Synthesis of several di- and trispiro cyclic siliconmethylene compounds: X-ray crystal structure of 5,7,13-trisila-trispiro [4.1.4.1.4.1]octadecane and 6,8,15-trisila-trispiro[5.1.5.1.5.1]heneicosane

Polyhedron

Volumn 15, Issue 9, 1996, Pages 1545-1551

  Kotlar, Anthony J ^a   Kriner, William A ^a   Mueller, Timothy E ^a   Falvello, Larry R ^b  

^a SAINT JOSEPH S UNIVERSITY   (United States)

^b UNIVERSITY OF ZARAGOZA   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0039334521     PISSN: 02775387     EISSN: None     Source Type: Journal    
DOI: 10.1016/0277-5387(95)00373-8     Document Type: Article

References (16)

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3. (c) N. Auner, C. Seidenschwarz and N. Sewald, Organometallics 1992, 11, 1137;
4. (d) A. Bassindale and P. Caspar (Eds), Front. Organosilicon Chem. (Proc. Int. Symp. Organosilicon Chem.) (1991) and references therein.
5. W. A. Kriner. J. Org. Chem. 1964, 29, 1601.
6. 3rd International Symposium on Organosilicon, Madison, WI (1972).
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8. (a) Computing was done on a Hewlett-Packard 715/50 (HP-UX V9.01) and on a Local Area VAX-cluster (VAX/VMS V5.5). Software was from the commercial package SHELXTL-PLUS, and the refinement was done by the program SHELXL-93;
9. (b) SHELXTL-PLUS Release 4.21/V. Siemens Analytical X-ray Instruments, Inc., Maddison, WI (1990);
10. (c) G. M. Sheldrick, SHELXL-93, FORTRAN-77 Program for the Refinement of Crystal Structures from Diffraction Data. University of Göttingen (1993);
11. (d) G. M. Sheldrick, J. Appl. Cryst., 1994, in preparation.
12. H. D. Flack, Acta Cryst. 1983, A39, 876.
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