In situ real-time environmental high resolution electron microscopy of nanometer size novel xerogel catalysts for hydrogenation reactions in Nylon 6,6

Microscopy and Microanalysis

Volumn 6, Issue 4, 2000, Pages 335-342

  Gai, Pratibha L ^a,b   Kourtakis, Kostantinos ^a   Ziemecki, Stanislav ^a  

^a Applied Science and Engineering Laboratories   (United States)

^b UNIVERSITY OF DELAWARE   (United States)

Author keywords

Adiponitrile hydrogenation; Atomic resolution; In situ real time environmental high resolution electron microscopy; Nylon; Polymerization; Scanning electron microscopy

Indexed keywords

EID: 0039594708     PISSN: 14319276     EISSN: None     Source Type: Journal    
DOI: 10.1017/S1431927602000582     Document Type: Article

References (15)

1. Boyes ED (1998) High resolution low voltage SEM imaging and chemical microanalysis. Adv Mater 10:1277
2. Bradford MCJ, Vannice MA (1998) Reforming of CH4 over supported Pt catalysts. J Catal 173:157
3. Bradley B, et al (1978) Metal Alkoxides. New York: Academic Press
4. Darji R, Howie A (1997) Scattering corrections in small particle imaging. Micron 28:95
5. de Bellefon C, Fouilloux P (1994) Nitriles in liquid phase. Cat Rev Sci Eng 36:459
6. Gai PL (1981) In situ, direct studies of metal oxide catalysts. Philos Mag 43:841
7. Gai PL (1992) Defects in oxide catalysts: Fundamental studies of catalysts in action. Cat Rev Sci Eng 34:1
8. Gai PL (ed) (1997) In-situ Microscopy in Materials Research. Boston: Kluwer
9. Gai PL (1998) Direct probing of gas molecule-catalyst interactions on the atomic scale. Adv Mater 10:1259
10. Gai PL (1999a) Probing selective oxidation catalysis under reaction conditions by atomic scale EHREM. Curr Opin Solid State Mater Sci 4:63
11. Gai PL (1999b) Environmental high resolution electron microscopy of gas-catalyst reactions. Top Catal 8:97
12. Gai PL, Kourtakis K (1995) Solid state defect mechanisms in vanadyl pyrophosphates: implications for selective oxidation. Science 267:647
13. Mares F, Galle J, Diamond S, Regina F (1988) Preparation and characterization of catalysts for aminonitriles. J Catal 112:145
14. Tauster S, Fung S, Garten JL (1978) Strong metal-support interactions. J Am Chem Soc 100:170
15. Ziemecki SB (1993) In: Studies Surf Sci Catal, Het Catal Fine Chem III, Guisnet M, et al. (eds). Elsevier, 78:283