The synthesis and X-ray crystal structure of S=CS2C2B10H10

Polyhedron

Volumn 16, Issue 11, 1997, Pages 1819-1824

  McKinney, James D ^a   Hamor, Thomas A ^a   Jones, Christopher J ^a   Paxton, Keith ^a  

^a UNIVERSITY OF BIRMINGHAM   (United Kingdom)

Author keywords

Crystal structure; Dicarbaborane; Disulfur heterocycle; Thione

Indexed keywords

EID: 0039415337     PISSN: 02775387     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0277-5387(96)00493-7     Document Type: Article

References (27)

1. (a) F. Wudl, G. M. Smith and E. F. Hufnagel, J. Chem. Soc., Chem. Commun. 1453, 1970;
2. (b) A. F. Garito and A. J. Heeger, Acc. Chem. Res. 1974, 7, 232;
3. (c) Kreif, A., Tetrahedron, 1986, 42, 1209;
4. (d) T. K. Hansen and J. Becher, Adv. Mat. 1993, 5, 288;
5. (e) T. Jørgensen, T. K. Hansen and J. Becher, Chem. Soc. Rev. 1994, 23, 41.
6. (a) T. J. Enge, W. A. Bryden, F. M. Wiygul, D. O. Cowan, T, J. Kistenmacher and A. N. Bloch, J. Chem. Phys. 1982, 77, 3188;
7. (b) A. Bondi, J. Phys. Chem. 1964, 68, 441.
8. (a) W. R. H. Hartley and S. S. Smiles, J. Chem. Soc. 2263, 1926;
9. (b) J. Nakayama, Synthesis, 1975, 168;
10. (c) C. A. Brown, R. D. Miller, C. M. Lindsey and K. Smith, Tetrahedron Lett. 1984, 991;
11. (d) C. M. Lindsey, K. Smith, C. A. Brown and K. Betterton-Cruz, Tetrahedron Lett. 1984, 995.
12. (a) J. R. Ferraro and J. M. Williams, Introduction to Synthetic Electrical Conductors, Academic Press, New York, (1987), pp 1-327.
13. (b) M. Williams, A. J. Schultz, A. E. Underhill and D. M. Watkins, Extended Linear Chain Compounds, Vol. 1. Plenum Press, New York, (1982), p. 73.
14. H. D. Smith Jr, C. O. Obenland and S. Papetti, Inorg. Chem. 1966, 5, 1013.
15. +. The conductivity of a solution of [4H] [3H] in acetonitrile was typical of a 1:1 electrolyte.
16. T. K. Hansen, J. Becher, T. Jørgensen, K. S. Varma, R. Khedeker and M. P. Cava, Org. Synth. 1996, 73, 270.
17. (a) T. K. Hansen, T. Jørgensen, P. C. Stein and J. Becher, J. Org. Chem. 1992, 57, 6403;
18. (b) J. Röhrich, P. Wolf, V. Enkelmann and K. Müllen, Angew. Chem. 1988, 100, 1429.
19. C. K. Johnson, ORTEPII. Report ORNL-5138. Oak Ridge National Laboratory, Tennessee, U.S.A., 1976.
20. (a) M. Bousseau, L. Valade, J.-P. Legros, P. Cassoux, M. Garbauskas and L. V. Interrante, J. Am. Chem. Soc. 1986, 108, 1908; T. A. James and J. A. McCleverty, J. Chem. Soc. A, 1970, 3308.
21. (a) M. Bousseau, L. Valade, J.-P. Legros, P. Cassoux, M. Garbauskas and L. V. Interrante, J. Am. Chem. Soc. 1986, 108, 1908; T. A. James and J. A. McCleverty, J. Chem. Soc. A, 1970, 3308.
22. F. H. Allen, O. Kennard, D. G. Watson, L. Brammer, A. G. Orpen and R. Taylor, J. Chem., Soc. Perkin Trans. 2, 1987, S1.
23. CSD. Cambridge Structural Database (April 1996 release). Cambridge Crystallographic Data Centre, Cambridge CB2 1EZ, U.K., 1996.
24. W. D. S. Motherwell and W. Clegg, PLUTO 88. Program for Plotting Molecular and Crystal Structures. Cambridge Structural Database System, Users Manual, Part II, Cambridge, 1988 (implemented at the Manchester Computing Centre).
25. F. Wudl and M. L. Kaplan, J. Org. Chem. 1974, 39, 3608.
26. TeXsan. Single Crystal Analysis Software, Version 1.6. Molecular Structure Corporation, The Woodlands, TX 77381, U.S.A., 1993.
27. G. M. Sheldrick, SHELXL-93. Program for Crystal Structure Refinement. University of Gottingen, Germany, 1993.