Nanotubes and nanofilaments from carbon monoxide disproportionation over Co/MgO catalysts: I. Growth versus catalyst state

Carbon

Volumn 41, Issue 15, 2003, Pages 2949-2959

  Pinheiro, J P ^a,b   Schouler, M C ^a   Gadelle, P ^a  

^a GRENOBLE INSTITUTE OF TECHNOLOGY   (France)

^b INSTITUTE FOR ENERGY TECHNOLOGY   (Norway)

Author keywords

A. Carbon filaments, Carbon nanotubes; B. Chemical vapor deposition; C. Transmission electron microscopy

Indexed keywords

CARBON MONOXIDE; CATALYSTS; CHEMICAL VAPOR DEPOSITION; DISSOLUTION; PYROLYSIS; TRANSMISSION ELECTRON MICROSCOPY;

CONICAL LAYERS;

CARBON NANOTUBES;

EID: 0242272510     PISSN: 00086223     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0008-6223(03)00410-X     Document Type: Article

References (48)

1. Ivanov V., Nagy J.B., Lambin Ph., Lucas A., Zhang X.B., Zhang X.F., et al. The study of carbon nanotubes produced by catalytic method. Chem. Phys. Lett. 223:1994;329-335.
2. Ivanov V., Fonseca A., Nagy J.B., Lucas A., Lambin Ph., Bernaerts D., et al. Catalytic production and purification of nanotubules having fullerene-scale diameters. Carbon. 33:1995;1727-1738.
3. Fonseca A., Hernardi K., Nagy J.B., Bernaerts D., Lucas A.A. Optimisation of catalytic production and purification of buckytubes. J. Mol. Catal. A. 107:1996;159-168.
4. Hernardi K., Fonseca A., Nagy J.B., Bernaerts D., Lucas A.A. Catalytic synthesis of carbon nanotubes using zeolite support. Zeolites. 17:1996;416-423.
5. Hernardi K., Fonseca A., Piedigrosso P., Delvaux M., Nagy J.B., Bernaerts D., et al. Carbon nanotubes production over Co/silica catalysts. Catal Lett. 48:1997;229-238.
6. Hernardi K., Fonseca A., Nagy J.B., Bernaerts D., Riga J., Lucas A. Catalytic synthesis and purification of carbon nanotubes. Synth. Met. 77:1996;31-34.
7. Hamwi A., Alvergnat H., Bonnamy S., Beguin F. Fluorination of carbon nanotubes. Carbon. 35:1997;723-728.
8. Diaz G., Benaissa M., Santiesteban J.G., José-Yacaman M. Carbon nanotubes prepared by catalytic decomposition of benzene over silica supported cobalt catalysts. Fullerene Sci. Technol. 6:1998;853-866.
9. Kamalakar G., Hwang D.W., Hwang L.P. Synthesis and characterization of multiwalled carbon nanotubes produced using zeolite Co-beta. Mater. Chem. 12:2002;1819-1823.
10. Fonseca A., Hernardi K., Piedigrosso P., Colomer J.F., Mukhopadhyay M., Doome R., et al. Synthesis of single- and multi-wall carbon nanotubes over supported catalysts. Appl. Phys. A. 67:1998;11-22.
11. Piedigrosso P., Konya Z., Colomer J.F., Fonseca A., Van Tendeloo G., Nagy J.B. Production of differently shaped multi-wall carbon nanotubes using various cobalt supported catalysts. Phys. Chem. Chem. Phys. 2:2000;163-1780.
12. Colomer J.F., Stephan C., Lefrant S., Van Tendeloo G., Willems I., Konya Z., et al. Large-scale synthesis of single-wall carbon nanotubes by catalytic chemical vapor deposition (CCVD) method. Chem. Phys. Lett. 317:2000;83-89.
13. Flahaut E., Peigney A., Laurent Ch., Rousset A. Synthesis of single-walled carbon nanotube-Co-MgO composite powders and extraction of the nanotubes. J. Mater. Chem. 10:2000;249-252.
14. 4 over Mo/Co/MgO catalysts. Chem. Phys. Lett. 350:2001;19-26.
15. Ning Y., Zhang X., Wang Y., Sun Y., Shen L., Yang X., et al. Bulk production of multi-wall carbon nanotube bundles on sol-gel prepared catalyst. Chem. Phys. Lett. 366:2002;555-560.
16. Soneda Y., Duclaux L., Beguin F. Synthesis of high quality multi-walled carbon nanotubes from the decomposition of acetylene on iron-group metal catalysts supported on MgO. Carbon. 40:2002;955-971.
17. Willems I., Konya Z., Fonseca A., Nagy J.B. Heterogeneous catalytic production and mechanical resistance of nanotubes prepared on magnesium oxide supported Co-based catalysts. Appl. Catal. 229:2002;229-233.
18. Delpeux S., Szostak K., Frackowiak E., Bonnamy S., Beguin F. High yield of pure multiwalled carbon nanotubes from the catalytic decomposition of acetylene on in-situ formed cobalt nanoparticles. J. Nanosci. Nanotechnol. 2:(5):2002;481-484.
19. Liu S., Zhu J., Mastai Y., Felner I., Gedanken A. Preparation and characteristics of carbon nanotubes filled with cobalt. Chem. Mater. 12:2000;2205-2211.
20. Rana R.K., Koltypin Y., Gedanken A. Synthesis of carbon nanotubes from in situ generated cobalt nanoparticles and carbon monoxide. Chem. Phys. Lett. 344:2001;256-262.
21. Khassin A.A., Yurieva T.M., Zaikovskii V.I., Parmon V.N. Effect of metallic cobalt particles size on occurrence of CO disproportionation. Role of fluidized metallic cobalt-carbon solution in carbon nanotube formation. React. Kinet. Catal. Lett. 64:1998;63-71.
22. Khassin A.A., Yur'eva T.M., Zaikovskii V.I., Plyasova L.M., Parmon V.N. Structural evolution of a Co-Mg oxide catalyst in hydrogen and carbon monoxide atmospheres: effect of the cobalt particle size on the structure of carbon formed in the reaction of CO disproportionation. Kinet. Catal. 39:1998;400-410.
23. 3 catalysts. Carbon. 38:2000;1469-1479.
24. 3 catalysts. Solid State Commun. 123:2002;161-166.
25. 4 or CO on a Ni-MgO catalyst. Carbon. 35:1997;1495-1501.
26. 4 and disproportionation of CO. Carbon. 38:2000;139-143.
27. Ruckenstein E., Wang H.Y. Effect of calcination conditions on the species formed and the reduction behavior of the cobalt-magnesia catalysts. Catal. Lett. 70:2000;15-21.
28. Wang H.Y., Ruckenstein E. Formation of filamentous carbon during methane decomposition over Co-MgO catalysts. Carbon. 40:2002;1911-1917.
29. Nolan P.E., Lynch D.C., Cutler A.H. Carbon deposition and hydrocarbon formation on group VIII metal catalysts. J. Phys. Chem. B. 102:1998;4165-4175.
30. Ros T.J., Van Dillen A.J., Geus J.W., Koningsberger D.C. Surface structure of untreated parallel and fishbone carbon nanofibres: an infrared study. Chem. Phys. Chem. 2:2002;209.
31. Walker P.L.J. Jr., Thomas J.M. The catalysed disproportionation of carbon monoxide. Carbon. 8:1970;103-104.
32. Potczna-Petru D., Krajczy L. Microstructure evolution of Co particles supported on carbon induced by oxidation-reduction treatment. J. Mater. Sci. Lett. 14:1995;1294-1297.
33. Potczna-Petru D., Krajczyk L. Nanostructural characterization of Co-C interaction in a thin film system. Carbon. 37:1999;2067-2070.
34. Audier M., Guyot P. Etude par microscopie électronique de la morphologie et de la structure cristalline de micro-particules de cobalt. J. Microsc. Spectrosc. Electron. 8:1983;261-268.
35. Audier M., Guyot P. Etude par microscopie électronique des transformations structurales de micro-particules de cobalt contenant du carbone en insertion. I. Caractérisation cristallographique et morphologique. J. Microsc. Spectrosc. Electron. 10:1985;8-16.
36. 2C→h.c. J. Microsc. Spectrosc. Electron. 10:1985;17-28.
37. Peigney A., Laurent Ch., Dobigeon F., Rousset A. Carbon nanotubes grown in situ by a novel catalytic method. J. Mater. Res. 12:(3):1997;613-615.
38. Peigney A., Coquay P., Flahaut E., Vandenberghe R.E., De Grave E., Laurent C. A study of the formation of single- and double-walled carbon nanotubes by a CVD method. J. Phys. Chem. B. 105:2001;9699-9710.
39. Li W.Z., Wen J.G., Yu Y., Ren Z.F. Effect of gas pressure on the growth and structure of carbon nanotubes by chemical vapor deposition. Appl. Phys. A. 73:2001;259-264.
40. Li W.Z., Wen J.G., Ren Z.F. Effect of temperature on growth and structure of carbon nanotubes by chemical vapor deposition. Appl. Phys. A. 74:2001;397-402.
41. Laurent C., Flahaut E., Peigney A., Rousset A. Metal nanoparticles for the catalytic synthesis of carbon nanotubes. New J. Chem. 1998;1229-1237.
42. Dai H., Rinzler A.G., Nikolaev P., Thess A., Colbert D.T., Smalley R.E. Single-wall nanotubes produced by metal-catalysed disproportionation of carbon monoxide. Chem. Phys. Lett. 260:1996;471-475.
43. Kukovitsky E.F., L'vov S.G., Sainov N.A., Shustov V.A., Chernozatonskii L.A. Correlation between metal catalyst particle size and carbon nanotube growth. Chem. Phys. Lett. 355:2002;497-503.
44. Herrera J.E., Balzano L., Borgna A., Alvarez W.E., Resaco D.E. Relationship between the structure/composition of Co-Mo catalysts and their ability to produce single-walled carbon nanotubes by CO disproportionation. J. Catal. 204:2001;129-145.
45. Alvarez W.E., Kitiyanan B., Borgna A., Resaco D.E. Synergism of Co and Mo in the catalytic production of single-wall carbon nanotubes by decomposition of CO. Carbon. 39:2001;547-558.
46. Zhu H., Xu C., Wei B., Wu D. A new method for synthesizing double-walled carbon nanotubes. Carbon. 40:2002;2023-2025.
47. Zhou Z., Ci L., Chen X., Tang D., Yan X., Liu D., et al. Controllable growth of double wall carbon nanotubes in a floating catalytic system. Carbon. 41:2003;337-342.
48. Li W.Z., Wen J.G., Sennet M., Ren Z.F. Clean double-walled carbon nanotubes synthesized by CVD. Chem. Phys. Lett. 368:2003;299-306.