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85031162540
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13C NMR, IR, and HRMS.
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13C NMR, IR, and HRMS.
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16
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0037162785
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Based on this result, a possibility that DMF acts as a CO source through decomposition of DMF can be ruled out. For reference of the example, see:
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Based on this result, a possibility that DMF acts as a CO source through decomposition of DMF can be ruled out. For reference of the example, see: Wan Y., Alterman M., Larhed M., Hallberg A. J. Org. Chem. 67:2002;6232.
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Hallberg, A.4
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85031169062
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note
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+), found 247.1575.
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18
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0001083573
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For some examples of Pd-catalyzed alkoxycarbonylation of alkynes using alcohol and CO, see: (a) Alper, H.; Despeyroux, B.; Woell, J. B. Tetrahedron Lett. 1983, 24, 5691; (b) Kushino, Y.; Itoh, K.; Miura, M.; Nomura, M. J. Mol. Catal. 1994, 89, 151; (c) Akao, M.; Sugawara, S.; Amino, K.; Inoue, Y. J. Mol. Catal. A: Chem. 2000, 157, 117.
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Alper, H.1
Despeyroux, B.2
Woell, J.B.3
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19
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0028416620
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For some examples of Pd-catalyzed alkoxycarbonylation of alkynes using alcohol and CO, see: (a) Alper, H.; Despeyroux, B.; Woell, J. B. Tetrahedron Lett. 1983, 24, 5691; (b) Kushino, Y.; Itoh, K.; Miura, M.; Nomura, M. J. Mol. Catal. 1994, 89, 151; (c) Akao, M.; Sugawara, S.; Amino, K.; Inoue, Y. J. Mol. Catal. A: Chem. 2000, 157, 117.
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J. Mol. Catal.
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Kushino, Y.1
Itoh, K.2
Miura, M.3
Nomura, M.4
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20
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0034690966
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For some examples of Pd-catalyzed alkoxycarbonylation of alkynes using alcohol and CO, see: (a) Alper, H.; Despeyroux, B.; Woell, J. B. Tetrahedron Lett. 1983, 24, 5691; (b) Kushino, Y.; Itoh, K.; Miura, M.; Nomura, M. J. Mol. Catal. 1994, 89, 151; (c) Akao, M.; Sugawara, S.; Amino, K.; Inoue, Y. J. Mol. Catal. A: Chem. 2000, 157, 117.
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Akao, M.1
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Inoue, Y.4
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21
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0003333344
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For hydroesterification of alkynes with methyl formate to methyl acrylate catalyzed by nickel catalyst, see:
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For hydroesterification of alkynes with methyl formate to methyl acrylate catalyzed by nickel catalyst, see: Yang X.-G., Zhang J.-Q., Liu Z.-T. Appl. Catal. A: General. 173:1998;11.
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Yang, X.-G.1
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Liu, Z.-T.3
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22
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0001214141
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For a previous example of Pd-catalyzed hydroesterification of alkynols, see:
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For a previous example of Pd-catalyzed hydroesterification of alkynols, see: El Ali B., Alper H. J. Mol. Catal. A Chem. 96:1995;197.
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El Ali, B.1
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23
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85031167488
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note
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Compound 4A is presumed to be formed from the hydroesterification of alkynol 3 with 1 at the opposite direction compared to 4B, and then by an intra-molecular cyclization.
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24
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0037139565
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Recently, ruthenium-catalyzed oxidative cyclization of alkynols has been reported, see:
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Recently, ruthenium-catalyzed oxidative cyclization of alkynols has been reported, see: Trost B.M., Rhee Y.H. J. Am. Chem. Soc. 124:2002;2528.
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J. Am. Chem. Soc.
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Trost, B.M.1
Rhee, Y.H.2
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25
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0011563050
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Alkoxycarbonylation of 1,2-polybutadiene with EtOH and CO was previously reported using Pd catalyst. See:
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Alkoxycarbonylation of 1,2-polybutadiene with EtOH and CO was previously reported using Pd catalyst. See: Ajjou A.N., Alper H. Macromolecules. 29:1996;1784.
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(1996)
Macromolecules
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Ajjou, A.N.1
Alper, H.2
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26
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0018354660
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For ruthenium-catalyzed isomerization of internal alkenes, see: (a) Suzuki, H.; Koyama, Y.; Moro-oka, Y.; Ikawa, T. Tetrahedron Lett. 1979, 20, 1415; (b) Zoran, A.; Sasson, Y.; Blum, J. J. Org. Chem. 1981, 46, 255; (c) Wakamatsu, H.; Nishida, M.; Adachi, N.; Mori, M. J. Org. Chem. 2000, 65, 3966.
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Tetrahedron Lett.
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Suzuki, H.1
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Ikawa, T.4
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27
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0001475503
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For ruthenium-catalyzed isomerization of internal alkenes, see: (a) Suzuki, H.; Koyama, Y.; Moro-oka, Y.; Ikawa, T. Tetrahedron Lett. 1979, 20, 1415; (b) Zoran, A.; Sasson, Y.; Blum, J. J. Org. Chem. 1981, 46, 255; (c) Wakamatsu, H.; Nishida, M.; Adachi, N.; Mori, M. J. Org. Chem. 2000, 65, 3966.
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Zoran, A.1
Sasson, Y.2
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28
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0034733140
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For ruthenium-catalyzed isomerization of internal alkenes, see: (a) Suzuki, H.; Koyama, Y.; Moro-oka, Y.; Ikawa, T. Tetrahedron Lett. 1979, 20, 1415; (b) Zoran, A.; Sasson, Y.; Blum, J. J. Org. Chem. 1981, 46, 255; (c) Wakamatsu, H.; Nishida, M.; Adachi, N.; Mori, M. J. Org. Chem. 2000, 65, 3966.
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Wakamatsu, H.1
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Mori, M.4
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