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note
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All new products showed satisfactory spectral and/or analytical data.
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30
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0343375919
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note
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The formation of the non-volatile Wurtz-coupling by-products biphenyl and 1,2-diphenylethane was observed in reactions involving phenyl and benzyl Grignards, respectively. In one case (PhMgBr) the reaction was repeated with slow addition (2-3h) of the Grignard in an effort to supress this phenomenon, without any significant change in product yields.
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