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The colored impurity can be reduced by passage through an alumina column.
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56
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0141692463
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note
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13C NMR spectroscopy.
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57
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0141580906
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note
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Reactions were also performed in the absence of PEP to prove the new chemical shifts were not due to byproducts formed in the reaction.
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58
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0141804046
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note
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1H NMR spectra. The standard deviation was calculated from these values and used as an estimate of the error for each sample.
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59
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3 and a longer relaxation delay time of 20 s; however, the carbonyl carbons could still not be distinguished.
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