Novel nuclear magnetic resonance techniques for the study of quadrupolar nuclei in clays and other layered materials

Clay Minerals

Volumn 38, Issue 3, 2003, Pages 259-278

  Rocha, J ^a   Morais, C M ^a,b   Fernandez, C ^b  

^a UNIVERSITY OF AVEIRO   (Portugal)

^b Normandy University   (France)

Author keywords

Clay; MQMAS; Nuclear magnetic resonance spectroscopy; Quadrupolar nuclei; Radio frequency radiation; STMAS

Indexed keywords

BORON; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; OXYGEN; SODIUM;

LAYERED MATERIALS;

CLAY MINERALS;

CLAY; LAYERED MEDIUM; NUCLEAR MAGNETIC RESONANCE; SPECTROSCOPY;

EID: 0141992634     PISSN: 00098558     EISSN: None     Source Type: Journal    
DOI: 10.1180/0009855033830094     Document Type: Article

References (75)

1. Ai X., Deng F., Dong J., Chen L. & Ye C. (2002) Stability of layered sodium disilicate during hydration process as studied by multinuclear solid state NMR spectroscopy. Journal of Physical Chemistry, 106, 9237-9244.
2. Amoureux J.P. & Fernandez C. (1998) Triple, quintuple and higher order multiple quantum MAS NMR of quadrupolar nuclei. Solid State Nuclear Magnetic Resonance, 10, 211-223.
3. Amoureux J.P. & Pruski M. (2002) Advances in MQMAS. Pp. 226-251 in: Encyclopedia of Nuclear Magnetic Resonance vol. 9 (D.M. Grant & R.K. Harris, editors). Wiley, Chichester, UK.
4. Amoureux J.P., Fernandez C. & Dumazy Y. (1995) A useful tool for the elaboration of new solid-state experiments: PULSAR. Journal de Chimie Physique, 2, 1939-1949.
5. Amoureux J.P., Fernandez C. & Steuernagel S. (1996) Z filtering in MQMAS NMR. Journal of Magnetic Resonance A, 123, 116-118.
6. Amoureux J.P., Morais C., Trebosc J., Rocha J. & Fernandez C. (2003) I- STMAS, a new high-resolution solid-state NMR method for half-integer quadrupolar nuclei. Solid State Nuclear Magnetic Resonance, 23, 213-223.
7. Ashbrook S.E. & Wimperis S. (1998) Multiple-quantum cross-polarization in MAS NMR of quadrupolar nuclei. Chemical Physics Letters, 288, 509-517.
8. Ashbrook S.E. & Wimperis S. (2000) Multiple-quantum cross-polarization and two-dimensional MQMAS NMR of quadrupolar nuclei. Journal of Magnetic Resonance, 147, 238-248.
9. Ashbrook S.E. & Wimperis S. (2001) Novel two-dimensional methods that combine single-quantum cross-polarization and multiple-quantum MAS of quadrupolar nuclei. Chemical Physics Letters, 340, 500-508.
10. Ashbrook S.E. & Wimperis S. (2002) High-resolution NMR spectroscopy of quadrupolar nuclei in solids: Satellite-transition MAS with self-compensation for magic-angle Misset. Journal of the American Chemical Society, 124, 11602-11603.
11. 27Al MAS NMR of mechanically treated mixtures of kaolinite and gibbsite. Journal of Physical Chemistry B, 104, 6408-6416.
12. Ashbrook S.E., Antonijevic S., Berry A.J. & Wimperis S. (2002) Motional broadening: an important distinction between multiple-quantum and satellite-transition MAS NMR of quadrupolar nuclei. Chemical Physics Letters, 364, 634-642.
13. Bak M., Rasmussen J.T. & Nielsen N.C. (2000) SIMPSON: A general simulation program for solid-state NMR spectroscopy. Journal of Magnetic Resonance, 147, 296-330.
14. Brown S.P. & Wimperis S. (1997) Two-dimensional multiple-quantum MAS NMR of quadrupolar nuclei: A Comparison of Methods. Journal of Magnetic Resonance, 128, 42-61
15. Brown S.P., Heyes S.J. & Wimperis S. (1996) Two-dimesional MAS multiple-quantum NMR of quadrupolar nuclei. Removal of inhomogeneous second-order broadening. Journal of Magnetic Resonance A, 119, 280-284.
16. Caldarelli S. & Ziarelli F. (2000) Spectral editing of solid-state MAS NMR spectra of half-integer quadrupolar nuclei. Journal of the American Chemical Society, 122, 12015-12016.
17. Chmelka B.F, Mueller K.T., Pines A., Stebbins J., Wu Y. & Zwanziger, J.W. (1989) Oxygen-17 NMR in solids by dynamic-angle spinning and double-rotation. Nature, 339, 42-43.
18. 31P MQHETCOR NMR experiments. Solid State Nuclear Magnetic Resonance, 21, 61-70.
19. 27Al MAS NMR investigation of Laponite and synthetic saponites of variable interlayer charge. Clay Minerals, 38, 63-69.
20. Ding S. & McDowell C.A. (1997) Shaped-pulse excitation in multi-quantum magic-angle spinning spectroscopy of half-integer quadrupole spin systems. Chemical Physics Letters, 270, 81-86.
21. Fenzke D., Freude D., Fröhlich T. & Haase J. (1984) NMR intensity measurements of half-integer quadrupolar nuclei. Chemical Physics Letters, 111, 171-175.
22. Fernandez C., Lang D.P. Amoureux J.P. & Pruski M. (1998) Measurement of heteronuclear dipolar interaction between quadrupolar and spin 1/2 nuclei by MQ REDOR NMR. Journal of the American Chemical Society, 120, 2672-2673.
23. 27Al in microporous aluminophosphates. Solid State Nuclear Magnetic Resonance, 21, 61-70.
24. 2O gels. Journal of the American Chemical Society, 124, 8435-8444.
25. Frydman L. & Harwood J.S. (1995) Isotropic spectra of half-integer quadrupole spins from bidimensional magic-angle-spinning NMR. Journal of the American Chemical Society, 117, 5367-5368.
26. Gan Z. (2000) Isotropic NMR spectra of half-integer quadrupolar nuclei using satellite transitions and MAS. Journal of the American Chemical Society, 122, 3242-3243.
27. Goldbourt A., Machu P.K. & Vega S. (2000) Enhanced conversion of triple to single-quantum coherence in the triple-quantum MAS NMR spectroscopy of spin-5/2 nuclei. Chemical Physics Letters, 320, 448-456.
28. Grey C.P. & Vega A.J. (1995) Determination of the quadrupole coupling constant of the invisble aluminum spins in zeolite HY with IH/27Al. Journal of the American Chemical Society, 117, 8232-8242.
29. Gullion T. (1995) Measurement of dipolar interactions between spin-1/2 and quadrupolar nuclei by rotational-echo, adiabatic-passage, double-resonance NMR. Chemical Physics Letters, 246, 325-330.
30. Gullion T. & Schaefer J. (1989) Detection of weak heteronuclear dipolar coupling by rotational-echo double-resonance nuclear magnetic resonance. Advances in Magnetic Resonance, Vol. 13. Academic Press, San Diego, pp. 57-83.
31. 23Na in a hydrous layered silicate. Solid State Nuclear Magnetic Resonance, 8, 147-151.
32. 23Na MQMAS NMR study of layered materials. Journal of Materials Chemistry, 8, 1073-1079.
33. Hayashi S. (1997) Solid-state NMR study of locations and dynamics of interlayer cations and water in kanemite. Journal of Materials Chemistry, 7, 1043-1048.
34. 27Al CP/MQMAS NMR. Journal of the Iron and Steel Institute of Japan, 88, 730-735.
35. Kentgens A.P.M. & Verhagen R. (1999) Advantages of double frequency sweeps in static, MAS and MQMAS NMR of spin 1=3/2 nuclei. Chemical Physics Letters, 300, 435-443.
36. Lee S.K. & Stebbins J.F. (2003) O atom sites in natural kaolinite and muscovite: O-17 MAS and 3QMAS NMR study. American Mineralogist, 88, 493-500.
37. 27Al MAS and 3QMAS NMR study of synthetic and natural layer silicates. Chemistry of Materials, 15, 2605-2613.
38. Levitt M.H. (2001) Spin Dynamics, Basics of Nuclear Magnetic Resonance. John Wiley & Sons, Ltd, Chichester, UK.
39. Lim K.H. & Grey C.P. (1998) Analysis of the anisotropic dimension in the RIACT (II) MQMAS NMR experiment for 1-3/2 nuclei. Solid State Nuclear Magnetic Resonance, 13, 101-112.
40. 23Na spin systems in solids. Chemical PhYsics Letters, 312, 45-56.
41. Llor A. & Virlet J. (1988) Towards high-resolution technique NMR of more nuclei in solids: sample spinning with time-dependent spinner axis angle. Chemical Physics Letters, 152, 248-253.
42. Madhu P.K & Levitt M.H. (2002) Signal enhancement in the triple-quantum Magic-Angle-Spinning NMR of spin-3/2 in solids: The FAM-RIACT-FAM sequence. Journal of Magnetic Resonance, 155, 150-155.
43. Madhu P.K., Goldbourt A., Frydman L. & Vega S. (1999) Sensitivity enhancement of the MQMAS NMR experiment by fast amplitude modulation of the pulses. Chemical Physics Letters, 307, 41-47.
44. Madhu P.K., Goldbourt A., Frydmam L. & Vega S. (2000) Fast radio-frequency amplitude modulation in multiple-quantum magic-angle-spinning nuclear magnetic resonance: Theory and experiments. Journal of Chemical Physics, 112, 2377-2391.
45. Man P.P., Klinowski J., Trokiner A., Zanni H. & Papon P. (1988) Selective and non-selective NMR excitation of quadrupolar nuclei in the solid state. Chemical Physics Letters, 151, 143-150.
46. Marinelli L., Medek A. & Frydman L. (1998) Composite pulse excitation schemes for MQMAS NMR of half-integer quadrupolar spins. Journal of Magnetic Resonance, 132, 88-95.
47. Massiot D. (1996) Sensitivity and lineshape improvements of MQ-MAS by rotor synchronized data acquisition. Journal of Magnetic Resonance A, 122, 240-244.
48. Massiot D., Touzo B., Trumeau D., Coutures J.P., Virlet J., Florian P. & Grandinetti P.J. (1996) Two-dimensional magic-angle-spinning isotropic reconstruction sequences for quadrupolar nuclei. Solid State Nuclear Magnetic Resonance, 6, 73-83.
49. Massiot D., Montouillout V., Fayon F., Florian P. & Bessada C. (1997) Order-resolved sideband separation in magic-angle-spinning NMR of half-integer quadrupolar nuclei. Chemical Physics Letters, 272, 295-300.
50. VI compounds by MAS and QPASS, extension of gallium aluminium NMR parameters correlation. Chemical Physics Letters, 272, 295-300.
51. Massiot D., Fayon F., Capron M., King I., Le Calvé S., Alonso B., Durand J.O., Bujoli B., Gan Z. & Hoatson G. (2002) Modelling one and two-dimensional solid-state NMR spectra. Magnetic Resonance in Chemistry, 40, 70-76.
52. Morais C.M., Lopes M., Fernandez C. & Rocha J. (2003) Assessing the potential of fast amplitude modulation pulses for improving triple-quantum magic angle spinning NMR spectra of half-integer quadrupolar nuclei. Magnetic Resonance in Chemistry (in press).
53. Pruski M., Lang D.P., Fernandez C. & Amoureux J.P. (1997) Multiple-quantum magic-angle-spinning NMR with cross-polarization: Spectral editing of high-resolution spectra of quadrupolar nuclei. Solid State Nuclear Magnetic Resonance, 7, 327-331.
54. Pruski M., Baily A., Lang D.P., Fernandez C. & Amoureux J.P. (1999) Studies of heteronuclear dipolar interactions between spin-1/2 and quadrupolar nuclei by using REDOR during multiple-quantum evolution. Chemical Physics Letters, 307, 35-40.
55. 27Al MAS NMR study of the thermal transformation of kaolinite. Journal of Physical Chemistry B, 103, 9801-9804.
56. 27Al MAS NMR study. Journal of Materials Chemistry, 9, 2499-2503.
57. Rovnyak D., Baldus M. & Griffin R.G. (2000) Multiple-quantum cross polarization in quadrupolar spin systems during Magic-Angle Spinning. Journal of Magnetic Resonance, 142, 145-152.
58. Samoson A. & Lippmaa E. (1983) Central transition NMR excitation spectra of half-integer quadrupole nuclei. Chemical Physics Letters, 100, 205-208.
59. Samoson A., Lipmaa E. & Pines A. (1988) High resolution solid state NMR averaging of second-order effects by means of a double-rotor. Molecular Physics, 65, 1013-1018.
60. Schäfer H., Iuga D., Verhagen R. & Kentgens A.P.M. (2000) Population and coherence transfer in half-integer quadrupolar spin systems induced by simultaneous rapid passages of the satellite transitions: A static and spinning single crystal NMR study. Journal of Chemical Physics, 114, 3073-3091.
61. Smith S.A., Levante T.O., Meier B.H. & Ernst R.R. (1994) Computer simulations in magnetic resonance. An object-oriented programming approach. Journal of Magnetic Resonance A, 106, 75-105.
62. Stebbins J.F., Du L.S., Kroecker S., Neuhoff P., Rice D., Frye J. & Jakobsen H.J. (2002) New opportunities for high-resolution solid-state NMR spectroscopy of oxide materials at 21.1- and 18.8-T fields. Solid State Nuclear Magnetic Resonance, 21, 105-115.
63. Tuel A., Gramlich V. & Baerlocher Ch. (2001) Synthesis, crystal structure and characterization of AP2DAO, a new layered aluminophosphate templated by 1,8-diaminooctane molecules. Microporous and Mesoporous Materials, 47, 217-229.
64. Tuel A., Gramlich V. & Baerlocher Ch. (2001) Synthesis, structure determination and characterization of a new layered aluminophosphate templated by piperazinium ions. Microporous and Mesoporous Materials, 46, 57-66.
65. Tuel A., Gramlich V. & Baerlocher Ch. (2002) Synthesis, characterization and structure determination of two novel layered aluminophosphates templated by 2-methylpiperazine. Microporous and Mesoporous Materials, 56, 119-130.
66. Van Eck E.R.H., Janssen R., Maas W.E.J.R. & Veeman W.S. (1990) A novel application of nuclear spin-echo double-resonance to aluminophosphates and aluminosilicates. Chemical Physics Letters, 174, 428-432.
67. Vega A.J. (1992) MAS NMR spin locking of half-integer quadrupolar nuclei. Journal of Magnetic Resonance, 96, 50-68.
68. Vega S. & Naor Y. (1981) Triple-quantum NMR on spin systems with I=3/2 in solids. Journal of Chemical Physics, 75, 75-86.
69. Vosegaard T., Larsen F.H., Jakobsen H.J., Ellis P.D. & Nielsen C.N. (1997) Sensitivity-enhanced multiple-quantum MAS NMR of half-integer quadrupolar nuclei. Journal of the American Chemical Society, 122, 9055-9056.
70. Vosegaard T., Massiot D. & Grandinetti P.J. (2000) Sensitivity enhancements in MQ-MAS NMR of spin-5/2 nuclei using modulated rf mixing pulses. Chemical Physics Letters, 326, 454-460.
71. Vosegaard T., Florian P., Massiol D. & Grandinetti P.J. (2001) Multiple quantum magic-angle spinning using rotary resonance excitation. Journal of Chemical Physics, 114, 4618-4624.
72. 2 on Pt, Physical Review Letters, 53, 82-85
73. Wang S.H., De Paul S.M. & Bull L.M. (1997) High-resolution heteronuclear correlation between quadrupolar and spin 1/2 nuclei using multiple-quantum magic-angle spinning. Journal of Magnetic Resonance, 125, 364-368.
74. Wu G., Rovnyak D. & Griffin R.G. (1996) Quantitative MQMAS NMR spectroscopy of quadrupolar nuclei in solids. Journal of the American Chemical Society, 118, 9326-9332.
75. Yao Z., Kwak H.T., Sakellariou D., Emsley L. & Grandinetti P.J. (2000) Sensitivity enhancement of the central transition NMR signal of quadrupolar nuclei under magic angle spinning. Chemical Physics Letters, 327, 85-90.