Electroreductive intramolecular coupling of aromatic δ- and ε-keto esters

Tetrahedron Letters

Volumn 44, Issue 33, 2003, Pages 6281-6284

  Kise, Naoki ^a   Arimoto, Kie ^a   Ueda, Nasuo ^a  

^a TOTTORI UNIVERSITY   (Japan)

Author keywords

Electroreduction; Reductive coupling; hydroxy ketones; keto esters; keto esters

Indexed keywords

CHLOROTRIMETHYLSILANE; ESTER DERIVATIVE; KETONE DERIVATIVE; OXOACID; TRIETHYLAMINE;

ARTICLE; CHEMICAL REACTION KINETICS; CYCLIZATION; MOLECULAR INTERACTION; REDUCTION; SILYLATION; THIN LAYER CHROMATOGRAPHY;

EID: 0041846777     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(03)01526-0     Document Type: Article

References (7)

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6. Although the role of triethylamine is not clear at present, it works as a base to neutralize hydrogen chloride generated by the reaction of CTMS with water slightly present.
7. 3) δ 1.73 (q), 17.32 (t), 35.61 (t), 39.29 (t), 82.39 (s), 126.55 (d), 127.77 (d), 128.12 (d), 140.32 (s), 216.08 (s).