An application of the XiX decoupling for solid state 13C NMR with mobile samples

Journal of Magnetic Resonance

Volumn 165, Issue 1, 2003, Pages 180-183

  Ashida, Jun ^a   Asakura, Tetsuo ^b  

^a Varian Technologies Japan Ltd   (Japan)

^b TOKYO UNIVERSITY OF AGRICULTURE AND TECHNOLOGY   (Japan)

Author keywords

High resolution solid state NMR; Mobile solid samples; XiX decoupling

Indexed keywords

FREQUENCY MODULATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; OPTICAL RESOLVING POWER; PROTONS;

DECOUPLING POWER;

SOLID STATE PHYSICS;

EID: 0142075312     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1016/S1090-7807(03)00269-6     Document Type: Article

References (12)

1. Mehring M. Principles of High Resolution NMR in Solids. 1983;Springer, Berlin.
2. Fyfe C.A. Solid State NMR for Chemists. 1983;CFC Press, Guelph.
3. Schmidt-Rohr K., Spiess H.W. Multidimensional Solid-State NMR and Polymers. 1994;Academic Press, London.
4. Freeman R. A Handbook of Nuclear Magnetic Resonance. 1988;Longman Group UK Limited, London.
5. Bennett A.E., Rienstra C.M., Auger M., Lakshmi K.V., Griffin R.G. J. Chem. Phys. 103:1995;6951-6958.
6. Gan Z., Ernst R.R. Solid State Nucl. Magn. Reson. 8:1997;153-159.
7. 1H decoupling with third averaging in solid NMR. Chem. Phys. Lett. 341:2000;540-544.
8. Detken A., Hardy E.H., Ernst M., Meier B.H. Simple and efficient decoupling in magic-angle spinning solid-state NMR: the XiX scheme. Chem. Phys. Lett. 356:2002;298-304.
9. Ernst M. Heteronuclear spin decoupling in solid-state NMR under magic-angle sample spinning. J. Magn. Reson. 162:2003;1-34.
10. Pratum T.P. Correction for anisotropic off-resonance decoupling effects in CPMAS of moderate susceptibility materials. Chem. Phys. Lett. 172:1990;291-294.
11. 13C MAS NMR linewidths. Phase-modulated irradiation for efficient heteronuclear decoupling in rapidly rotating solids. J. Magn. Reson. A. 107:1994;129-133.
12. 13C magic-angle spinning NMR spectra. Chem. Phys. Lett. 227:1994;639-644.