Synthesis of acylamido ketene dithioacetals and 5-oxo-4,5-dihydrobenzo[f]-1,4-thiazepine-derivatives by dithiocarboxylation of α-aza-c-nucleophiles

Phosphorus, Sulfur and Silicon and Related Elements

Volumn 122, Issue , 1997, Pages 71-86

  Dölling, Wolfgang ^a  

^a MARTIN LUTHER UNIVERSITY HALLE WITTENBERG   (Germany)

Author keywords

2,2,N trimethyl propionamides; 2 alkylthio 4 methyl 5 oxo 4,5 dihydrobenzo f 1,4 thiazepine 3 carbonitriles; 2 chloro N cyanomethyl N methyl benzamide; 3,3 bis(methylthio) prop 2 ene 1 ones; Carbon disulfide; Methyl 3,3 bis(methylthio) acrylates

Indexed keywords

EID: 0040090603     PISSN: 10426507     EISSN: None     Source Type: Journal    
DOI: 10.1080/10426509708043496     Document Type: Article

References (30)

1. W. Dölling, K. Frost, F. Heinemann and H. Hartung, Z. Naturforsch. B, 48b, 493, (1993).
2. W. Dölling, Phosphorus, Sulfur, and Silicon, 86, 129, (1994).
3. J. R. Housley, J. E. Jeffery, K. J. Nichol and B. J. Sargent, (Boots Co PLC), WO 9411360, Chem. Abstr. 121, 134167, (1994).
4. T. Oosawa, H. Murooka and A. Miwa, (Kirin Brewery), JP Patent 05271208 (1993); Chem. Abstr. 120, 245182, (1994).
5. T. Oosawa, H. Murooka and A. Miwa, (Kirin Brewery), JP Patent 05271208 (1993); Chem. Abstr. 120, 245182, (1994).
6. S. Kakehi and S. Ito, (Kissei Pharmaceutical, Japan), Jpn. Kokai Tokkyo Koho 06025257 A2 (1994); Chem. Abstr. 121, 134166, (1994).
7. S. Kakehi and S. Ito, (Kissei Pharmaceutical, Japan), Jpn. Kokai Tokkyo Koho 06025257 A2 (1994); Chem. Abstr. 121, 134166, (1994).
8. L. E. Brieaddy, (Wellcome Foundation Ltd., UK), WO 9605188 (1996); Chem. Abstr. 125, 114724, (1996).
9. L. E. Brieaddy, (Wellcome Foundation Ltd., UK), WO 9605188 (1996); Chem. Abstr. 125, 114724, (1996).
10. L. E. Brieaddy, (Wellcome Foundation Ltd.), WO 9316055 (1993); Chem. Abstr. 120, 164244, (1994).
11. L. E. Brieaddy, (Wellcome Foundation Ltd.), WO 9316055 (1993); Chem. Abstr. 120, 164244, (1994).
12. H. Junjappa, H. Ila and C. V. Asokan, Tetrahedron, 46, 5423, (1990).
13. H. Junjappa and H. Ila, Phosphorous, Sulfur, and Silicon, 95&96, 35, (1994).
14. M. Kolb, Synthesis, 171, (1990).
15. A. D. Dunn and W. -D. Rudorf, Carbon Disulfide in Organic Chemistry (Ellis Horwood Limited Publishers, Chichester, 1989).
16. W. -D. Rudorf, A. Schierhorn and M. Augustin, Tetrahedron, 35, 551, (1979).
17. W. -D. Rudorf, Tetrahedron, 34, 725, (1978).
18. W. -D. Rudorf, A. Schierhorn and M. Augustin, J. Prakt. Chem., 321, 1021, (1979).
19. W. -D. Rudorf and D. Janietz Synthesis, 854, (1984).
20. K. -H. Wünsch and A. Ehlers, Z. Chem., 10, 361, (1970).
21. J. T. Sharp, Seven-membered Rings with Two or More Heteroatoms, in Comprehensive Heterocyclic Chemistry, Vol. 7, A. R. Katritzky and C. W. Rees, eds, (Pergamon Press, Oxford New York Toronto Sydney Paris Frankfurt, 1984) pp. 631-636.
22. H. Shimizu, N. Ueda, T. Kataoka and M. Hori, Chem. Pharm. Bull., 32, 2571, (1984).
23. H. Hofmann and H. Fischer, Chem. Ber., 121, 2147, (1988).
24. R. B. Morin and D. O. Spry, J. Chem. Soc. D, 335, (1970).
25. J. F. Bunnett and R. E. Zahler, Chem. Rev., 49, 273, (1951).
26. J. Miller, Aromatic Nucleophilic Substitution (Elsevier, Amsterdam, 1968).
27. N. Kornblum, L. Cheng, R. C. Kerber, M. M. Kestner, B. N. Newton, H. W. Pinnick, R. G. Smith and P. A. Wade, J. Org. Chem., 41, 1560, (1976).
28. C. Paradisi, Arene Substitution via Nucleophilic Addition to Electron Deficient Arenes, in Comprehensive Organic Chemistry, Vol. 4, B. M. Trost, I. Fleming and M. F. Semmelhack, eds, (Pergamon Press, Oxford New York Seoul Tokyo, 1991), pp. 423-450.
29. A. Garofalo, V. Nacci, F. Corelli and G. Campiani, Heterocycles, 31, 1291, (1949).
30. M. Asscher, Rec. trav. Chim. Pays-Bas, 68, 960, (1949).