Quantitative determination of loadings and oxidation products of polystyrene-bound phosphines using 31P MAS NMR

Journal of Combinatorial Chemistry

Volumn 5, Issue 5, 2003, Pages 610-616

  Rentsch, Daniel ^a   Hany, Roland ^a   Barthélémy, Sophie ^b   Steinauer, René ^b  

^a SWISS FEDERAL LABORATORIES FOR MATERIALS SCIENCE AND TECHNOLOGY   (Switzerland)

^b Merck Biosciences AG   (Switzerland)

Author keywords

[No Author keywords available]

Indexed keywords

PHOSPHINE DERIVATIVE; POLYSTYRENE;

ADDITION REACTION; ANALYTIC METHOD; ARTICLE; BIOLOGICAL MONITORING; CARBON NUCLEAR MAGNETIC RESONANCE; EVALUATION; HORNER REACTION; MITSUNOBU REACTION; OXIDATION; PHOSPHORUS NUCLEAR MAGNETIC RESONANCE; QUANTITATIVE ASSAY; TEMPERATURE DEPENDENCE;

MAGNETIC RESONANCE SPECTROSCOPY; OXIDATION-REDUCTION; PHOSPHINES; PHOSPHORUS ISOTOPES; POLYSTYRENES;

EID: 0141683725     PISSN: 15204766     EISSN: None     Source Type: Journal    
DOI: 10.1021/cc030004a     Document Type: Article

References (34)

1. Hodge, P.; Richardson, G. J. Chem. Soc., Chem. Commun. 1975, 622-623.
2. Hughes, I. Tetrahedron Lett. 1996, 37, 7595-7598.
3. Bernard, M.; Ford, W. T.; Nelson, E. C. J. Org. Chem. 1983, 48, 3164-3168.
4. Bernard, M.; Ford, W. T. J. Org. Chem. 1983, 48, 326-332.
5. Gentles, R. G.; Wodka, D.; Park, D. C.; Vasudevan, A. J. Comb. Chem. 2002, 4, 442-456.
6. White, J. M.; Tunoori, A. R.; Dutta, D.; Georg, G. I. Comb. Chem. High Throughput Screening 2000, 3, 103-106.
7. Tunoori, A. R.; Dutta, D.; Georg, G. I. Tetrahedron Lett. 1998, 39, 8751-8754.
8. Jacobson, S.; Clements, W.; Hiramoto, H.; Pittman, C. U. J. Mol. Catalysis 1975, 1, 73-76.
9. Pittman, C. U.; Jacobson, S. E.; Hiramoto, H. J. Am. Chem. Soc. 1975, 97, 4774-4775.
10. Pittman, C. U.; Smith, L. R. J. Am. Chem. Soc. 1975, 97, 341-344.
11. Grubbs, R. H.; Kroll, L. C. J. Am. Chem. Soc. 1971, 93, 3062-3063.
12. Pittman, C. U.; Hanes, R. M. J. Am. Chem. Soc. 1976, 98, 5402-5405.
13. Pittman, C. U.; Honnick, W. D.; Yang, J. J. J. Org. Chem. 1980, 45, 684-689.
14. Pittman, C. U.; Wilemon, G. M. J. Org. Chem. 1981, 46, 1901-1905.
15. Fenger, I.; Le Drian, C. Tetrahedron Lett. 1998, 39, 4287-4290.
16. Jang, S. B. Tetrahedron Lett. 1997, 38, 4421-4424.
17. Park, H. J.; Han, J. W.; Seo, H. M.; Jang, H. Y.; Chung, Y. K.; Suh, J. H. J. Mol. Catal. A-Chem. 2001, 174, 151-157.
18. Pittman, C. U.; Wuu, S. K.; Jacobson, S. E. J. Catal. 1976, 44, 87-100.
19. Ben-Aroya, B. B.-N.; Portnoy, M. Tetrahedron 2002, 58, 5147-5158.
20. Parrish, C. A.; Buchwald, S. L. J. Org. Chem. 2001, 66, 3820-3827.
21. Irving, M.; Cournoyer, J.; Li, R. S.; Santos, C.; Yan, B. Comb. Chem. High Throughput Screening 2001, 4, 353-362.
22. Svensson, A.; Bergquist, K.-E.; Fex, T.; Kihlberg, J. Tetrahedron Lett. 1998, 39, 7193-7196.
23. Svensson, A.; Fex, T.; Khilberg, J. J. Comb. Chem. 2000, 2, 736-748.
24. Drew, M.; Orton, E.; Krolikowski, P.; Salvino, J. M.; Kumar, N. V. J. Comb. Chem. 2000, 2, 8-9.
25. Stones, D.; Miller, D. J.; Beaton, M. W.; Rutherford, T. J.; Gani, D. Tetrahedron Lett. 1998, 39, 4875-4878.
26. Hany, R.; Rentsch, D.; Dhanapal, B.; Obrecht, D. J. Comb. Chem. 2001, 3, 85-89.
27. Berger, S.; Braun, S.; Kalinowski, H.-O. NMR Spectroscopy of the Non-Metallic Elements; John Wiley & Sons: Chichester, 1996.
28. Kupka, T.; Wawer, A.; Dziegielewski, J. O.; Zacharias, P. S. Fresenius' J. Anal. Chem. 1991, 339, 253-257.
29. Davis, A. L.; Keeler, J.; Laue, E. D.; Moskau, D. J. Magn. Reson. 1992, 98, 207-216.
30. Wilker, W.; Leibfritz, D.; Kerssebaum, R.; Bermel, W. Magn. Reson. Chem. 1993, 31, 287-292.
31. Massiot, D.; Fayon, F.; Capron, M.; King, I.; Le Calve, S.; Alonso, B.; Durand, J. O.; Bujoli, B.; Gan, Z. H.; Hoatson, G. Magn. Reson. Chem. 2002, 40, 70-76.
32. Fung, B. M.; Khitrin, A. K.; Ermolaev, K. J. Magn. Reson. 2000, 142, 97-101.
33. Vold, R. L.; Waugh, J. S.; Klein, M. P.; Phelps, D. E. J. Chem. Phys. 1968, 48, 3831-3832.
34. Shaka, A. J.; Keeler, J.; Frenkiel, T.; Freeman, R. J. Magn. Reson. 1983, 52, 335-338.