The characterisation of lead fatty acid soaps in 'protrusions' in aged traditional oil paint

Polyhedron

Volumn 22, Issue 24, 2003, Pages 3171-3179

  Plater, M John ^a   De Silva, Ben ^a   Gelbrich, Thomas ^b   Hursthouse, Michael B ^b   Higgitt, Catherine L ^c   Saunders, David R ^c  

^a UNIVERSITY OF ABERDEEN   (United Kingdom)

^b UNIVERSITY OF SOUTHAMPTON   (United Kingdom)

^c National Gallery   (United Kingdom)

Author keywords

Hydrothermal; Lead soaps; Lead tin yellow; Palmitic acid; Red lead; Stearic acid

Indexed keywords

CARBOXYLATION; CRYSTAL STRUCTURE; LEAD; LEAD COMPOUNDS; PAINT; PALMITIC ACID; SATURATED FATTY ACIDS; SINGLE CRYSTALS; STEARIC ACID; TIN; UNSATURATED FATTY ACIDS;

AZELAIC ACID; DICARBOXYLIC ACID; FATTY ACID SOAPS; HYDROTHERMAL; LEAD SOAP; LEAD-TIN; LEAD-TIN YELLOW; OIL PAINTS; RED-LEAD; SYNTHESISED;

FOURIER TRANSFORM INFRARED SPECTROSCOPY;

AZELAIC ACID; DICARBOXYLIC ACID; FATTY ACID; LEAD; LEAD AZELATE; LEAD CARBOXYLATE SOAP; LEAD SOAP; LEAD STEARATE; OIL; PAINT; PALMITATE LEAD; PALMITIC ACID; SOAP; STEARIC ACID; UNCLASSIFIED DRUG; UNSATURATED FATTY ACID;

ARTICLE; CRYSTAL STRUCTURE; CRYSTALLOGRAPHY; HYDROTHERMAL SYNTHESIS; INFRARED SPECTROSCOPY; OXIDATION; POLYMERIZATION; STRUCTURE ANALYSIS; SYNTHESIS; X RAY ANALYSIS;

EID: 0142153143     PISSN: 02775387     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0277-5387(03)00461-3     Document Type: Article

References (33)

1. C. Higgitt, M. Spring, D. Saunders, Pigment-medium interactions in oil paint films containing red lead or lead-tin yellow, National Gallery Technical Bulletin, vol. 24, National Gallery Company, London, 2003 (in press).
2. (a) R.M.A. Heeren, J.J. Boon, P. Noble, J. Wadum, in: J. Bridgland (Ed.), 12th Triennial Meeting Lyon, ICOM Committee for Conservation Preprints, James and James, London, 1999, p. 228;
3. (b) J. van der Weerd, J.J. Boon, M. Geldof, R.M.A. Heeren, P. Noble, Zeitschrift fur Kunsttechnologie und Konservierung 16 (2002) 36;
4. (c) J. van der Weerd, Ph.D. Thesis, FOM Institute for Atomic and Molecular Physics, Amsterdam, 2002.
5. (a) M.-C. Corbeil, L. Robinet, Powder Diffr. 17 (2002) 52;
6. (b) L. Robinet, M.-C. Corbeil, Stud. Conserv. 48 (2003) 23.
7. M.S. Akanni, E.K. Okoh, H.D. Burrows, H.A. Ellis, Thermochim. Acta 208 (1991) 1.
8. (a) E.J. Dunn Jr., in: T.C. Patton (Ed.), Red Lead, Pigment Handbook, Properties and Economics, vol. 1, Wiley-Interscience, New York, 1973, p. 837;
9. (b) J.E.O. Mayne, in: T.C. Patton (Ed.), Pigment Electrochemistry, Pigment Handbook, Characterisation and Physical Relationships, vol. 3, Wiley-Interscience, New York, 1973, p. 457.
10. E. Rocca, J. Steinmetz, Corros. Sci. 43 (2001) 891.
11. J.-M. Rueff, N. Masciocchi, P. Rabu, A. Sironi, A. Skoulios, Chem. Eur. J. 8 (2002) 1813.
12. J.-M. Rueff, N. Masciocchi, P. Rabu, A. Sironi, A. Skoulios, Eur. J. Inorg. Chem. 11 (2001) 2843.
13. J.S. Mills, R. White, The Organic Chemistry of Museum Objects, second ed., Butterworths, London, 1994, 33 and 171.
14. M.R.St.J. Foreman, M.J. Plater, J.M.S. Skakle, J. Chem. Soc., Dalton Trans. (2001) 1897.
15. Lacouture, M. Francois, C. Didierjean, J.P. Rivera, E. Rocca, J. Steinmetz, Acta Crystallogr., Sect. C. 57 (2001) 530.
16. G. Feio, H.D. Burrows, C.F.G.C. Geraldes, T.J.T. Pinheiro, Liq. Crystals 9 (1991) 417.
17. M.A. Mesubi, J. Mol. Struct. 81 (1982) 61.
18. M.R.St.J. Foreman, T. Gelbrich, M.B. Hursthouse, M.J. Plater, Inorg. Chem. Commun. 13 (2000) 234.
19. M.J. Plater, M.R.St.J. Foreman, E. Coronado, C.J. Gó mez-García, A.M.Z. Slawin, J. Chem. Soc., Dalton Trans. (1999) 4209.
20. R. White, J. Pilc, in: The Application of FTIR-Microscopy to the Analysis of Paint Binders in Easel Paintings, National Gallery Technical Bulletin, vol. 16, National Gallery Company, London, 1995, p. 73.
21. J. MacGee, K.G. Allen, J. Chromatogr. 100 (1974) 35.
22. R.C. Mehrotra, R. Bohra, Metal Carboxylates, Academic Press, London, 1983 (Chapter 2).
23. R.C. Weast (Ed.), Handbook of Chemistry and Physics, 68th ed., CRC Press, Boca Raton, 1987, p. B-100.
24. A.M. Duisenberg, DIRAX, J. Appl. Cryst. 25 (1992) 92.
25. R. Hooft, B.V. Nonius, COLLECT: data collection software, 1998.
26. (a) R.H. Blessing, SORTAV, Acta Cryst. A 51 (1995) 33;
27. (b) R.H. Blessing, J. Appl. Cryst. 30 (1997) 421.
28. P.T. Beurskens, G. Beurskens, W.P. Bosman, R. de Gelder, S. Garcia-Granda, R.O. Gould, R. Israël, J.M.M. Smits, DIRDIF-96, Crystallography Laboratory, University of Nijmegen, The Netherlands, 1996.
29. G.M. Sheldrick, SHELXL97, University of Göttingen, Germany, 1997.
30. E.J. Dunn Jr., in: R.R. Myers, J.S. Long (Eds.), Lead Pigments, Treatise on Coatings, Pigments, Part 1, vol. 3, Marcel Dekker, New York, 1975, p. 403.
31. R.G. Bryant, V.P. Chacko, M.C. Etter, Inorg. Chem. 23 (1984) 3580.
32. W. Clegg, I.R. Little, B.P. Straughan, Acta. Cryst. C 42 (1986) 1319.
33. I.R. Amiraslanov, N.Kh. Dzhafarov, G.N. Nadzhafov, Kh.S. Mamedov, E.M. Movsumov, B.T. Usubaliev, Zh. Strukt. Khim. 21 (1980) 131.