Orthometalation in calixarenes: Synthesis and structural characterization of a novel orthopalladated calix[4]arene bisphosphite

Current Science

Volumn 83, Issue 7, 2002, Pages 870-873

  Mahalakshmi, L ^a   Krishnamurthy, S S ^a   Nethaji, M ^a  

^a INDIAN INSTITUTE OF SCIENCE   (India)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0042808680     PISSN: 00113891     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (43)

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28. 3].
29. An Enraf Nonius MACH3 diffractometer was used for data collection. Crystallographic data (excluding the structure factors) have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC 133305. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ, UK (fax: (+44) 1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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32. The dihedral angles of the aromatic rings (C1-C6, C8-C13, C15-C20, and C22-C27) with the mean plane defined by the methylene carbons for (2) are 71.1, 37.1, 65.7 and 45.9° respectively and the corresponding dihedral angles for (1) are 65.4, 51.4, 65.4 and 51.4°, respectively.
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