Upper rim substituted thiacalix[4]arenes

Tetrahedron Letters

Volumn 44, Issue 38, 2003, Pages 7167-7170

  Kasyan, Oleg ^a   Swierczynski, Dariusz ^b   Drapailo, Andrew ^a   Suwinska, Kinga ^b   Lipkowski, Janusz ^b   Kalchenko, Vitaly ^a  

^a INSTITUTE OF ORGANIC CHEMISTRY   (Ukraine)

^b INSTITUTE OF PHYSICAL CHEMISTRY   (Poland)

Author keywords

Arbuzov reaction; Organophosphorus compounds; Thiacalixarenes; X ray analysis

Indexed keywords

BROMIDE; MACROCYCLIC COMPOUND; METHYL GROUP; PHOSPHORIC ACID DERIVATIVE; POLYCYCLIC AROMATIC HYDROCARBON DERIVATIVE;

ARTICLE; CHEMICAL STRUCTURE; CONFORMATIONAL TRANSITION; HYDROGEN BOND; STRUCTURE ANALYSIS; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

ARENE;

EID: 0042510227     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(03)01809-4     Document Type: Article

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16. 4, %: C, 58.10; H, 3.20; S, 25.80. Found, %: C, 58.00; H, 3.40; S, 25.50.
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19. 4, %: C, 35.49; H, 1.49; Br, 39.35; S, 15.79. Found, %: C, 35.26; H, 1.41; Br, 39.26; S, 15.79.
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24. 4, %: C, 48.70; H, 2.92; Cl, 20.54; S, 18.57. Found, %: C, 48.63; H, 3.00; Cl, 20.13; S, 18.63.
25. 4, %: C, 59.99; H, 5.35; P, 9.67; S, 10.01. Found, %: C, 59.30; H, 4.98; P, 9.56; S, 9.93.
26. 2) all data -0.0774, 0.1152. The crystallographic data for the crystal structure has been deposited at the Cambridge Crystallographic Data Centre and allocated the deposition number CCDC 203909.