1H{15N} GHMQC study of 5,7-diphenyl-1,2,4-triazolo[1, 5-a] pyrimidine and 1H, 13C and 15N NMR coordination shifts in Au(III) chloride complexes of 1,2,4-triazolo[1,5-a] pyrimidines

Magnetic Resonance in Chemistry

Volumn 40, Issue 8, 2002, Pages 529-532

  Szłyk, Edward ^a   Pazderski, Leszek ^a   Łakomska, Iwona ^a   Kozerski, Lech ^b   Sitkowski, Jerzy ^b  

^a NICOLAUS COPERNICUS UNIVERSITY   (Poland)

^b NATIONAL MEDICINES INSTITUTE   (Poland)

Author keywords

1,2,4 triazolo 1,5 a pyrimidines; 13C NMR; 1H NMR; 1N NMR; Au(III) complexes; Coordination shifts; GHMBC; GHMQC; NMR

Indexed keywords

AROMATIC COMPOUNDS; CHLORINE COMPOUNDS; COMPLEXATION; COORDINATION REACTIONS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PALLADIUM COMPOUNDS; PLATINUM COMPOUNDS; SYNTHESIS (CHEMICAL);

1,2,4-TRIAZOLO[1,5-A]PYRIMIDINE; 13C NMR; 1H NMR; 1N NMR; AU(III) COMPLEX; COORDINATION SHIFT; GHMBC; GHMQC; NMR SPECTRUM; SPECTRA'S;

GOLD COMPOUNDS;

5,7 DIPHENYL 1,2,4 TRIAZOLO[1,5 A]PYRIMIDINE; CHLORIDE; COORDINATION COMPOUND; GOLD COMPLEX; ION; PALLADIUM COMPLEX; PLATINUM COMPLEX; PYRIMIDINE DERIVATIVE; TRIAZOLE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; COMPLEX FORMATION; MOLECULAR DYNAMICS; NITROGEN NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE; PROTON NUCLEAR MAGNETIC RESONANCE; SPECTRUM;

EID: 0142015466     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/mrc.1051     Document Type: Article

References (28)

1. Fischer G. Z. Chem. 1990; 30: 305.
2. Fischer G. Adv. Het. Chem. 1993; 57: 81.
3. Kleinpeter E, Borsdorf R, Fischer G, Hofmann HJ. J. Prakt. Chem. 1972; 314: 515.
4. La Noce T, Giuliani AM. Tetrahedron 1978; 34: 2927.
5. Bajwa JS, Sykes PJ. J. Chem. Soc., Perkin Trans 1 1979; 3085.
6. Hori M, Tanaka K, Kataoka T, Shimizu H, Jimai E. J. Chem. Soc., Perkin Trans. 11985; 2333.
7. Pugmire RJ, Smith JC, Grant DM, Stanovnik B, Tisler B, Vercek B. J. Heterocycl. Chem. 1987; 24: 805.
8. Wiench JW, Stefaniak L, Webb GA. Magn. Reson. Chem. 1994; 32: 373.
9. Paudler WW, Sheets RM, Goodson B. Org. Magn. Reson. 1982; 18: 87.
10. Künstlinger M, Breitmeier E. Synthesis 1983; 1: 44.
11. Stefaniak L, Witanowski M, Mahmoud U, Roberts JD, Webb GA. J. Crystallogr. Spectrosc. Res. 1989; 19: 159.
12. Kleinpeter E, Thomas S, Fischer G. J. Mol. Struct. 1995; 355: 273.
13. Szłyk E, Grodzicki A, Pazderski L, Wojtczak A, Chatłas J, Wrzeszcz G, Sitkowski J, Kamieński B. J. Chem. Soc., Dalton Trans. 2000; 867.
14. Szłyk E, Grodzicki A, Pazderski L, Bednarek E, Kamieński B. Polyhedron 2000; 19: 965.
15. Grodzicki A, Szłyk E, Pazderski L, Goliński A, Haasnoot JG. Magn. Reson. Chem. 1996; 34: 725.
16. Salas J, Romero MA, Sanchez MP, Quiros M. Coord. Chem. Rev 1999; 193-195: 1119.
17. Szłyk E, Pazderski L, Łakomska I, Surdykowski A, Głowiak T, Sitkowski J, Kozerski L. Polyhedron 2002; 21: 343.
18. Best SL, Sadler PJ. Gold Bull. 1996; 29: 87.
19. Berners-Price SJ, Sadler PJ. Coord. Chem. Rev. 1996; 151: 1.
20. Sadler PJ, Sue RE. Handb. Met.-Ligand Interact. Biol. Fluids: Bioinorg. Chem. 1995; 2: 1039-1051.
21. Sadler PJ, Sue RE. Met.-Based Drugs 1994; 2: 107.
22. Bülow C, Haas K. Chem. Ber. 1909; 42: 4640.
23. Adams HN, Strähle J. Z. Anorg. Allg. Chem. 1982; 485: 65.
24. Strähle J, Gelinek J, Kölmel M. Z. Anorg. Allg. Chem. 1979; 456: 241.
25. Zou J, Zijian G, Parkinson J, Chen Y, Sadler PJ. Chem. Commun. 1999; 1359.
26. Witanowski M, Stefaniak L, Webb GA. Annu. Rep. NMR Spectrosc. 1993; 25: 56.
27. Witanowski M, Stefaniak L, Webb GA. Annu. Rep. NMR Spectrosc. 1993; 25: 40.
28. Mason J. Chem. Rev. 1981; 81: 205.