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5844355934
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note
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Labeling of the atoms refers to those shown in Scheme 1. For compounds 2b and 3b, the assignment of the signals is based on comparison of the spectrum of the enriched fractions and those of the pure complexes 2a and 3a, respectively.
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51
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5844361045
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note
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Data given have for complex 4b were obtained at 240 K inmediately after the mixing of compound 1 and the stoichiometric amount of (-)-binap. The number of signals and their multiplicities were identical with those obtained from the comparison of the spectra recorded at 240 K for the solution obtained immediately after the mixing of compound 1 and the stoichiometric amount of (±)-binap and that of pure 4a at 240 K.
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53
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5844390183
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Manuscript in preparation
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Sheldrick, G. M. Manuscript in preparation.
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Sheldrick, G.M.1
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54
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