Synthesis of trinuclear rhenium halide sulfide cluster complexes with triethylphosphine ligands [Re3(μ3-S)2(μ2-S) 2(μ2-Br)Br2(PEt3)4] and [Re3(μ3-S)2(μ2-S) 2(μ2-Cl)Cl3(PEt3)3]

Chemistry Letters

Volumn , Issue 7, 1997, Pages 671-672

  Yamada, Soichiro ^a   Miyake, Naofumi ^a   Imoto, Hideo ^a   Saito, Taro ^a  

^a UNIVERSITY OF TOKYO   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0040997839     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.1997.671     Document Type: Article

References (14)

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2. "Early Transition Metal Clusters with π-Donor Ligands," ed by M. H. Chisholm, VCH, New York (1995).
3. N. N. Timoshchenko, V. L. Kolosnichenko, S. V. Volkov, Y. L. Slovokhotov, and Y. T. Struchkov, Koord. Khim., 16, 1062 (1990).
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7. T. Saito, in "Early Transition Metal Clusters with π-Donor Ligands," ed by M.H. Chisholm, VCH, New York (1995), p. 63.
8. 14 The Re, Br, and P atoms were refined anisotropically, and other atoms isotropically. Hydrogen atoms were not included in the refinements.
9. 0|); 6° < 2θ < 60°). The intensity data were collected by a Rigaku AFC-7R diffractometer with MoKα (λ = 0.7107 Å) radiation at 297 K. The structure was solved by the similar procedure described for the compound 1.
10. T. Saito, Y. Kajitani, T. Yamagata, and H. Imoto, Inorg. Chem., 29, 2951 (1990).
11. K. Hashizume, Y. Mizobe, and M. Hidai, Organometallics, 14, 5367 (1995).
12. K. Tsuge, H. Imoto, and T. Saito, Inorg. Chem., 34, 3404 (1995).
13. teXsan, Molecular Structure Corporation, (1985 & 1992).
14. H. Imoto, Program for the Least-Squares Refinement of Atomic Parameters with Full Matrix and Block Diagonal Matrix Methods. The University of Tokyo, (1989).