Preparation of methyl 2-[Bis(trimethylsiloxy)phosphoryl]-3,3,3-trifluoro-2-(trimethylsiloxy)propionate and some derivatives -molecular structure of methyl 2-[bis(trimethylsiloxy)phosphoryl]-3,3,3-trifluoro-2-hydroxypropionate

Chemische Berichte

Volumn 130, Issue 2, 1997, Pages 279-281

  Schoth, Ralph Matthias ^a   Lork, Enno ^a   Seifert, Frank Uwe ^a   Breuer, Eli ^b   Röschenthaler, Gerd Volker ^b  

^a UNIVERSITY OF BREMEN   (Germany)

^b HEBREW UNIVERSITY OF JERUSALEM   (Israel)

Author keywords

Methyl trifluoropyruvate; Tris(trimethylsilyl) phosphite

Indexed keywords

EID: 0042407477     PISSN: 00092940     EISSN: None     Source Type: Journal    
DOI: 10.1002/cber.19971300222     Document Type: Article

References (13)

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4. C. von dem Bussche-Hünnefeld, C. Cescato, D. Seebach, Chem. Ber. 1992, 725, 2795-2802.
5. F. U. Seifert, G.-V. Röschenthaler, Z. Natiirforscli. 1993, 48b, 1089-1093.
6. R.-M. Schoth, H. Cohen, E. Lork, F. U. Seifert, G. Golomb, E. Breuer, G.-V. Röschenthaler, Naturwissenschaften, in press.
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8. L. Wozniak, J. Chojnowski, Tetrahedron, 1989, 45, 2465-2524.
9. A similar value was observed in ref.[6].
10. R. Dittrich, G. Hagele, Phosphorus Sulfur, 1981, 10, 127-132.
11. H.-O. Kalinowski, S. Berger, S. Braun, "C-NMR Spektroskopie, Thieme, Stuttgart, 1984, pp. 115, 520, 530.
12. Further details of the crystal structure investigation are available from the Fachinformationsdienst Karlsruhe, D-76344 Eg-
13. genstein-LeopoIdshafen (Germany), on quoting the depository number CSD-405962 and the journal citation.