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Volumn 4, Issue 16, 2002, Pages 2719-2722

Cyclopropanation with Fischer acyloxycarbene complexes: Preparation of cyclopropane and cycloheptane-fused γ-lactones

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ARTICLE;

EID: 0043192549     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol026225r     Document Type: Article
Times cited : (30)

References (35)
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    • (1991) Comprehensive Organic Synthesis , vol.5 , pp. 1065-1113
    • Wulff, W.D.1
  • 3
    • 0000887836 scopus 로고
    • Abel, E. W., Stone, F. G. A., Wilkinson, G., Eds; Pergamon: Oxford
    • (b) Wulff, W. D. In Comprehensive Organometallic Chemistry II; Abel, E. W., Stone, F. G. A., Wilkinson, G., Eds; Pergamon: Oxford, 1995; Vol. 12, pp 470-547.
    • (1995) Comprehensive Organometallic Chemistry II , vol.12 , pp. 470-547
    • Wulff, W.D.1
  • 16
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    • Murray, C. K.; Yang, D. C.; Wulff, W. D. J. Am. Chem. Soc. 1990, 112, 5660-5662. The methodology developed by these authors has been recently applied by Takeda et al.: Takeda, K.; Sakumura, K.; Yoshii, E. Tetrahedron Lett. 1977, 38, 3257-3260.
    • (1990) J. Am. Chem. Soc. , vol.112 , pp. 5660-5662
    • Murray, C.K.1    Yang, D.C.2    Wulff, W.D.3
  • 17
    • 0030938841 scopus 로고
    • Murray, C. K.; Yang, D. C.; Wulff, W. D. J. Am. Chem. Soc. 1990, 112, 5660-5662. The methodology developed by these authors has been recently applied by Takeda et al.: Takeda, K.; Sakumura, K.; Yoshii, E. Tetrahedron Lett. 1977, 38, 3257-3260.
    • (1977) Tetrahedron Lett. , vol.38 , pp. 3257-3260
    • Takeda, K.1    Sakumura, K.2    Yoshii, E.3
  • 19
    • 0000695788 scopus 로고
    • Tetraalkylammonium chromates are readily available from the corresponding lithium chromates and tetraalkylammonium bromide. For several examples, see: (a) Semmelhack, M. F.; Bozell, J. J. Tetrahedron Lett. 1982, 23, 2931-2934.
    • (1982) Tetrahedron Lett. , vol.23 , pp. 2931-2934
    • Semmelhack, M.F.1    Bozell, J.J.2
  • 23
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    • (d) Soderberg, B. C.; Hegedus, L. S.; Sierra, M. A. J. Am. Chem. Soc. 1990, 112, 4364. Vernier, J. M.; Hegedus, L. S.; Miller, D. B. J. Org. Chem. 1992, 57, 6914-6920.
    • (1992) J. Org. Chem. , vol.57 , pp. 6914-6920
    • Vernier, J.M.1    Hegedus, L.S.2    Miller, D.B.3
  • 26
    • 0043006708 scopus 로고    scopus 로고
    • note
    • 2), 19.4 (CH). HRMS (IE): calcd, 174.0681; found, 174.0682
  • 28
    • 0043006709 scopus 로고    scopus 로고
    • PM3 implemented in MOPAC V6
    • PM3 implemented in MOPAC V6.
  • 29
    • 0042005002 scopus 로고    scopus 로고
    • note
    • 3J (H,H) calcd = 5.9 Hz, observed for the minor isomer = 6.9 Hz.


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