Synthesis, structural and spectral studies of N-p-methylbenzyliden-N-phenyl-p,p′-dimethoxybenzoyl acetic acid hydrazide

Zeitschrift fur Kristallographie

Volumn 218, Issue 5, 2003, Pages 377-380

  Ulku D ^a   Arici, C ^a   Ercan, F ^a   Sacmaci M ^b   Saripinar, E ^b   Akcamur Y ^b  

^a HACETTEPE UNIVERSITY   (Turkey)

^b ERCIYES UNIVERSITY   (Turkey)

Author keywords

[No Author keywords available]

Indexed keywords

HYDRAZIDE; N 4 METHYLBENZYLIDENE N PHENYL 4,4' DIMETHOXYBENZOYLACETIC ACID HYDRAZIDE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL STRUCTURE; CRYSTAL STRUCTURE; CRYSTALLIZATION; HYDROGEN BOND; INFRARED SPECTROSCOPY; MOLECULAR INTERACTION; SPECTROSCOPY; STRUCTURE ANALYSIS; SYNTHESIS; X RAY DIFFRACTION;

EID: 0042305040     PISSN: 00442968     EISSN: None     Source Type: Journal    
DOI: 10.1524/zkri.218.5.377.20737     Document Type: Article

References (19)

1. Akçamur, Y.; Penn, G.; Ziegler, E.; Sterk, H.; Kollenz, G.; Peters, K.; Peters, E.-M.; Schnering, H. G.: Reaktionen mit cyclischen Oxalyverbindungen, XXIVI. Zur Reaktion von 4-Benzoyl-5-phenyl-furan-2,3-dion mit Phenylhydrazonen bzw. Phenylhydrazin. Monatsch. Chem. 117 (1986) 231-245.
2. Wentrup, C.; Heilmeyer, W.; Kollenz, G.: α-Oxoketenes-Preparation and Chemistry. Synthesis (1994) 1219.
3. Nakatani, K.; Shirai, J.; Sando, S.; Saito, I.: Guanine Specific DNA Cleavage by Photoirradiation of Dibenzoyldiazo-methane Oligonucleotide Conjugates. J. Am. Chem. Soc. 119 (1997) 7626.
4. Hyatt, J. A.; Felman, P. L.; Clemens, R. J.: Thermal Decomposition of 2,2,6-Trimethyl-4H-1,3-dioxin-4-one and 1-Ethoxybutyn-3-one. Acetylketene. J. Org. Chem. 49 (1984) 5105.
5. Clemens, R. J.; Hyatt, J.: Acetoacetylation with 2,2,6-trimethyl-4H-1,3-dioxin-4-one: a convenient alternative to diketene. J. Org. Chem. 50 (1985) 2431.
6. Bibas, H.; Kappe, C. O.; Wong, M. W.; Wentrup, C.: Carboxy(vinyl) ketene Intermediates in the Thermolysis of Methylthio- and Methoxy-Substitued Meldrum's Acid Derivatives. J. Chem. Soc. (1998) 493.
7. Stadler, A.; Zangger, K.; Belaj, F.; Kollenz, G.: Neat carbomethoxypivaloylketene-preparation and chemical reactivity. Tetrahedron 57 (2001) 6757.
8. Fabian, W. M. F; Kollenz, G.; Akçamur, Y.; Kök, T. R.; Tezcan, M.; Akkurt, M.; Hiller, W.: Synthese von Dibenzoylacet-N-carb-oxyalkylamiden und semiempirische Rechnungen zur Keto-Enol Tautomerie. Monatsch. Chem. 123 (1992) 265.
9. Kappe, C. O.; Farber, G.; Wentrup, C.; Kolenz, G.: A Novel and Convenient Approach to Functionalized 2,6,9-Trioxabicyclo [3,3,1]nona-3,7-dienes (Bridged Bis-Dioxines). Tetrahedron Lett. 33 (1992) 4553.
10. Yildirim, I.; Ilhan, I. O.: Functionalization and Cyclization Reactions of Various Acetanilides with 4-Benzoyl-5-phenyl-2,3-furandione. Experimental and Theroetical Investigations. J. Heterocyclic Chem. 34 (1997) 1047.
11. Kappe, C. O.; Farber, G.; Wentrup, C.; Kollenz, G.: Dipivalylketene and its Dimers. [2 + 4] versus [2 + 2] Cycloaddition Reactions of Oxoketenes. J. Org. Chem. 57 (1992) 7078.
12. Abd El Nabi, H. A.; Kollenz, G.: Reactions of 4-Ethoxycarbonyl-5-phenyl-2,3-dihydrofuran-2,3-dione with Heterocumulenes and Schiff Bases Monatsch. Chem. 128 (1997) 381.
13. Saripinar, E.; Güzel, Y.; Onal, Z.; Ilhan, I. O. Akcamur, Y.: 4-(-4methoxybenzoyl)-5-(-4-methoxyphenyl)-2,3-dihydro-2,3-furandione, its Synthesis, Thermolysis and Diels-Alder Reactions with Schiff Bases: Experimental Data and Calculations. J. Chem. Soc. Pak. 22(4) (2000) 308.
14. Enraf Nonius: Cad-4 Express Version 1.1. Delft, The Netherlands, 1993.
15. Sheldrick, G. M.: SHELXS-97 and SHELXL-97. [Program for Crystal Structure Solution and Refinement University of Göttingen. Germany 1997.
16. Farrugia, L. J.: WinGX. Program for Crystallography package. J. Apply Cryst. 32 (1999) 837.
17. Spek, A. L.: PLATON. Program for Crystal Molecular Drawing. University of Ultrech, The Netherlands.
18. Beyer, H.: Lehbruch der Organischen Chemie. 18. Auflage (1980) 460.
19. Hökelek, T.; Saripinar, E.; Yildirim, I.; Akkurt, M.; Akçamur, Y.: 4-(4-Methoxybenzoyl)-5-(4-methoxyphenyl)-2,3-dihydro-2,3-furandione. Acta Cryst. E58 (2002) 030-032.