Transverse magnetization transfer under planar mixing conditions in spin systems consisting of three coupled spins 1/2

Journal of Magnetic Resonance

Volumn 164, Issue 2, 2003, Pages 304-309

  Luy, Burkhard ^a   Glaser, Steffen J ^a  

^a TECHNICAL UNIVERSITY OF MUNICH   (Germany)

Author keywords

Analytical transfer functions; Hartmann Hahn transfer; Planar mixing; Residual dipolar couplings

Indexed keywords

ALGEBRA; IRRADIATION; MAGNETIZATION; POLARIZATION; TRANSFER FUNCTIONS;

PLANAR MIXING;

ELECTRON ENERGY LEVELS;

1,2 DIBROMOPROPANOIC ACID; 1,2-DIBROMOPROPANOIC ACID; PROPIONIC ACID DERIVATIVE;

ALGORITHM; ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; COMPARATIVE STUDY; COMPUTER SIMULATION; EVALUATION; MAGNETISM; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; QUALITY CONTROL; SPIN LABELING; SPIN TRAPPING; VALIDATION STUDY;

ALGORITHMS; COMPUTER SIMULATION; MAGNETIC RESONANCE SPECTROSCOPY; MAGNETICS; MODELS, MOLECULAR; PROPIONIC ACIDS; QUALITY CONTROL; SPIN LABELS; SPIN TRAPPING;

EID: 0141615835     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1016/S1090-7807(03)00251-9     Document Type: Article

References (22)

1. Glaser S.J., Quant J.J. Homonuclear and heteronuclear Hartmann-Hahn transfer in isotropic liquids. Warren W.S. Advances in Magnetic and Optical Resonance. vol. 19:1996;59-252 Academic Press, San Diego.
2. Schulte-Herbrüggen T., Mádi Z.L., Sørensen O.W., Ernst R.R. Reduction of multiplet complexity in COSY-type NMR spectra. The bilinear and planar COSY experiment. Mol. Phys. 72:1991;847-871.
3. Schedletzky O., Luy B., Glaser S.J. Analytical polarization and coherence transfer functions for three coupled spins 1/2 under planar mixing conditions. J. Magn. Reson. 130:1998;27-32.
4. Hartmann S.R., Hahn E.L. Nuclear double resonance in the rotating frame. Phys. Rev. 128:1962;2042-2053.
5. N systems J. Chem. Phys. 74:1981;127-156.
6. Müller L., Ernst R.R. Coherence transfer in the rotating frame. Application to heteronuclear cross-correlation spectroscopy. Mol. Phys. 38:1979;963-992.
7. Bearden D.W., Brown L.R. Heteronuclear isotropic mixing in liquids. Chem. Phys. Lett. 163:1989;432-436.
8. Ernst M., Griesinger C., Ernst R.R., Bermel W. Optimized heteronuclear cross polarization in liquids. Mol. Phys. 74:1991;219-252.
9. Schwendinger M.G., Quant J., Glaser S.J., Griesinger C. Broadband heteronuclear Hartmann-Hahn sequences. J. Magn. Reson. B. 111:1994;115-120.
10. Carlomagno T., Luy B., Glaser S.J. "Kin" HEHAHA sequences, heteronuclear Hartmann-Hahn transfer with different bandwidths for spins I and S. J. Magn. Reson. 126:1997;110-119.
11. Mádi Z.L., Brutscher B., Schulte-Herbrüggen T., Brüschweiler R., Ernst R.R. Time-resolved observation of spin waves in a linear chain of nuclear spins. Chem. Phys. Lett. 268:1997;300-305.
12. Konrat R., Burghardt I., Bodenhausen G. Coherence transfer in nuclear magnetic resonance by selective homonuclear Hartmann-Hahn correlation spectroscopy. J. Am. Chem. Soc. 113:1991;9135-9140.
13. Kupče Ē., Freeman R. Multiple Hartmann-Hahn coherence transfer in nuclear magnetic resonance spectroscopy. J. Am. Chem. Soc. 114:1992;10671-10672.
14. aromatic correlations J. Biomol. NMR. 8:1996;161-170.
15. Zuiderweg E.R.P., Zeng L., Brutscher B., Morshauer R.C. Band-selective hetero- and homonuclear cross-polarization using trains of shaped pulses. J. Biomol. NMR. 8:1996;147-160.
16. 15N. J. Biomol. NMR. 5:1995;323-326.
17. Glaser S.J. Coupling topology dependence of polarization-transfer efficiency in TOCSY and TACSY experiments. J. Magn. Reson. A. 104:1993;283-301.
18. Luy B., Glaser S.J. Superposition of scalar and residual dipolar couplings: analytical transfer functions for three spins 1/2 under cylindrical mixing conditions. J. Magn. Reson. 148:2001;169-181.
19. Majumdar A., Zuiderweg E.P. Efficiencies of double- and triple-resonance. J cross polarization in multidimensional NMR J. Magn. Reson. A. 113:1995;19-31.
20. Banwell C.N., Primas H. On the analysis of high-resolution nuclear magnetic resonance spectra. I. Methods of calculating NMR spectra. Mol. Phys. 6:1963;225-256.
21. Chung C.-W., Keeler J., Wimperis S. Spin topology from "Taylored" TOCSY. J. Magn. Reson. A. 114:1995;188-200.
22. Freeman, McLauchlan K.A., Musher J.I., Pachler K.G.R. The relative signs of geminal and vicinal proton spin coupling constants. Mol. Phys. 5:1962;321-327.