The benefit of the retrofitting of a conventional LC system to micro LC: A practical evaluation in the field of bioanalysis with fluorimetric detection

Biomedical Chromatography

Volumn 17, Issue 5, 2003, Pages 297-305

  Roy, S ^a,b   Rieutord, A ^a,b   Zhou, J Y ^a   Baillet, A ^a   Prognon, P ^a   Chaminade, Pierre ^a  

^a University Paris Saclay   (France)

^b HÔPITAL ROBERT DEBRÉ   (France)

Author keywords

Fluorescence; Fluoroquinolones; Micro HPLC; Signal enhancement

Indexed keywords

CELLS; COLUMN CHROMATOGRAPHY; CYTOLOGY; EFFICIENCY; LIQUID CHROMATOGRAPHY;

BIOANALYSIS; COLUMN EFFICIENCY; DETECTION CELLS; EFFICIENCY INCREASE; FLUORIMETRIC; FLUORIMETRIC DETECTION; FLUOROQUINOLONES; INNER DIAMETERS; MICRO-HPLC; SIGNAL ENHANCEMENT;

FLUORESCENCE;

ANTIBIOTIC AGENT; CIPROFLOXACIN; ENOXACIN; FLEROXACIN; LOMEFLOXACIN; QUINOLINE DERIVED ANTIINFECTIVE AGENT;

ANALYTIC METHOD; ARTICLE; BLOOD ANALYSIS; CELL STRUCTURE; CONTROLLED STUDY; DRUG DETERMINATION; DRUG STRUCTURE; FLOW KINETICS; FLUOROMETRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; IMAGE ENHANCEMENT; LIQUID CHROMATOGRAPHY; SENSITIVITY ANALYSIS; SIGNAL TRANSDUCTION;

EID: 0042063788     PISSN: 02693879     EISSN: None     Source Type: Journal    
DOI: 10.1002/bmc.239     Document Type: Article

References (25)

1. Ahuja S. Trace and Ultratrace Analysis by HPLC. John Wiley: New York, 1991; 59.
2. Aiello M and McLaren R. A sensitive small-volume UV/Vis flow cell and total absorbance detection system for micro-HPLC. Analytical Chemistry 2001; 73: 1387-1392.
3. Becher F, Pruvost A, Goujard C, Guerreiro C, Delfraissy JF, Grassi J and Benech H. Improved method for the simultaneous determination of d4T, 3TC and ddI intracellular phosphorylated anabolites in human peripheral-blood mononuclear cells using high-performance liquid chromatography/tandem mass spectrometry. Rapid Communications in Mass Spectrometry 2002; 16: 555-565.
4. Carlucci G. Analysis of fluoroquinolones in biological fluids by high-performance liquid chromatography. Journal of Chromatography A 1998; 812: 343-367.
5. Chervet JP, van Soest REJ and Salzman JP. Recent advances in capillary liquid chromatography: enhanced detectability in bioanalysis. LC GC International 1992; 5: 33-38.
6. Chervet JP, Ursem M and Salzmann JP. Instrumental requirements for nanoscale liquid chromatography. Analytical Chemistry 1996; 68: 1507-1512.
7. Claessens HA and Kuyken MAJ. A comparative study of large volume injection techniques for microbore columns in HPLC. Chromatographia 1987; 23: 331-336.
8. Gooijer C, Baumann RA and Hofstraat JW. Sensitized fluorescence: a potential method to enhance the concentration sensitivity of fluorescence detection in small-bore LC. Journal of Chromatographic Science 1986; 24: 361-363.
9. Héron S, Tchapla A and Chervet JP. Influence of injection parameters on column performance in nanoscale high-performance liquid chromatography. Chromatographia 2000; 51: 495-499.
10. Janecek M, Kahle V and Krejci M. Ultraviolet fibre optic photometric cell with an effective volume of 30 nl for micro-scale high-performance liquid chromatography. Journal of Chromatography 1998; 438: 409-419.
11. Menet H, Gareil P, Caude M and Rosset R. Microchromatographie en phase liquide. Analusis 1983; 11: 141-155.
12. Mills MJ, Maltas J and Lough WJ. Assessment of injection volume limits when using on-column focusing with microbore liquid chromatography. Journal of Chromatography A 1997; 759: 1-11.
13. Möller JG, Staß H, Heinig R and Blascke G. Capillary electrophoresis with laser-induced fluorescence: a routine method to determine moxifloxacin in human body fluids in very small sample volumes. Journal of Chromatography B 1998; 716: 325-334.
14. Novotny M. Recent advances in microcolumn liquid chromatography. Analytical Chemistry 1988; 60: 500A-510A.
15. Paton JH and Reeves DS. Fluoroquinolone antibiotics: microbiology, pharmacokinetics and clinical use. Drugs 1998; 36: 193-228.
16. Rezai MA, Famiglini G and Cappiello A. Enhanced detection sensitivity by large volume injection in reversed-phase micro-high-performance liquid chromatography. Journal of Chromatography A 1996; 742: 69-78.
17. Takeuchi T and Ishii D. A multichannel photodiode array ultraviolet-visibles detector for micro high-performance liquid chromatography. Journal of Chromatography 1984; 288: 451-456.
18. Tao L and Kennedy T. Laser-induced fluorescence detection in microcolumn separations. TRACS 1998; 17: 484-491.
19. van Soest REJ, Chervet JP, Ursem. M and Suijlen JM. Analysis of fluorescent water tracers using on-line preconcentration in micro HPLC. LC GC International 1996; 9: 586-593.
20. van Straten MA, Vermeer EA and Claessens HA. A first step towards miniaturized HPLC systems in analytical routine laboratories. LC GC International 1996; 9: 42-50.
21. Vigny P and Duquesne M. A spectrofluorometer for measuring very weak fluorescences from biological molecules. Photochemistry and Photobiology 1974; 20: 15-25.
22. Vissers JPC. Recent developments in microcolumn liquid chromatography. Journal of Chromatography A 1999; 856: 117-143.
23. Vurek GG. Nanoliter-volume flow-through fluorometer. Analytical Chemistry 1982; 54: 840-842.
24. Wang P, Zhou M, Feng Y and Chen L. Simultaneus determination of trace ofloxacin and enoxacin by TLC-fluorescence spectrodensitometry. Analytical Letters 1998; 31: 1523-1531.
25. Zhou X, Furushima N, Terashima C, Tanaka H and Turano M. New micro-flow pumping system for liquid chromatography. Journal of Chromatography A 2001; 913: 165-171.