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[12a] Preparation of 5a from p-toluensulfonylhydrazine in the presence of acetic acid has been reported but no spectroscopic data were given, see: P. K. Freeman, D. M. Balls, J. Org. Chem. 1967, 32, 2354-2356.[12b] For an unsuccessful attempt to prepare tosylhydrazone 5a in the presence of acid, see ref.[10]
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[12a] Preparation of 5a from p-toluensulfonylhydrazine in the presence of acetic acid has been reported but no spectroscopic data were given, see: P. K. Freeman, D. M. Balls, J. Org. Chem. 1967, 32, 2354-2356.[12b] For an unsuccessful attempt to prepare tosylhydrazone 5a in the presence of acid, see ref.[10]
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19
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0043109788
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13C NMR spectra of 7 are identical with literature data; see: [13a] D. Farcasiu, J. Slutsky, P. v. R. Schleyer, K. H. Overton, K. Luk, J. B. Stothers, Tetrahedron 1977, 33, 3269-3274. [13b] Z. Majerski, Z. Hameršak, J. Org. Chem. 1984, 49, 1182-1185.
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Overton, K.H.4
Luk, K.5
Stothers, J.B.6
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20
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0043109787
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13C NMR spectra of 7 are identical with literature data; see: [13a] D. Farcasiu, J. Slutsky, P. v. R. Schleyer, K. H. Overton, K. Luk, J. B. Stothers, Tetrahedron 1977, 33, 3269-3274. [13b] Z. Majerski, Z. Hameršak, J. Org. Chem. 1984, 49, 1182-1185.
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[16a] G. W. Kabalka, D. T. C. Yang, J. D. Baker, Jr., J. Org. Chem. 1976, 41, 574-575. [16b] G. W. Kabalka, D. T. C. Yang, J. H. Chandler, J. H. Baker, Jr., Synthesis 1977, 124-126. [16c] L. Caglioti, Tetrahedron 1966, 22, 487-493.
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0043109766
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note
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13C NMR spectra of deuterated and non-deuterated samples.
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30
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0041606978
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note
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13C NMR spectra of 7 was confirmed with the help of two-dimensional COSY and HETCOR spectra.
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31
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