Synthesis and X-ray crystal analysis of [Cu2(HCOO)tpmc]-[Cu2(CH3COO)tpmc](CIO4)6 6H2O (tpmc = N,N,B,B-tetrakis-(2-pyridylmethyl)-1,4,8,11-tetraazacyclotetradecane). Preparation and characterization of [Cu2(HCOO)tpmc](CIO4)3 H2O

Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry

Volumn 31, Issue 7, 2001, Pages 1189-1203

  Bogdanović, Goran A ^a,c   Miodragović, Zoran M ^b   Vučković, Gordana ^b   Marković, Rade ^b   Biré, Anne Spasojević De ^c  

^a UNIVERSITY OF BELGRADE   (Serbia)

^b UNIVERSITY OF BELGRADE   (Serbia)

^c ECOLE CENTRALE PARIS   (France)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0040483743     PISSN: 00945714     EISSN: None     Source Type: Journal    
DOI: 10.1081/SIM-100106857     Document Type: Article

References (20)

1. Miodragović, Z.M.; Vučković, G.; Sovilj, S.P.; Manojlović, D.D.; Malinar, M.J. Carbonato, Oxalato and Malonato Bridged Cu(II) and Co(II) Complexes with an Octaazamacrocyclic Ligand. J. Serb. Chem. Soc. 1998, 63 (10), 781-791; Chem. Abstr. 1999, 130, 60169z.
2. Miodragović, Z.M.; Vučković, G.; Sovilj, S.P.; Manojlović, D.D.; Malinar, M.J. Carbonato, Oxalato and Malonato Bridged Cu(II) and Co(II) Complexes with an Octaazamacrocyclic Ligand. J. Serb. Chem. Soc. 1998, 63 (10), 781-791; Chem. Abstr. 1999, 130, 60169z.
3. Asato, E.; Toftlund, H.; Kida, S.; Mikuriya, M.; Murray, K.S. Preparation and Characterization of Copper(II) Complexes with 1,4,8,11-Tetrakis(2-pyridylmethyl)-1,4,8,11-tetraazacyclotetradecane. Inorg. Chim. Acta 1989, 165, 207-214.
4. 2 O. Inorg. Chim. Acta 1990, 171, 45-52.
5. 2 . J. Chem. Soc. Dalton Trans. 1986, (8), 1743-1745.
6. 3 COO; n = 0, 1, or 2). Effect of Incorporation of an Anion X on the Structure of the Complex Cation. Bull. Chem. Soc. Jpn. 1987, 60 (5), 1681-1689.
7. Enraf-Nonius. CAD-4 Software. Version 5. Enraf-Nonius, Delft, The Netherlands, 1989.
8. Fair, C.K. MolEN, An Interactive Intelligent System for Crystal Structure Analysis, Enraf-Nonius, Delft, The Netherlands 1990.
9. a) Sheldrick, G.M. Phase Annealing in SHELX-90: Direct Methods for Larger Structures. Acta Cryst. A46, 1990, 467-473.
10. b) Sheldrick, G.M. SHELXS86 Program for the Solution of Crystal Structures, University of Göttingen, Germany, 1985.
11. Sheldrick, G.M. SHELXL97, Program for the Refinement of Crystal Structures, University of Göttingen, Germany, 1997.
12. Nardelli, M. PARST95 - an Update to PARST: a System of Fortran Routines for Calculating Molecular Structure Parameters from the Results of Crystal Structure Analyses. J. Appl. Cryst. 1995, 28, 659.
13. Burnett, M.N.; Johnson, C.K. ORTEPIII, Report ORNL-6895; Oak Ridge National Laboratory: Tennessee, USA, 1996.
14. Geary, W.J. The Use of Conductivity Measurements in Organic Solvents for the Characterization of Coordination Compounds. Coord. Chem. Rev. 1971, 7, 79-122.
15. Silverstein, R.M.; Bassler, G.C.; Morrill T.C. Infrared Spectrometry. In Spectrometric Identification of Organic Compounds; 3rd Edn.: J. Wiley and Sons, New York, 1974, 101-102, 116.
16. Schmelz, M.J.; Nikagava, I.; Nizushima, S.; Quagliano, Q. Infrared Absorption Spectra of Inorganic Coordination Complexes. XVIII. Infrared Studies of Malonato Metal Complexes. J. Am. Chem. Soc. 1959, 81, 287-290.
17. Nakamoto, K. Infrared and Raman Spectra of Inorganic and Coordination Compounds; Part B, 5th Edn.; John Wiley and Sons: New York, 1997.
18. Deacon, G.B.; Philips, R.J. Relationships Between the Carbon-Oxygen Stretching Frequencies of Carboxylato Complexes and the Type of Carboxylate Coordination. Coord. Chem. Rev., 1980, 33, 227-250.
19. Ferarro, J.R. Inorganic Infrared Spectroscopy. J. Chem. Edu. 1961, 38, 201-208.
20. Cotton, F.A.; Wilkinson, G. Advanced Inorganic Chemistry; 5th Edn.; John Wiley and Sons: New York, 1988.