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46
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0039663882
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note
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It was verified in a separate experiment that the observed signal resulted really from an interaction of the phenoxyl radical with the catalyst: Phenoxyl radicals generated with lead dioxide were mixed with the catalyst leading to the same signal in UV/Vis spectrum with a maximum at λ = 707 nm.
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47
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0039663883
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note
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The product 12 which was also formed in the catalytic cycle could not be isolated due to its decomposition during the reaction and on the silica gel column being turned into the iminoquinone 11.
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48
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0039071867
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note
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Recent investigations [1c] have shown that the nitrobenzene (13) is formed by oxidation of the primary product nitrosobenzene (10) by an excess of TBHP.
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50
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