The preparation of methyl 9-iodo-perfluorononanoate: An access to reverse fluorinated amphiphiles

Tetrahedron Letters

Volumn 38, Issue 50, 1997, Pages 8757-8760

  Szlávik, Zoltán ^a   Csámpai, Antal ^a   Krafft, Marie Pierre ^b   Riess, Jean G ^c   Rábai, József ^a  

^a EÖTVÖS LORÁND UNIVERSITY   (Hungary)

^b UNIVERSITÉ CÔTE D'AZUR   (France)

^c UNIVERSITY OF CALIFORNIA   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ORGANOFLUORINE DERIVATIVE;

ARTICLE; DRUG SYNTHESIS; IN VITRO STUDY; METHODOLOGY; REACTION ANALYSIS;

EID: 0041538565     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)10344-6     Document Type: Article

References (19)

1. Greiner, J.; Riess, J. G.; Vierling, P. Organofluorine Compounds in Medicinal Chemistry; Filler, R.; Kobayashi, Y.; Yagupolskii, L. M., Eds.; Elsevier: Amsterdam, 1993; 339-380.; Kissa, E. Fluorinated Surfactants (Surfactant Science Series, Vol. 50.); Marcel Dekker: New York, 1994. Chapter 2.
2. Greiner, J.; Riess, J. G.; Vierling, P. Organofluorine Compounds in Medicinal Chemistry; Filler, R.; Kobayashi, Y.; Yagupolskii, L. M., Eds.; Elsevier: Amsterdam, 1993; 339-380.; Kissa, E. Fluorinated Surfactants (Surfactant Science Series, Vol. 50.); Marcel Dekker: New York, 1994; Chapter 2.
3. Krafft, M. P.; Giulieri, F.; Riess, J. G. Angew. Chem. Int. Ed. Engl. 1993, 32, 741-743.; Giulieri, F.; Krafft, M. P.; Riess, J. G. Angew. Chem. Int. Ed. Engl. 1994, 33, 1514-15.
4. Krafft, M. P.; Giulieri, F.; Riess, J. G. Angew. Chem. Int. Ed. Engl. 1993, 32, 741-743.; Giulieri, F.; Krafft, M. P.; Riess, J. G. Angew. Chem. Int. Ed. Engl. 1994, 33, 1514-15.
5. Riess, J. G. Colloids Surfaces 1994, 84, 33-48.; Riess, J. G.; Krafft, M. P. Art. Cells, Blood Subst., Immob. Biotechn. 1997, 25, 43-52.; Sadtler, V.; Krafft, M. P.; Riess, J. G. Angew. Chem. Int. Ed. Eng. 1996, 35, 1976-78.
6. Riess, J. G. Colloids Surfaces 1994, 84, 33-48.; Riess, J. G.; Krafft, M. P. Art. Cells, Blood Subst., Immob. Biotechn. 1997, 25, 43-52.; Sadtler, V.; Krafft, M. P.; Riess, J. G. Angew. Chem. Int. Ed. Eng. 1996, 35, 1976-78.
7. Riess, J. G. Colloids Surfaces 1994, 84, 33-48.; Riess, J. G.; Krafft, M. P. Art. Cells, Blood Subst., Immob. Biotechn. 1997, 25, 43-52.; Sadtler, V.; Krafft, M. P.; Riess, J. G. Angew. Chem. Int. Ed. Eng. 1996, 35, 1976-78.
8. Brace, N. O. J. Org. Chem. 1962, 27, 3033-38.; ibid. 1966, 31, 2879-85.
9. Brace, N. O. J. Org. Chem. 1962, 27, 3033-38.; ibid. 1966, 31, 2879-85.
10. 8) 106.11-113.12, δ (C=O) 158.99 t; purity was tested with GC (HP 5890 Series II, PONA): 97.6%.
11. 8) 106.11-113.12, δ (C=O) 158.99 t; purity was tested with GC (HP 5890 Series II, PONA): 97.6%.
12. 8-COOEt.
13. +: 586.
14. 3Na have been prepared; see: Hu, C.-M.; Qing, F.-L. J. Org. Chem. 1991, 56, 6348-51.
15. Brace, N. O. J. Fluorine Chem. 1982, 20, 313-327.
16. +: 614.
17. +: 586.
18. 31P δ 15.53 s.
19. This research was supported by the Hungarian Scientific Research Foundation (OTKA no. T 022169).