Synthesis and characterization of [(CO)4FeL-L] and [(CO)4feL-LFe(CO)4] wherein L-L is N(CH2CH2)3N and also P(NMeNMe)3P in the latter complex. Single crystal X-ray molecular structure of [Fe(CO)4DABCO]

Journal of the Brazilian Chemical Society

Volumn 14, Issue 1, 2003, Pages 71-75

  Matos, Robson M ^a,b   Verkade, John G ^a  

^a IOWA STATE UNIVERSITY   (United States)

^b FEDERAL UNIVERSITY OF MINAS GERAIS   (Brazil)

Author keywords

DABCO; NMR spectroscopy; Tetracarbonyliron

Indexed keywords

CARBONYL IRON; IRON DERIVATIVE;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; CRYSTAL STRUCTURE; INFRARED SPECTROSCOPY; PHOSPHORUS NUCLEAR MAGNETIC RESONANCE; PROTON NUCLEAR MAGNETIC RESONANCE; ROTATION; STRUCTURE ANALYSIS; SYNTHESIS; ULTRAVIOLET IRRADIATION; X RAY ANALYSIS;

EID: 0038755136     PISSN: 01035053     EISSN: None     Source Type: Journal    
DOI: 10.1590/S0103-50532003000100012     Document Type: Article

References (28)

1. Whitmire, K. H. In Comprehensive Organometallic Chemistry II; Abel; E. A.; Stone, F. G. A.; Wilkinson, G., eds.; Elsevier Science: Oxford, UK, 1995, vol. 7, p.1.
2. Shubert, E. H.; Sheline, R. K.; Inorg. Chem. 1966, 5, 1071.
3. Cotton, F. A.; Troup, J. M.; J. Am. Chem. Soc. 1974, 96, 3438.
4. Fanchinetti, G.; Fochi, G.; Funaioli, T.; Zanazzi, P. F.; J. Chem. Soc., Chem. Commun. 1987, 87.
5. Mealli, C.; Proserpio, D. M.; Fachinetti, G.; Funaioli, T.; Fochi, G.; Zanazzi, P. F.; Inorg. Chem. 1989, 28, 1122.
6. Birencwaig, F.; Shamai, H.; Shvo, Y.; Tetrahedron Letters 1979, 31, 2947.
7. Elzinga, J.; Hogeveen, H.; J. Chem. Soc., Chem. Commun. 1977, 705.
8. Hieber, W.; Wemer, R.; Chem. Ber. 1957, 90, 286.
9. Hieber, W.; Angew. Chem. 1960, 72, 795.
10. Hieber, W.; Kahlen, R.; Chem. Ber. 1958, 91, 2223.
11. Edgell, W. F.; Yang, M. T.; J. Am. Chem. Soc. 1966, 88, 4839.
12. Shriver, D. F.; Whitmire, K. H., In Comprehensive Organometallic Chemistry, Wilkinson, G.; Stone, F. G. A.; Abel, E. W. eds., Pergamon Press: Oxford, UK, 1982, vol. 4, p. 243.
13. Hieber, W.; Beutner, H.; Angew. Chem., Int. Ed. Engl. 1962, 1, 116.
14. Goetze, R.; Nöth, H.; Payne, D. S.; Chem. Ber. 1972, 105, 2637.
15. Nöth, H.; Ullmann, R.; Chem. Ber. 1974, 107, 1019.
16. Blessing, R. H.; Acta Cryst. 1995, A51, 33.
17. All software and sources of the scattering factors are contained in the SHELXTL (version 5.1) program library (G. Sheldrick, Bruker Analytical X-Ray Systems, Madison, WI).
18. Adams, R. D.; Cotton, F. A.; In Dynamic Nuclear Magnetic Resonance Spectroscopy, Jackman, L. M.; Cotton,F. A., eds., Academic Press: New York, 1975, p. 489.
19. Udovich, C. A.; Clark, R. J.; Hass, H.; Inorg. Chem. 1969, 8, 1066.
20. Langford, G. R.; Akhtar, M.; Ellis, P. D.; MacDiarmid; A. G.; Odom, J. D.; Inorg. Chem. 1975, 98, 5728.
21. Jesson, J. P.; Meakin, P.; J. Am. Chem. Soc. 1973, 95, 1344.
22. Darensbourg, D. J.; Nelson, III, H. H.; Hyde, C. L.; Inorg. Chem. 1974, 13, 2135.
23. Riley, P.; Davis, R. E; Inorg. Chem., 1980, 19, 159.
24. Pickardt, J.; Rosch, L.; Schumann, H.; J. Organomet. Chem. 1976, 107, 241.
25. Kilbourn, B. T.; Raeburn, U. A.; Thompson, D. T.; J. Chem. Soc. 1969, 1906.
26. Cotton, F. A.; Hanson, B. E.; Isr. J. Chem. 1977, 15, 165.
27. Lee, I. S.; Lee, S. S.; Chung, Y. K.; Kim, D.; Song, N. W.; Inorg. Chim. Acta, 1998, 279, 243.
28. P. M. Stricklen; J.G. Verkade, unpublished work.