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3. See Supporting Information or ref 5
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27
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85034126142
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note
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2 (0.03 mmol) in dry THF (4 mL). The resulting mixture was refluxed under an argon atmosphere until consumption of the starting material (0.5-7 h); then the reaction was quenched by addition of a few drops of MeOH. Usual workup and flash chromatography affords the cross-coupling product.
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28
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85034149182
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2 gave lower yields
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2 gave lower yields.
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33
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33751386638
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