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Volumn 5, Issue 6, 2003, Pages 857-859

Total synthesis of (±)-trachyspic acid and determination of the relative configuration

Author keywords

[No Author keywords available]

Indexed keywords

ALDEHYDE; CHROMIUM; CITRIC ACID; HEPARANASE; NATURAL PRODUCT; NICKEL; TRACHYSPIC ACID; TRIFLUOROMETHANESULFONIC ACID; UNCLASSIFIED DRUG;

EID: 0141627490     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol0275264     Document Type: Article
Times cited : (39)

References (15)
  • 7
    • 0000458709 scopus 로고
    • Trost, B. M., Ed.; Pergamon: Oxford, UK, Chapter 1.6.4
    • For a review see: Saccomano, N. A. In Comprehensive Organic Synthesis; Trost, B. M., Ed.; Pergamon: Oxford, UK, 1991; Vol. 1, Chapter 1.6.4, pp 193-201.
    • (1991) Comprehensive Organic Synthesis , pp. 193-201
    • Saccomano, N.A.1
  • 8
    • 0141709350 scopus 로고    scopus 로고
    • note
    • After aldol reaction with acetone, dehydration gave β,γ -unsaturated ester almost exclusively.
  • 9
    • 0141709349 scopus 로고    scopus 로고
    • note
    • The triflation reaction proceeded with perfect regioselectivity.
  • 12
    • 0030754285 scopus 로고    scopus 로고
    • In this particular case, use of 4-tert-butylpyridine as an additive turned out to decrease the yield of the coupling product (<60%). For the procedure with 4-tert-butylpyridine see: Sheng, D. P. X. C.; Chen, S. S.; Kishi, Y. Tetrahedron Lett. 1997, 38, 6355-6358.
    • (1997) Tetrahedron Lett. , vol.38 , pp. 6355-6358
    • Sheng, D.P.X.C.1    Chen, S.S.2    Kishi, Y.3
  • 13
    • 0141820644 scopus 로고    scopus 로고
    • note
    • When DMSO was used as a solvent, the coupling reaction became very sluggish.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.