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Organometallics

Volumn 15, Issue 16, 1996, Pages 3474-3476

Study of paramagnetic chromocenes by solid-state NMR spectroscopy

(4) Blümel, Janet a Herker, Martin a,b Hiller, Wolfgang a,b Köhler, Frank H a

a TECHNICAL UNIVERSITY OF MUNICH (Germany)

b Crystal Structure Analysis ^*

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0040226711 PISSN: 02767333 EISSN: None Source Type: Journal
DOI: 10.1021/om960042p Document Type: Article

Times cited : (56)

References (46)

1
- 0004236045
- VCH Publishers: New York
- Kahn, O. Molecular Magnetism; VCH Publishers: New York, 1993.
- (1993) Molecular Magnetism
- Kahn, O.¹

2
- 5244268259
- Academic Press: New York
- (a) Kochi, J. K. Organometallic Reaction Mechanisms and Catalysis; Academic Press: New York, 1987.
- (1987) Organometallic Reaction Mechanisms and Catalysis
- Kochi, J.K.¹

3
- 0003827131
- Marcel Dekker Inc.: New York
- (b) Bell, A. T., Pines, A., Eds. NMR Techniques in Catalysis; Marcel Dekker Inc.: New York, 1994.
- (1994) NMR Techniques in Catalysis
- Bell, A.T.¹ Pines, A.²

4
- 84990156612
- (c) Astruc, D. Angew. Chem., Int. Ed. Engl. 1988, 27, 643-660.
- (1988) Angew. Chem., Int. Ed. Engl. , vol.27 , pp. 643-660
- Astruc, D.¹

5
- 0346361128
- (d) Astruc, D. Chem. Rev. 1989, 89, 1189.
- (1989) Chem. Rev. , vol.89 , pp. 1189
- Astruc, D.¹

6
- 5244316004
- (e) Lindblad, T.; Rebenstorf, B. J. Chem. Soc., Faraday Trans. 1991, 87, 2474.
- (1991) J. Chem. Soc., Faraday Trans. , vol.87 , pp. 2474
- Lindblad, T.¹ Rebenstorf, B.²

7
- 0000433711
- (f) Herrmann, W. A.; Scherer, W.; Fischer, R. W.; Blümel, J.; Kleine, M.; Mertin, W.; Gruehn, R.; Mink, J.; Boysen, H.; Wilson, C. C.; Ibberson, R. M.; Bachmann, L.; Mattner, M. J. Am. Chem. Soc. 1995, 117, 3231.
- (1995) J. Am. Chem. Soc. , vol.117 , pp. 3231
- Herrmann, W.A.¹ Scherer, W.² Fischer, R.W.³ Blümel, J.⁴ Kleine, M.⁵ Mertin, W.⁶ Gruehn, R.⁷ Mink, J.⁸ Boysen, H.⁹ Wilson, C.C.¹⁰ Ibberson, R.M.¹¹ Bachmann, L.¹² Mattner, M.¹³

8
- 0001569439
- Day, P. Science 1993, 267, 431. Gatteschi, D. Adv. Mater. 1994, 6, 635. Miller, J. S.; Epstein, J. Angew. Chem., Int. Ed. Engl. 1994, 33, 385.
- (1993) Science , vol.267 , pp. 431
- Day, P.¹

9
- 0028513233
- Day, P. Science 1993, 267, 431. Gatteschi, D. Adv. Mater. 1994, 6, 635. Miller, J. S.; Epstein, J. Angew. Chem., Int. Ed. Engl. 1994, 33, 385.
- (1994) Adv. Mater. , vol.6 , pp. 635
- Gatteschi, D.¹

10
- 33748886713
- Day, P. Science 1993, 267, 431. Gatteschi, D. Adv. Mater. 1994, 6, 635. Miller, J. S.; Epstein, J. Angew. Chem., Int. Ed. Engl. 1994, 33, 385.
- (1994) Angew. Chem., Int. Ed. Engl. , vol.33 , pp. 385
- Miller, J.S.¹ Epstein, J.²

11
- 0001643121
- Recent contributions are as follows: (a) Ganapathy, S.; Chacko, V. P.; Bryant, R. G.; Etter, M. C. J. Am. Chem. Soc. 1986, 108, 3159. (b) Walter, T. H.; Oldfield, E. J. Chem. Soc., Chem. Commun. 1987, 646. (c) Nayeem, A.; Yesinowski, J. P. J. Chem. Phys. 1988, 89, 4600. (d) Campbell, G. C.; Reibenspies, J. H.; Haw, J. F. Inorg. Chem. 1991, 30, 171. (e) Brough, A. R.; Grey, P. C.; Dobson, C. M. J. Am. Chem. Soc. 1993, 115, 7318. (f) Lin, H. T.; DiNatale, J. A.; Void, R. R. J. Am. Chem. Soc. 1994, 116, 2133. (g) Liu, K,; Ryan, D.; Nakanishi, K.; McDermott, A. J. Am. Chem. Soc. 1995, 117, 6897. (h) van Moorsel, G.-J. M. P.; van Eck, E. R. H.; Grey, C. P. J. Magn. Reson., Ser. A 1995, 773, 159.
- (1986) J. Am. Chem. Soc. , vol.108 , pp. 3159
- Ganapathy, S.¹ Chacko, V.P.² Bryant, R.G.³ Etter, M.C.⁴

12
- 37049084771
- Recent contributions are as follows: (a) Ganapathy, S.; Chacko, V. P.; Bryant, R. G.; Etter, M. C. J. Am. Chem. Soc. 1986, 108, 3159. (b) Walter, T. H.; Oldfield, E. J. Chem. Soc., Chem. Commun. 1987, 646. (c) Nayeem, A.; Yesinowski, J. P. J. Chem. Phys. 1988, 89, 4600. (d) Campbell, G. C.; Reibenspies, J. H.; Haw, J. F. Inorg. Chem. 1991, 30, 171. (e) Brough, A. R.; Grey, P. C.; Dobson, C. M. J. Am. Chem. Soc. 1993, 115, 7318. (f) Lin, H. T.; DiNatale, J. A.; Void, R. R. J. Am. Chem. Soc. 1994, 116, 2133. (g) Liu, K,; Ryan, D.; Nakanishi, K.; McDermott, A. J. Am. Chem. Soc. 1995, 117, 6897. (h) van Moorsel, G.-J. M. P.; van Eck, E. R. H.; Grey, C. P. J. Magn. Reson., Ser. A 1995, 773, 159.
- (1987) J. Chem. Soc., Chem. Commun. , pp. 646
- Walter, T.H.¹ Oldfield, E.²

13
- 36549097451
- Recent contributions are as follows: (a) Ganapathy, S.; Chacko, V. P.; Bryant, R. G.; Etter, M. C. J. Am. Chem. Soc. 1986, 108, 3159. (b) Walter, T. H.; Oldfield, E. J. Chem. Soc., Chem. Commun. 1987, 646. (c) Nayeem, A.; Yesinowski, J. P. J. Chem. Phys. 1988, 89, 4600. (d) Campbell, G. C.; Reibenspies, J. H.; Haw, J. F. Inorg. Chem. 1991, 30, 171. (e) Brough, A. R.; Grey, P. C.; Dobson, C. M. J. Am. Chem. Soc. 1993, 115, 7318. (f) Lin, H. T.; DiNatale, J. A.; Void, R. R. J. Am. Chem. Soc. 1994, 116, 2133. (g) Liu, K,; Ryan, D.; Nakanishi, K.; McDermott, A. J. Am. Chem. Soc. 1995, 117, 6897. (h) van Moorsel, G.-J. M. P.; van Eck, E. R. H.; Grey, C. P. J. Magn. Reson., Ser. A 1995, 773, 159.
- (1988) J. Chem. Phys. , vol.89 , pp. 4600
- Nayeem, A.¹ Yesinowski, J.P.²

14
- 0000663499
- Recent contributions are as follows: (a) Ganapathy, S.; Chacko, V. P.; Bryant, R. G.; Etter, M. C. J. Am. Chem. Soc. 1986, 108, 3159. (b) Walter, T. H.; Oldfield, E. J. Chem. Soc., Chem. Commun. 1987, 646. (c) Nayeem, A.; Yesinowski, J. P. J. Chem. Phys. 1988, 89, 4600. (d) Campbell, G. C.; Reibenspies, J. H.; Haw, J. F. Inorg. Chem. 1991, 30, 171. (e) Brough, A. R.; Grey, P. C.; Dobson, C. M. J. Am. Chem. Soc. 1993, 115, 7318. (f) Lin, H. T.; DiNatale, J. A.; Void, R. R. J. Am. Chem. Soc. 1994, 116, 2133. (g) Liu, K,; Ryan, D.; Nakanishi, K.; McDermott, A. J. Am. Chem. Soc. 1995, 117, 6897. (h) van Moorsel, G.-J. M. P.; van Eck, E. R. H.; Grey, C. P. J. Magn. Reson., Ser. A 1995, 773, 159.
- (1991) Inorg. Chem. , vol.30 , pp. 171
- Campbell, G.C.¹ Reibenspies, J.H.² Haw, J.F.³

15
- 0001144182
- Recent contributions are as follows: (a) Ganapathy, S.; Chacko, V. P.; Bryant, R. G.; Etter, M. C. J. Am. Chem. Soc. 1986, 108, 3159. (b) Walter, T. H.; Oldfield, E. J. Chem. Soc., Chem. Commun. 1987, 646. (c) Nayeem, A.; Yesinowski, J. P. J. Chem. Phys. 1988, 89, 4600. (d) Campbell, G. C.; Reibenspies, J. H.; Haw, J. F. Inorg. Chem. 1991, 30, 171. (e) Brough, A. R.; Grey, P. C.; Dobson, C. M. J. Am. Chem. Soc. 1993, 115, 7318. (f) Lin, H. T.; DiNatale, J. A.; Void, R. R. J. Am. Chem. Soc. 1994, 116, 2133. (g) Liu, K,; Ryan, D.; Nakanishi, K.; McDermott, A. J. Am. Chem. Soc. 1995, 117, 6897. (h) van Moorsel, G.-J. M. P.; van Eck, E. R. H.; Grey, C. P. J. Magn. Reson., Ser. A 1995, 773, 159.
- (1993) J. Am. Chem. Soc. , vol.115 , pp. 7318
- Brough, A.R.¹ Grey, P.C.² Dobson, C.M.³

16
- 0001414393
- Recent contributions are as follows: (a) Ganapathy, S.; Chacko, V. P.; Bryant, R. G.; Etter, M. C. J. Am. Chem. Soc. 1986, 108, 3159. (b) Walter, T. H.; Oldfield, E. J. Chem. Soc., Chem. Commun. 1987, 646. (c) Nayeem, A.; Yesinowski, J. P. J. Chem. Phys. 1988, 89, 4600. (d) Campbell, G. C.; Reibenspies, J. H.; Haw, J. F. Inorg. Chem. 1991, 30, 171. (e) Brough, A. R.; Grey, P. C.; Dobson, C. M. J. Am. Chem. Soc. 1993, 115, 7318. (f) Lin, H. T.; DiNatale, J. A.; Void, R. R. J. Am. Chem. Soc. 1994, 116, 2133. (g) Liu, K,; Ryan, D.; Nakanishi, K.; McDermott, A. J. Am. Chem. Soc. 1995, 117, 6897. (h) van Moorsel, G.-J. M. P.; van Eck, E. R. H.; Grey, C. P. J. Magn. Reson., Ser. A 1995, 773, 159.
- (1994) J. Am. Chem. Soc. , vol.116 , pp. 2133
- Lin, H.T.¹ DiNatale, J.A.² Void, R.R.³

17
- 0001013040
- Recent contributions are as follows: (a) Ganapathy, S.; Chacko, V. P.; Bryant, R. G.; Etter, M. C. J. Am. Chem. Soc. 1986, 108, 3159. (b) Walter, T. H.; Oldfield, E. J. Chem. Soc., Chem. Commun. 1987, 646. (c) Nayeem, A.; Yesinowski, J. P. J. Chem. Phys. 1988, 89, 4600. (d) Campbell, G. C.; Reibenspies, J. H.; Haw, J. F. Inorg. Chem. 1991, 30, 171. (e) Brough, A. R.; Grey, P. C.; Dobson, C. M. J. Am. Chem. Soc. 1993, 115, 7318. (f) Lin, H. T.; DiNatale, J. A.; Void, R. R. J. Am. Chem. Soc. 1994, 116, 2133. (g) Liu, K,; Ryan, D.; Nakanishi, K.; McDermott, A. J. Am. Chem. Soc. 1995, 117, 6897. (h) van Moorsel, G.-J. M. P.; van Eck, E. R. H.; Grey, C. P. J. Magn. Reson., Ser. A 1995, 773, 159.
- (1995) J. Am. Chem. Soc. , vol.117 , pp. 6897
- Liu, K.¹ Ryan, D.² Nakanishi, K.³ McDermott, A.⁴

18
- 37149034829
- Recent contributions are as follows: (a) Ganapathy, S.; Chacko, V. P.; Bryant, R. G.; Etter, M. C. J. Am. Chem. Soc. 1986, 108, 3159. (b) Walter, T. H.; Oldfield, E. J. Chem. Soc., Chem. Commun. 1987, 646. (c) Nayeem, A.; Yesinowski, J. P. J. Chem. Phys. 1988, 89, 4600. (d) Campbell, G. C.; Reibenspies, J. H.; Haw, J. F. Inorg. Chem. 1991, 30, 171. (e) Brough, A. R.; Grey, P. C.; Dobson, C. M. J. Am. Chem. Soc. 1993, 115, 7318. (f) Lin, H. T.; DiNatale, J. A.; Void, R. R. J. Am. Chem. Soc. 1994, 116, 2133. (g) Liu, K,; Ryan, D.; Nakanishi, K.; McDermott, A. J. Am. Chem. Soc. 1995, 117, 6897. (h) van Moorsel, G.-J. M. P.; van Eck, E. R. H.; Grey, C. P. J. Magn. Reson., Ser. A 1995, 773, 159.
- (1995) J. Magn. Reson., Ser. A , vol.773 , pp. 159
- Van Moorsel, G.-J.M.P.¹ Van Eck, E.R.H.² Grey, C.P.³

19
- 0346109802
- (a) Haw, J. F.; Campbell, G. C. J. Magn. Reson. 1986, 66, 558.
- (1986) J. Magn. Reson. , vol.66 , pp. 558
- Haw, J.F.¹ Campbell, G.C.²

20
- 0542419227
- (b) McGarvey, B. R.; Nagy, S. Inorg. Chim. Acta 1987, 739, 319 and Inorg. Chem. 1987, 26, 4198.
- (1987) Inorg. Chim. Acta , vol.739 , pp. 319
- McGarvey, B.R.¹ Nagy, S.²

21
- 0040214081
- (b) McGarvey, B. R.; Nagy, S. Inorg. Chim. Acta 1987, 739, 319 and Inorg. Chem. 1987, 26, 4198.
- (1987) Inorg. Chem. , vol.26 , pp. 4198

22
- 0001414011
- (c) Finch, W. C.; Gillespie, R. D.; Hedden, D.; Marks, T. J. J. Am. Chem. Soc. 1990, 112, 6221.
- (1990) J. Am. Chem. Soc. , vol.112 , pp. 6221
- Finch, W.C.¹ Gillespie, R.D.² Hedden, D.³ Marks, T.J.⁴

23
- 0039412798
- (d) Benn, R.; Grondey, H. J. Magn. Reson. 1990, 89, 375.
- (1990) J. Magn. Reson. , vol.89 , pp. 375
- Benn, R.¹ Grondey, H.²

24
- 33748216891
- (e) Kölle, U.; Kossakowski, J.; Klaff, N.; Wesemann, L.; Englert, U.; Herberich, G. E. Angew. Chem., Int. Ed. Engl. 1991, 30, 690.
- (1991) Angew. Chem., Int. Ed. Engl. , vol.30 , pp. 690
- Kölle, U.¹ Kossakowski, J.² Klaff, N.³ Wesemann, L.⁴ Englert, U.⁵ Herberich, G.E.⁶

25
- 33845555055
- The chromocenes were prepared as described in: (a) Robbins, J. L.; Edelstein, N.; Spencer, B.; Smart, J. C. J. Am. Chem. Soc. 1982, 104, 1882. (b) Köhler, F. H. In Organometallic Synthesis; King, R. B., Eisch, J. J., Eds.; Elsevier: Amsterdam, 1988; Vol. 4, p 52. (c) Hebendanz, N.; Köhler, F. H.; Scherbaum, F.; Schlesinger, B. J. Magn. Reson. 1989, 27, 798.
- (1982) J. Am. Chem. Soc. , vol.104 , pp. 1882
- Robbins, J.L.¹ Edelstein, N.² Spencer, B.³ Smart, J.C.⁴

26
- 33845555055
- King, R. B., Eisch, J. J., Eds.; Elsevier: Amsterdam
- The chromocenes were prepared as described in: (a) Robbins, J. L.; Edelstein, N.; Spencer, B.; Smart, J. C. J. Am. Chem. Soc. 1982, 104, 1882. (b) Köhler, F. H. In Organometallic Synthesis; King, R. B., Eisch, J. J., Eds.; Elsevier: Amsterdam, 1988; Vol. 4, p 52. (c) Hebendanz, N.; Köhler, F. H.; Scherbaum, F.; Schlesinger, B. J. Magn. Reson. 1989, 27, 798.
- (1988) Organometallic Synthesis , vol.4 , pp. 52
- Köhler, F.H.¹

27
- 84989064988
- The chromocenes were prepared as described in: (a) Robbins, J. L.; Edelstein, N.; Spencer, B.; Smart, J. C. J. Am. Chem. Soc. 1982, 104, 1882. (b) Köhler, F. H. In Organometallic Synthesis; King, R. B., Eisch, J. J., Eds.; Elsevier: Amsterdam, 1988; Vol. 4, p 52. (c) Hebendanz, N.; Köhler, F. H.; Scherbaum, F.; Schlesinger, B. J. Magn. Reson. 1989, 27, 798.
- (1989) J. Magn. Reson. , vol.27 , pp. 798
- Hebendanz, N.¹ Köhler, F.H.² Scherbaum, F.³ Schlesinger, B.⁴

28
- 0030600618
- Flower, K. R.; Hitchcock, P. B. J. Organomet. Chem. 1996, 507, 275.
- (1996) J. Organomet. Chem. , vol.507 , pp. 275
- Flower, K.R.¹ Hitchcock, P.B.²

29
- 0003922654
- Academic Press: New York
- Haeberlen, U. High Resolution NMR in Solids. Selective Averaging; Academic Press: New York, 1976; p 17. Spiess, H. W.; Zimmermann, H.; Haeberlen, U. Chem. Phys. 1976, 12, 123.
- (1976) High Resolution NMR in Solids. Selective Averaging , pp. 17
- Haeberlen, U.¹

30
- 0012398762
- Haeberlen, U. High Resolution NMR in Solids. Selective Averaging; Academic Press: New York, 1976; p 17. Spiess, H. W.; Zimmermann, H.; Haeberlen, U. Chem. Phys. 1976, 12, 123.
- (1976) Chem. Phys. , vol.12 , pp. 123
- Spiess, H.W.¹ Zimmermann, H.² Haeberlen, U.³

31
- 85033868346
- note
- 1H) scans, i.e., after 10 min or less; line broadening factors of 20, 100, and 0 Hz, respectively were applied. Water and adamantane (low-frequency signal) were used as external standards.

32
- 0000194687
- McDermott, A. E.; Creuzet, F. J.; Kolbert, A. C.; Griffin, R. G. J. Magn. Reson. 1992, 98, 408.
- (1992) J. Magn. Reson. , vol.98 , pp. 408
- McDermott, A.E.¹ Creuzet, F.J.² Kolbert, A.C.³ Griffin, R.G.⁴

33
- 0242464536
- Clayton, A. N.; Dobson, C. M.; Grey, C. P. J. Chem. Soc., Chem. Commun. 1990, 72-74. Groombridge, C. J.; Perkins, M. J. J. Chem. Soc., Chem. Commun. 1991, 1164.
- (1990) J. Chem. Soc., Chem. Commun. , pp. 72-74
- Clayton, A.N.¹ Dobson, C.M.² Grey, C.P.³

34
- 0025876039
- Clayton, A. N.; Dobson, C. M.; Grey, C. P. J. Chem. Soc., Chem. Commun. 1990, 72-74. Groombridge, C. J.; Perkins, M. J. J. Chem. Soc., Chem. Commun. 1991, 1164.
- (1991) J. Chem. Soc., Chem. Commun. , pp. 1164
- Groombridge, C.J.¹ Perkins, M.J.²

35
- 0344968679
- Laukin, G.; Noack, F. Z. Phys. 1960, 159, 311.
- (1960) Z. Phys. , vol.159 , pp. 311
- Laukin, G.¹ Noack, F.²

36
- 85033859238
- note
- 8: Cao, R.; Köhler, F. H. Unpublished data.

37
- 85033838610
- note
- 1H) = 5.0 and -16.1.

38
- 0000194882
- (a) Bjorholm, T.; Jakobsen, H. J. J. Magn. Reson. 1989, 84, 204.
- (1989) J. Magn. Reson. , vol.84 , pp. 204
- Bjorholm, T.¹ Jakobsen, H.J.²

39
- 0000717771
- (b) Aguillar-Parrilla, F.; Wehle, B.; Bäunling, H.; Limbach, H.-H. J. Magn. Reson. 1990, 87, 592.
- (1990) J. Magn. Reson. , vol.87 , pp. 592
- Aguillar-Parrilla, F.¹ Wehle, B.² Bäunling, H.³ Limbach, H.-H.⁴

40
- 0000097909
- Grey, C. P.; Cheetham, A. K.; Dobson, C. M. J. Magn. Reson., Ser. A 1993, 101, 299.
- (1993) J. Magn. Reson., Ser. A , vol.101 , pp. 299
- Grey, C.P.¹ Cheetham, A.K.² Dobson, C.M.³

41
- 0001489662
- First attempt: Bottomley, F.; Chen, J.; McIntosh, S. M. Thompson, R. C. Organometallics 1991, 10, 906. These authors described the crystal structure to be in the orthorhombic C-centered space group Ccmm with disorder.
- (1991) Organometallics , vol.10 , pp. 906
- Bottomley, F.¹ Chen, J.² McIntosh, S.M.³ Thompson, R.C.⁴

42
- 85033837875
- note
- 9 was applied.

43
- 0003659725
- Springer-Verlag: Berlin, Chapter 4.4
- A reviewer suggested that off-resonance proton irradiation (Mehring, M. Principles of High Resolution NMR in Solids, 2nd ed.; Springer-Verlag: Berlin, 1983; Chapter 4.4) might be another reason.
- (1983) Principles of High Resolution NMR in Solids, 2nd Ed.
- Mehring, M.¹

44
- 36749105542
- (a) Rothwell, W. P.; Waugh, J. S. J. Chem.Phys. 1981, 74, 2721.
- (1981) J. Chem.Phys. , vol.74 , pp. 2721
- Rothwell, W.P.¹ Waugh, J.S.²

45
- 5244324650
- (b) Baumann, W.; Oprunenko, Y.; Günther, H. Z. Naturforsch. A 1994, 50, 429.
- (1994) Z. Naturforsch. A , vol.50 , pp. 429
- Baumann, W.¹ Oprunenko, Y.² Günther, H.³

46
- 0001066789
- (c) Long, J. R.; Sun, Q. B.; Bowen, A.; Griffin, R. G. J. Am. Chem. Soc. 1994, 116, 1150.
- (1994) J. Am. Chem. Soc. , vol.116 , pp. 1150
- Long, J.R.¹ Sun, Q.B.² Bowen, A.³ Griffin, R.G.⁴

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