The early stages in the behaviour of tetrapropylammonium cations in the synthesis of gel precursor to pure siliceous MFI zeolite: An in situ multinuclear NMR study

Microporous and Mesoporous Materials

Volumn 26, Issue 1-3, 1998, Pages 143-151

  Gougeon, R ^a   Delmotte, L ^a   Le Nouen, D ^a   Gabelica, Z ^a  

^a Ecole Nationale Superieure de Chimie de Mulhouse   (France)

Author keywords

Dynamics; In situ nuclear magnetic resonance spectroscopy; Silicalite gel; Tetrapropylammonium cation

Indexed keywords

AMMONIUM COMPOUNDS; GELS; IONS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SYNTHESIS (CHEMICAL);

ALKYLAMMONIUM CATIONS; SILICALITE;

ZEOLITES;

EID: 0041193148     PISSN: 13871811     EISSN: None     Source Type: Journal    
DOI: 10.1016/S1387-1811(98)00226-1     Document Type: Article

References (49)

1. Davis M.E., Lobo R.F. Chem. Mater. 4:1992;756.
2. Flanigen E.M. Adv. Chem. Ser. 121:1973;119.
3. Lok B.M., Cannan T.R., Messina C.A. Zeolites. 3:1983;282.
4. Barrer R.M. Stud. Surf. Sci. Catal. 24:1985;1.
5. van Santen R.A., Keijsper J.J., Ooms G., Kortbeek A.G.T.G. Stud. Surf. Sci. Catal. 28:1986;169.
6. R. Szostak, Handbook of Molecular Sieves, Van Nostrand Reinhold, New York, 1992.
7. Chao K.J., Lin J.C., Wang Y., Lee G.H. Zeolites. 6:1986;35.
8. Flanigen E.M., Bennett J.M., Grose R.W., Cohen J.P., Patton R.L., Kirchner R.M., Smith J.V. Nature. 271:1978;512.
9. Dutta P.K., Puri M. J. Phys. Chem. 91:1987;4329.
10. Twu J., Dutta P.K., Kresge C.T. Zeolites. 11:1991;672.
11. Chang C.D., Bell A.T. Catal. Lett. 8:1991;305.
12. Gittelman C.S., Bell A.T., Radke C.J. Microporous Mater. 2:1994;145.
13. Gabelica Z., Nagy B.J., Bodart P., Dewaele N., Nastro A. Zeolites. 7:1987;67.
14. B. Subotic, A.M. Tonejc, D. Bagovic, A. Cizmek, T. Antonic, in: J. Weitkamp, H.G. Karge, H. Pfeiffer, W. Hölderich (Eds.), Proceedings of the 10th International Zeolite Conference, Elsevier, Amsterdam, 1994, p. 259.
15. Ito T., Fraissard J., B.Nagy J., Dewaele N., Gabelica Z., Nastro A., Derouane E.G. Stud. Surf. Sci. Catal. 49A:1989;579.
16. Burkett S.L., Davis M.E. J. Phys. Chem. 98:1994;4647.
17. Gies H., Marler B. Zeolites. 12:1992;42.
18. Dougherty J., Iton L.E., White J.W. Zeolites. 15:1995;640.
19. Dokter W.H., van Garderen H.F., Beelen T.P.M., van Santen R.A., Bras W. Angew. Chem. Int. Ed. Engl. 34:1995;73.
20. Regev O., Cohen Y., Kehat E., Talmon Y. Zeolites. 14:1994;314.
21. Schoeman B.J., Sterte J., Otterstedt J.-E. J. Porous Mater. 1:1995;185.
22. Twomey T.A.M., Mackay M., Kuipers H.P.C.E., Thompson R.W. Zeolites. 14:1994;162.
23. F. Marcuccilli-Hoffner, Ph.D. thesis, Université de Haute Alsace, Mulhouse, France, 1994.
24. Axon S.A., Klinowski J. J. Chem. Soc., Faraday Trans. 89:1993;4245.
25. Bodart P., B.Nagy J., Gabelica Z., Derouane E.G. J. Chim. Phys. 83:1986;777.
26. Chen C.Y., Burkett S.L., Li H.X., Davis M.E. Microporous Mater. 2:1993;27.
27. Shi J.M., Anderson M.W., Carr S.W. Chem. Mater. 8:1996;369.
28. Iton L.E., Trouw F., Brun T.O., Epperson J.E., White J.W., Henderson S.J. Langmuir. 8:1992;1045.
29. Norby P., Christensen A.N., Hanson J.C. Stud. Surf. Sci. Catal. 84:1994;179.
30. Rey F., Sankar G., Thomas J.M., Barrett P.A., Lewis D.W., Catlow C.R.A., Clark S.M., Greaves G.N. Chem. Mater. 7:1995;1435.
31. Schoeman B.J. Stud. Surf. Sci. Catal. 105:1997;647.
32. Gora L., Streletzky K., Thompson R.W., Phillies G.D.J. Zeolites. 18:1997;119.
33. Schoeman B.J. Zeolites. 18:1997;97.
34. Watson J.N., Iton L.E., Keir R.I., Thomas J.C., Dowling T.L., White J.W. J. Phys. Chem. B. 101(48):1997;10094.
35. Gougeon R., Chezeau J.M., Meurer B. Solid State Nucl. Magn. Reson. 4:1995;281.
36. B.Nagy J., Gabelica Z., Derouane E.G. Zeolites. 3:1983;43.
37. Chezeau J.M., Delmotte L., Hasebe T., Chanh N.B. Zeolites. 11:1991;729.
38. G. Engelhardt, D. Michel, High Resolution Solid-State NMR of Silicates and Zeolites, Wiley, New York, 1987.
39. R.K. Harris, Nuclear Magnetic Resonance Spectroscopy, Longman Scientific and Technical, Essex, 1983, p. 119.
40. Carles J.E., Scallan A.M. J. Appl. Polym. Sci. 17:1973;1855.
41. Schneider W.A., Bernstein H.J., Pople J.A. J. Chem. Phys. 28:1958;601.
42. Muller N. J. Chem. Phys. 43:1965;2555.
43. I. Hasegawa, S. Sakka, in: M.L. Occelli, H.E. Robson (eds.), Zeolite Synthesis, ACS Symp. Ser. 398, American Chemical Society, Washington, DC, 1989, p. 140.
44. McCormick A.V., Bell A.T. Catal. Rev. Sci. Eng. 31:1989;97.
45. Hoebbel D., Garzó G., Engelhardt G., Vargha A. Z. Anorg. Allg. Chem. 494:1982;31.
46. J.P. Gilson, in: E.G. Derouane, F. Lemos, C. Naccache, F.R. Ribeiro (Eds.), Zeolites Microporous Solids: Synthesis, Structure and Reactivity, NATO ASI Ser. 352, 1992, p. 19.
47. R.K. Iler, The Chemistry of Silica, Wiley, New York, 1979, p. 42.
48. J.L. Guth, H. Kessler, R. Wey, in: Y. Murakami, A. Iijima, J.W. Ward (Eds.), New Developments in Zeolite Science and Technology, Elsevier, Tokyo, 1986, p. 121.
49. A. Abragam, The Principles of Nuclear Magnetism, Clarendon Press, Oxford, 1962.