A rapid procedure to prepare cefotaxime

Farmaco

Volumn 55, Issue 5, 2000, Pages 393-396

  Rodríguez, Juan C ^a   Hernández, Ricardo ^a   González, Maritza ^a   López, Miguel A ^a   Fini, Adamo ^b  

^a PO Box 16042   (Cuba)

^b UNIVERSITY OF BOLOGNA   (Italy)

Author keywords

7 Aminocephalosporanic acid; Cefotaxime; MAEM; Synthesis

Indexed keywords

2 AMINOTHIAZOLE DERIVATIVE; 2 MERCAPTOBENZOTHIAZOLE; 7 AMINOCEPHALOSPORANIC ACID; CEFOTAXIME; REAGENT; THIOESTER;

ACYLATION; ARTICLE; CHEMICAL MODIFICATION; CHEMICAL REACTION; DRUG SYNTHESIS; REACTION ANALYSIS;

CEFOTAXIME; CEPHALOSPORINS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CHROMATOGRAPHY, THIN LAYER; MAGNETIC RESONANCE SPECTROSCOPY;

EID: 0342520600     PISSN: 0014827X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0014-827X(00)00058-6     Document Type: Article

References (19)

1. Dürckheimer W., Blumbach J., Lattrell R., Scheunemann K.H. Recent developments in the field of β-lactam antibiotics. Angew. Chem., Int. Ed. Engl. 24:1985;180-202.
2. Martindale, The Extra Pharmacopeia, 29th ed., The Pharmaceutical Press, , London, 1989, pp. 151-156.
3. Fujimoto K., Ishihara S., Yanagisawa H., Ide J., Nakayama E., Nakao H., Sugawara S., Iwata M. Studies on orally active cephalosporins esters. J. Antibiot. 40:1987;370-384.
4. Tood W.M. Cefpodoxime proxetil a comprehensive review. Int. J. Antimicrob. Agents. 4:1994;37-62.
5. V. Hitzel, R. Latrell, D. Bormann, Verfahren zur Herstellung von Cephemverbindungen, OF Patent 2 804 040, Chem. Abstracts (1979) 92:P22513w.
6. M. Ochiai, T. Okada, O. Aki, A. Morimoto, K. Kawakita, Y. Matsushita, Thiazolylacetamido cephalosporin type compounds, US Patent 4 098 888, Chem. Abstracts (1978) 88:P89656.
7. Bucort R., Heymes R., Lutz L., Pénasse L., Perronet J. Influence de la presence et la presence et de la configuration d'un oxymino sur l'activite antibacterienne. Tetrahedron. 34:1978;2233-2243.
8. R. Heymes, A. Lutz, Nouvelles oximes dérivées de l'acide 3-alkiloxy ou 3-alkylthiométhyl 7-amino thiazolylacetamido céphalosporanique, leur préparation, leur application comme médicaments, les compositions les renfermant et les nouveaux intermédiaires obtenus, US Patent 4 152 432 Chem. Abstracts (1979) 88:P37815n.
9. Ochiai M., Morimoto A., Miyawaki T., Matsushita Y., Okada T., Natsugari H., Kida M. Synthesis and antibacterial activity of 7β-[2-(2-aminothiazol-4-yl)-2-methoxyiminoacetamido]-cephalosporin derivatives and related compounds. J. Antibiot. 34:1981;171-185.
10. J. Blumbach, W. Dürckheimer, J. Reden, H. Sliger, Verfahren zur Herstellung von Penicillinen und Cephalosporinen, OF Patent 27 58 000 Chem. Abstracts (1979) 91:P140858q.
11. W.J. Kim, C.H. Lee, B.J. Kim, G.S. Lee, Process for the preparation of cephem derivatives, GB Patent 2 158 432 Chem. Abstracts (1985) 05:P152813s.
12. S.K. Lim, S.K. Moon, G.S. Lee, Process for preparing cephem derivatives, E Patent 0 175 814 Chem. Abstracts (1986) 105:p114832q.
13. G. Ascher, New process for producing cephalosporin antibiotics and novel intermediates for use in such process and their production, GO Patent 3 002 659 Chem. Abstracts (1980) 94:P47345x.
14. G. Bonfanti, Method for producing crystalline products, E Patent 0 273 156 Chem. Abstracts (1988) 109:P170127h.
15. Lab-base R 2 13, TRIO 1, Copyrights Fisons plc. 1988-1992, Hampden Dates Services Ltd., Eclipse Computer Solutions, Switzerland, 1992.
16. T. Mills, J.C. Roberson, Instrumental Data for Drug Analysis, second ed., vol. 1, Elsevier, Amsterdam, 1987, p. 367.
17. United States XXII Pharmacopeia, The United States Pharmacopeia Convention Inc., 12601 Twinbrook Parkway, Roockville, MD 20852, 1990, pp. 249-250.
18. F.J. Muthadi, M.A. Hassan, in: K. Florey (Ed.), Analytical Profiles of Drug Substances, Academy Press, New York, vol. 11, 1982, p. 159.
19. Dean J.A. Handbook of Organic Chemistry. 1987;1-273 McGraw-Hill, New York.