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note
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2Sb: C, 53.64; H, 3.71. Found C, 53.68; H, 3.89.
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22
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0242355352
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note
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-3. The final cycle of full-matrix least-squares refinement was based on 10995 observed reflections and 835 variable parameters and converged at R1 = 0.0988 (1 > 2σ(I)) and wR2 (all data) = 0.1917 with a GOF = 1.382.
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23
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Olefin synthesis via a hexacoordinate 1,2-oxastibetanide, see: Kojima, S.; Takagi, R.; Akiba, K.-y. J. Am. Chem. Soc. 1997, 119, 5970.
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