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19
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0042405750
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note
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-1): 3341 (m), 3245 (w), 1631 (m), 1620 (m), 1607 (s), 1588 (m), 1534 (s), 1516 (s), 1497 (s), 1431 (s), 1401 (vs), 1316 (w), 1258 (vw), 1174 (m), 1087 (vw), 849 (vw), 785 (m), 700 (w), 625 (m), 548 (w).
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20
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0042405751
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note
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int = 0.0226, 2.43 ≤ θ ≤ 25.05), R1 = 0.0331, wR2 = 0.0878, GOF = 1.032 for 357 parameters. The intensity data were measured on a Siemens Smart CCD diffractometer with graphite-monochromated Mo Kα radiation (λ = 0.71073 Å) at 298 K. Empirical absorption corrections were applied by using the SADABS program. All calculations were performed using the SHELXL-97 program package. The structure was solved by direct methods and refined by full-matrix least-squares methods. All nonhydrogen atoms were refined anisotropically, while all hydrogen atoms were located from differential Fourier maps.
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21
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