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85170507484
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note
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The synthesis of 3-hydroxyphenalenone 5 was carried out by the standard procedure; see, Ref. [6].
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85170492323
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The spin density distribution of the 3-oxophenalenoxyl derivative 2 was determined by ESR measurement and a simple HMO-McLachlan calculation, indicating that the spin density of the 3-oxophenalenoxyl system is dominantly delocalized on the carbon atom at 2-position and two oxygen atoms; see: Ref. [6]. The generation and the characterization of a 5,8-di-tert-butylated 3-oxophenalenoxyl derivative are in progress.
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27
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85170501795
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note
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In a 6-oxophenelenoxyl neutral radical system, the resonance structures keeping a benzene ring in the phenalenyl skeleton show the important contributions in all resonance structures calculated by VB method in terms of MO calculations; see: Ref. [4b].
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