Iron-nickel mixed metal clusters: Synthesis, reactivity and vibrational spectroscopy of [FeNi5(CO)13]2-. Solid state structure of the anions [FeNi5(CO)13]2- and [Fe3Ni(CO)12]2-

Inorganica Chimica Acta

Volumn 350, Issue , 2003, Pages 107-113

  Della Pergola, Roberto ^a   Diana, Eliano ^b   Garlaschelli, Luigi ^c   Peli, Giulia ^c   Manassero, Mario ^d   Sansoni, Mirella ^d   Strumolo, Donatella ^c  

^a UNIVERSITY OF MILANO BICOCCA   (Italy)

^b UNIVERSITY OF TURIN   (Italy)

^c Dipartimento di Chimica Inorganica e Metallorganica   (Italy)

^d Dipto Chim Strutturale S   (Italy)

Author keywords

Heterometallic clusters; Iron; Nickel; Solid state structures; Vibrational spectroscopy

Indexed keywords

IRON; IRON COMPOUNDS; LIGANDS; NEGATIVE IONS; NICKEL; VIBRATIONAL SPECTROSCOPY;

CARBONYL GROUPS; EDGE-BRIDGING; HETEROMETALLIC CLUSTERS; IRON-NICKEL; MIXED METAL CLUSTERS; NICKEL CLUSTERS; NUCLEARITY; SOLID-STATE STRUCTURES;

NICKEL COMPOUNDS;

ACETONITRILE; ACID; ANION; CARBON MONOXIDE; CARBONYL DERIVATIVE; IRON DERIVATIVE; NICKEL;

ARTICLE; CHEMICAL STRUCTURE; ROOM TEMPERATURE; SOLID STATE; SPECTROSCOPY; STRUCTURE ANALYSIS; VIBRATION;

EID: 0142088980     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0020-1693(02)01495-0     Document Type: Article

References (43)

1. Albano V.G., Canè M., Iapalucci M.C., Longoni G., Monari M. J. Organomet. Chem. 407:1991;C9.
2. Demartin F., Iapalucci M.C., Longoni G. Inorg. Chem. 32:1993;5536.
3. M.R. Churchill, J. Wormald, J. Chem. Soc., Dalton Trans. (1974) 2410.
4. Beattie J.K., Masters A.F., Meyer J.T. Polyhedron. 14:1995;829. and references therein.
5. Calderoni F., Demartin F., Iapalucci M.C., Longoni G. Angew. Chem., Int. Ed. Engl. 35:1996;2225.
6. Anema S.G., Mackay K.M., Nicholson B.K. Inorg. Chem. 28:1989;3158.
7. Whitmire K.H., Lagrone C.B., Churchill M.R., Fettinger J.C., Robinson B.H. Inorg. Chem. 26:1987;3491.
8. A. Ceriotti, F. Demartin, B.T. Heaton, P. Ingallina, G. Longoni, M. Manassero, M. Marchionna, N. Masciocchi, J. Chem. Soc., Chem. Commun. (1989) 786.
9. Anema S.K., Mackay K.M., Nicholson B.K. J. Organomet. Chem. 372:1989;25.
10. Canè M., Iapalucci M.C., Longoni G., Demartin F., Grossi L. Mater. Chem. Phys. 29:1991;395.
11. Rieck D.F., Gavney J.A., Norman R.L., Hayashi R.K., Dahl L.F. J. Am. Chem. Soc. 114:1992;10369.
12. P. Henderson, M. Rossignoli, R.C. Burns, M.L. Scudder, D.C. Craig, J. Chem. Soc., Dalton Trans. (1994) 1641.
13. Rieck D.F., Montag R.A., McKechnie T.S., Dahl L.F. J. Am. Chem. Soc. 108:1986;1330.
14. Luo S., Whitmire K.H. Inorg. Chem. 28:1989;1424 C. Femoni, M.C. Iapalucci, G. Longoni, P.H. Svennson, J. Chem. Soc., Chem. Commun. (2000) 655.
15. Eveland J.R., Saillard J.Y., Whitmire K.H. Inorg. Chem. 36:1997;330 V.G. Albano, F. Demartin, M.C. Iapalucci, G. Longoni, M. Monari, P. Zanello, J. Chem. Soc., Dalton Trans. (1992) 497.
16. Ceriotti A., Chini P., Fumagalli A., Koetzle T.F., Longoni G., Takusagawa F. Inorg. Chem. 23:1984;1363.
17. Sappa E., Tiripicchio A., Camellini M.T. J. Organomet. Chem. 199:1980;243.
18. Mlekuz M., Bougeard P., Sayer B.G., Peng S., McGlinchey M.J., Marinetti A., Saillard J.Y., Naceur J.B., Mentzen B., Jaouen G. Organometallics. 4:1985;1123.
19. Deck W., Powell A.K., Vahrenkamp H. J. Organomet. Chem. 411:1991;431.
20. Marr A.C., Spencer D.J.E., Schroder M. Coord. Chem. Rev. 219-221:2001;1055.
21. R.Della. Pergola, V. Betti, A. Ceriotti, M. Fontani, M. Manassero, M. Sansoni, P. Zanello, XX Congresso Nazionale della Società Chimica Italiana, Rimini, 4-9 June 2000.
22. Calabrese J.C., Dahl L.F., Cavalieri A., Chini P., Longoni G., Martinengo S. J. Am. Chem. Soc. 96:1974;2616.
23. Kettle S.F.A., Diana E., Rossetti R., Stanghellini P.L. Inorg. Chem. 37:1998;6502.
24. Panda R.N., Gajbhiye N.S. J. Appl. Phys. 86:1999;3295.
25. Matar S., Mohn P., Demazeau G., Schwarz K. J. Magn. Magn. Mater. 101:1991;251.
26. Nagaki D.A., Lower L.D., Longoni G., Chini P., Dahl L.F. Organometallics. 5:1986;1764.
27. Ceriotti A., Chini P., Della Pergola R., Longoni G. Inorg. Chem. 22:1983;1595.
28. Longoni G., Chini P., Lower L.D., Dahl L.F. J. Am. Chem. Soc. 97:1975;5035.
29. K. Farmery, M. Kilner, R. Greatrex, N.N. Greenwood, J. Chem. Soc. (A) (1969) 2339.
30. Bachman R.E., Whitmire K.H. Acta Crystallgr., Sect. C. 49:1993;1121.
31. Beattie J.K., Hambley T.W., Masters A.F., Meyer J.T. Inorg. Chim. Acta. 213:1993;49.
32. Brivio E., Ceriotti A., Della Pergola R., Garlaschelli L., Manassero M., Sansoni M. J. Cluster Sci. 6:1995;271.
33. Fumagalli A., Italia D., Malatesta M.C., Ciani G., Moret M., Sironi A. Inorg. Chem. 35:1996;1765.
34. Della Pergola R., Garlaschelli L., Demartin F., Manassero M., Masciocchi N., Longoni G. J. Organomet. Chem. 352:1988;C59.
35. Kettle S.F.A., Diana E., Rossetti R., Stanghellini P.L., Della Pergola R., Garlaschelli L. Inorg. Chim. Acta. 227:1994;241.
36. Kettle S.F.A., Boccaleri E., Diana E., Iapalucci M.C., Rossetti R., Stanghellini P.L. Inorg. Chem. 41:2002;3620.
37. Shriver D.F., Dredzon M.A. The Manipulation of Air-Sensitive Compounds. second ed:1986;Wiley, New York.
38. Ceriotti A., Longoni G., Piva G. Inorg. Synth. 26:1989;312.
39. SAINT, Reference manual, Siemens Energy and Automation, Madison, WI, 1994-1996.
40. G.M. Sheldrick, SADABS, Empirical Absorption Correction Program, University of Göttingen, Göttingen, Germany, 1997.
41. Frenz B.A. Comput. Phys. 2:1988;42 Crystallographic Computing, vol. 5, Oxford University Press, Oxford, 1991, p. 126, Chapter 11.
42. International Tables for X-ray Crystallography, vol. 4, Kynoch Press, Birmingham, 1974.
43. Sheldrick G.M. SHELXS86, Program for the Solution of Crystal Structures. 1985;University of Göttingen, Göttingen, Germany.