An improved HPLC-enzyme-reactor method for the determination of oxalic acid in complex matrices

Clinica Chimica Acta

Volumn 261, Issue 2, 1997, Pages 131-139

  Honow R ^a   Bongartz, D ^a   Hesse, A ^a  

^a UNIVERSITY OF BONN   (Germany)

Author keywords

Electrochemical detection; Enzymatic kit; Enzymatic reactor; HPLC; Oxalic acid

Indexed keywords

OXALIC ACID; OXIDOREDUCTASE;

ACCURACY; AMPEROMETRY; ARTICLE; CONTROLLED STUDY; DRUG BLOOD LEVEL; DRUG DETERMINATION; DRUG URINE LEVEL; ELECTROCHEMICAL DETECTION; ENZYME ASSAY; ENZYME IMMOBILIZATION; FOOD ANALYSIS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; HUMAN TISSUE; PRIORITY JOURNAL; TECHNIQUE;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; HUMANS; OXALATES; OXALIC ACID; SENSITIVITY AND SPECIFICITY;

EID: 0142130498     PISSN: 00098981     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0009-8981(97)06521-2     Document Type: Article

References (20)

1. Hodgkinson A, Williams A. An improved colorimetric procedure for urine oxalate. Clin Chim Acta 1972;36:127-132.
2. Zarembski PM, Hodgkinson A. The fluorimetric determination of oxalate in blood and other biological fluids. Biochem J 1965;96:717-721.
3. Koehl C, Abeassis I. Determination of oxalic acid in urine by atomic absorption spectrophotometry. Clin Chim Acta 1976;70:71-77.
4. Wolthers BG, Hayer M. The determination of oxalic acid in plasma and urine by means of capillary gas chromatography. Clin Chim Acta 1982;120:87-102.
5. Koolstra W, Wolthers BG, Hayer M, Eizinga H. Development of a reference method for determining urinary oxalate by means of isotope dilution - mass spectrometry (ID - MS) and its use in testing existing assays for urinary oxalate. Clin Chim Acta 1987;170:227-236.
6. Classen A, Hesse A. Measurement of urinary oxalate: an enzymatic and an ion chromatographic method compared. J Clin Chem Clin Biochem 1987;25:95-99.
7. Petrarulo M, Cerelli E, Marangella M, Maglienti F, Linari F. Ion-chromatographic determination of plasma oxalate reexamined. Clin Chem 1993;39:537-9.
8. Skotty DR, Nieman TA. Determination of oxalate in urine and plasma using reversed-phase ion-pair high-performance liquid chromatography with tris(2,2′-bipyridyl)ruthenium(11)-electrogenerated chemiluminescence detection. J Chromatogr B Biomed Appl 1995;665:27-36.
9. Galensa R, Müller G, Schirmer A, Hippe H, Stadler H. Bestimmung von Lebensmittelinhaltsstoffen durch HPLC - Enzymreaktor-Kopplung. Lebens-mittelchem Gerichtl Chem 1988;42:84-85.
10. Yamato S, Wakabayashi H, Nakajima M, Shimada K. Amperometric determination of oxalate in plasma and urine by liquid chromatography with immobilized oxalate oxidase. J Chromatogr B Biomed Appl 1994;656(1):29-35.
11. Mazzachi BC, Teuber JK, Ryall RG. Factors affecting measurement of urinary oxalate. Clin Chem 1984;30(8):1339-1343.
12. Lewin S. Recent advances in the biology of vitamin C. In: Birch GG, Parker KJ, editors. Vitamin C: Recent aspects of its physiological and technological importance. London: Applied Science Publishers, 1974:221-251.
13. Kasidas GP, Rose GA. Oxalate content of some common foods: determination by an enzymatic method. J Hum Nutr 1980;34:255-266.
14. Frehse H, Thier HP. Die Ermittlung der Nachweisgrenzen und Bestimmungsgrenzen bei Rückstandsanalysen nach dem neuen DFG-Konzept, GIT Fachz La 1991;4:285-290.
15. Haeckel R. Statistische Probleme beim Vergleich von klinisch-chemischen Analysen-Verfahren. J Clin Chem Clin Biochem 1980;18:433-437.
16. Passing H, Bablok W. A New Biometrical Procedure for testing the Equality of Measurements from Two Different Analytical Methods. J Clin Chem Clin Biochem 1983;21:709-720.
17. Kasidas GP. Assaying of oxalate in plasma. In: Rose GA, editor. Oxalate metabolism in relation to urinary stone. London: Springer, 1988:45-64.
18. Wilson DM, Liedtke RR. Modified enzyme-based colorimetric assay of urinary and plasma oxalate with improved sensitivity and no ascorbate interference: reference values and sample handling procedures. Clin Chem 1991;37(7): 1229-35.
19. Barratt TM, Kasidas GP, Murdoch I, Rose GA. Urinary oxalate and glycolate excretion and plasma oxalate concentration. Arch Dis Child 1991;66(4):501-503.
20. Bland LM, Altman DG. Statistical method for assessing agreement between two methods of clinical measurement. Lancet 1986;1(8476):307-310.