Electrochemically induced fluorinative ring expansion of cycloalkylideneacetates

Tetrahedron Letters

Volumn 37, Issue 47, 1996, Pages 8511-8514

  Hara, Shoji ^b   Chen, Sheng Qi ^a   Hoshio, Takuro ^a   Fukuhara, Tsuyoshi ^a   Yoneda, Norihiko ^b  

^a HOKKAIDO UNIVERSITY   (Japan)

^b NONE

Author keywords

[No Author keywords available]

Indexed keywords

CYCLOALKANE DERIVATIVE;

ARTICLE; DRUG SYNTHESIS; ELECTROCHEMISTRY; FLUORINATION; REACTION ANALYSIS;

EID: 0042443017     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(96)01953-3     Document Type: Article

References (8)

1. 1. Yoneda, N.; Chen, S.-Q.; Hatakeyama, T.; Hara, S.; Fukuhara, T. Chem. Lett., 1994, 849-850.
2. 2. Hara, S.; Chen, S.-Q.; Hatakeyama, T.; Fukuhara, T.; Sekiguchi, M.; Yoneda, N. Tetrahedron Lett., 1995, 36, 6511-6514.
3. 3. Chen, S.-Q.; Hatakeyama, T.; Fukuhara, T.; Hara, S.; Yoneda, N. Electrochimica Acta, 1996, in press.
4. 4. Meurs, J. H. H.; Eilenberg, W. Tetrahedron, 1991, 47, 705-714.
5. 3N-3HF and a significant decrease in the yield of 2 under the reaction conditions.
6. 6 From the substrate of the 8-membered ring, a complex mixture of the products was obtained.
7. 7. Wovkulich, P. M. Comprehensive Organic Synthesis Volume 1; Schreiber, S. Ed.; Pergamon Press: Oxford, 1991; pp. 843-899.
8. 3COOEt as co-solvent is effective.