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Volumn 41, Issue 15, 2000, Pages 2671-2674

Stereoselective radical bromination of α-chloro hydrocinnamic acid derivatives

Author keywords

[No Author keywords available]

Indexed keywords

AMIDE; CARBOXYLIC ACID DERIVATIVE; ESTER DERIVATIVE; HYDROCINNAMIC ACID DERIVATIVE;

EID: 0342264629     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(00)00220-3     Document Type: Article
Times cited : (3)

References (11)
  • 2
    • 0000775245 scopus 로고
    • In Free Radicals
    • For an overview, see Kochi, J. K., Ed. John Wiley & Sons: New York
    • For an overview, see: Skell, P. S.; Shea, K. J. In Free Radicals; Kochi, J. K., Ed. Bridged free radicals. John Wiley & Sons: New York, 1973; Vol. II, pp. 809-852.
    • (1973) Bridged Free Radicals , vol.2 , pp. 809-852
    • Skell, P.S.1    Shea, K.J.2
  • 6
    • 84992571415 scopus 로고    scopus 로고
    • 4. The solvent was removed under reduced pressure and the crude product recrystallised from hexane/ethyl acetate to give pure 1e in 24% yield. All new compounds were fully characterised
    • 4. The solvent was removed under reduced pressure and the crude product recrystallised from hexane/ethyl acetate to give pure 1e in 24% yield. All new compounds were fully characterised.
  • 7
    • 84992618309 scopus 로고    scopus 로고
    • 4 (5 ml) was heated at reflux under nitrogen. The reaction was initiated by irradiation with a 160 W mercury lamp. After 2 h the mixture was cooled and the solvent was removed under reduced pressure. The composition of the crude product was determined by NMR spectroscopy. All new compounds were fully characterised
    • 4 (5 ml) was heated at reflux under nitrogen. The reaction was initiated by irradiation with a 160 W mercury lamp. After 2 h the mixture was cooled and the solvent was removed under reduced pressure. The composition of the crude product was determined by NMR spectroscopy. All new compounds were fully characterised.
  • 8
    • 84992618307 scopus 로고    scopus 로고
    • 3) δ 1.35 (6H, d, J=6.8 Hz), 1.48 (6H, d, J=6.8 Hz), 3.65 (1H, m), 4.16 (1H, m), 5.04 (1H, d, J=10.7 Hz), 5.55 (1H, d, J=10.7 Hz), 7.20-7.40 (5H, m) ppm
    • 3) δ 1.35 (6H, d, J=6.8 Hz), 1.48 (6H, d, J=6.8 Hz), 3.65 (1H, m), 4.16 (1H, m), 5.04 (1H, d, J=10.7 Hz), 5.55 (1H, d, J=10.7 Hz), 7.20-7.40 (5H, m) ppm.
    • Acta Crystallogr.
    • Simpson, J.1    Chan, B.2    Wong, L.S.3    Tan, E.W.4
  • 9
    • 84992677147 scopus 로고    scopus 로고
    • ™, Wavefunction, Inc., 18401 Von Karman, Suite 370, Irvine, California, 92612, USA
    • ™, Wavefunction, Inc., 18401 Von Karman, Suite 370, Irvine, California, 92612, USA.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.