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note
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-1. Totals of 2498 unique reflections were collected at 24±1°C, using the ω-2θ scan technique to a maximum 29 value of 55.0°. Data sets were corrected for Lorentz and polarization effects. Absorption correction was not necessary for the compound. Structure was solved by direct methods using 738 reflections with I>3σ(I). The final residuals were R=0.064 and Rw=0.073.
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