia, P.; Conti, F.; Gregori, G. Chem. Ind. (Milan), 1971, 53, 361-362.
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(1971)
Chem. Ind. (Milan)
, vol.53
, pp. 361-362
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Roffia, P.1
Conti, F.2
Gregori, G.3
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15
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0342685525
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note
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In a typical experiment, the palladium complex 4 (1.25 mmol) and phosphorous acid (15 mmol) were dissolved, under argon, in 110 ml of HCl 4.3 M. A solution of zirconium chloride octahydrated (8.3 mmol) in 15 ml of water was added dropwise. The resulting suspension was heated for 3 days. The precipitate was filtered off, washed with water to afford, after air drying, 3.25 g of orange solid ( 5).
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17
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0342685524
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note
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Found. % : H : 1.4 ; Cl : 4.46 ; P : 19.55, Zr : 27.12 ; Pd : 3.38 ; C : 10.27
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18
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0000221333
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Dines, M.B.; DiGiacomo, P.M.; Callahan, K.P.; Griffith, P.C.; Lane, R.H.; Cooksey, R.E. A.C.S. Symp. Ser., 1982, 192, 223-240
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(1982)
A.C.S. Symp. Ser.
, vol.192
, pp. 223-240
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Dines, M.B.1
DiGiacomo, P.M.2
Callahan, K.P.3
Griffith, P.C.4
Lane, R.H.5
Cooksey, R.E.6
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19
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0343991838
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note
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The catalyst 5 (20 mg), triethylsilane (0.01 ml) and toluene (1 ml) are placed under argon in a Schlenk tube. The solution was refluxed for 30 min. in order to reduce the palladium (II) complex to palladium (O). lodobenzene (1 mmol), methyl acrylate (0.13 ml, 1.5 eq.) and triethylamine (0.21 ml, 1.5 eq.) in 2 ml of toluene were then added and the reflux was continued for 24 h. After hydrolysis and purification by column chromatography, the methyl cinnamate was isolated with 92 % yield.
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20
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0021366619
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Csicsery, S.M. Zeolites , 1984, 4, 202-213 ; Csicsery, S.M. Pure Appl. Chem., 1986, 58, 841-856; Chen, N.Y.; Garwood, W.E. Cat. Rev. Sc. Eng., 1986, 28, 185-264; Y. Sugi Y.; Toba, M. Cat. Today, 1994, 19, 187-212.
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(1984)
Zeolites
, vol.4
, pp. 202-213
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Csicsery, S.M.1
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21
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0022736497
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Csicsery, S.M. Zeolites , 1984, 4, 202-213 ; Csicsery, S.M. Pure Appl. Chem., 1986, 58, 841-856; Chen, N.Y.; Garwood, W.E. Cat. Rev. Sc. Eng., 1986, 28, 185-264; Y. Sugi Y.; Toba, M. Cat. Today, 1994, 19, 187-212.
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(1986)
Pure Appl. Chem.
, vol.58
, pp. 841-856
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Csicsery, S.M.1
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22
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0022735884
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Csicsery, S.M. Zeolites , 1984, 4, 202-213 ; Csicsery, S.M. Pure Appl. Chem., 1986, 58, 841-856; Chen, N.Y.; Garwood, W.E. Cat. Rev. Sc. Eng., 1986, 28, 185-264; Y. Sugi Y.; Toba, M. Cat. Today, 1994, 19, 187-212.
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(1986)
Cat. Rev. Sc. Eng.
, vol.28
, pp. 185-264
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Chen, N.Y.1
Garwood, W.E.2
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23
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0028768974
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Csicsery, S.M. Zeolites , 1984, 4, 202-213 ; Csicsery, S.M. Pure Appl. Chem., 1986, 58, 841-856; Chen, N.Y.; Garwood, W.E. Cat. Rev. Sc. Eng., 1986, 28, 185-264; Y. Sugi Y.; Toba, M. Cat. Today, 1994, 19, 187-212.
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(1994)
Cat. Today
, vol.19
, pp. 187-212
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Sugi, Y.1
Toba, M.2
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24
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0025168554
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Choudary, B.M.; Ravichandra Sarma, M.; Rao, K.K. Tetrahedron letters, 1990, 31, 5781-5784.
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(1990)
Tetrahedron Letters
, vol.31
, pp. 5781-5784
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Choudary, B.M.1
Ravichandra Sarma, M.2
Rao, K.K.3
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26
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0007108145
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Oxford Molecular Group Inc.
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CAChe Scientific, Oxford Molecular Group Inc.
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CAChe Scientific
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