Polymorphism in mercury(I) selenite(IV): Preparation, crystal structures of α-, β-and γ-Hg2SeO3, and thermal behavior of the α- and β-modification

Journal of Solid State Chemistry

Volumn 172, Issue 1, 2003, Pages 35-44

  Weil, Matthias ^a  

^a VIENNA UNIVERSITY OF TECHNOLOGY   (Austria)

Author keywords

Crystal structure; Hg2SeO3; Mercury(I); Oxoselenites(IV); Polymorphism; Thermal behavior

Indexed keywords

CRYSTAL STRUCTURE; CRYSTALLIZATION; CRYSTALLOGRAPHY; DECOMPOSITION; DIFFRACTOMETERS; DIFFUSION; HYDROTHERMAL SYNTHESIS; POLYCRYSTALLINE MATERIALS; PRECIPITATION (CHEMICAL); SELENIUM COMPOUNDS; SINGLE CRYSTALS; SOLUTIONS; STEREOCHEMISTRY;

CRYSTALLOGRAPHIC AXIS;

MERCURY (METAL);

MERCURY; MERCURY DERIVATIVE; NITRIC ACID DERIVATIVE; SELENIOUS ACID; SELENITE; SELENIUM DERIVATIVE; WATER;

ARTICLE; ATMOSPHERE; CHEMICAL MODIFICATION; CONCENTRATION (PARAMETERS); CRYSTAL STRUCTURE; CRYSTALLIZATION; DEMINERALIZATION; DIFFUSION; HEATING; STEREOCHEMISTRY;

EID: 0038739086     PISSN: 00224596     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-4596(02)00082-8     Document Type: Article

References (27)

1. Gmelins Handbuch der anorganischen Chemie. 1969;1094 34 Quecksilber B4, 8th Edition, Verlag Chemie, Weinheim.
2. Koskenlinna M., Valkonen J. Acta Crystallogr. C. 51:1995;1040.
3. Koskenlinna M., Valkonen J. Acta Crystallogr. C. 52:1996;491.
4. Koskenlinna M., Valkonen J. Acta Crystallogr. C. 52:1996;1070.
5. Stålhandske C. Acta Crystallogr. B. 34:1978;1049.
6. Dorm E. Acta Chem. Scand. 23:1969;1607.
7. Weil M. Z. Naturforsch. 57b:2002;1043.
8. Weil M., Kolitsch U. Acta Crystallogr. C. 58:2002;i47.
9. Weil M. Solid State Sci. 4:2002;1153.
10. Verma V.P. Thermochim. Acta. 327:1999;63.
11. Berzelius J.J. Afh. Fys. Kemi Mineral. 6:1818;42.
12. J.J. Berzelius, Ann. Chim. Phys. 9 (1818) 160, 225, 337.
13. J.J. Berzelius, Schweiggers J. Chem. Physik. 23 (1818) 309, 430.
14. Werner P.-E., Eriksson L., Westdahl M. J. Appl. Crystallogr. 18:1985;367.
15. A.C. Larson, R.B. Von Dreele, General Structure Analysis System (GSAS), LANSCE, MS-H805, Los Alamos National Laboratory, Los Alamos, NM, USA, 2000.
16. P.J. Mohr, B.N. Taylor, CODATA, Recommended Values of the Fundamental Physical Constants, National Institute of Standards and Technology, Gaithersburg, MD, USA, 1998.
17. Sheldrick G.M. SHELX97, Program for Crystal Structure Solution and Refinement. 1997;University of Göttingen, Germany.
18. W. Herrendorf, HABITUS, Program for Optimization of the Crystal Shape for the Numerical Absorption Correction, Universities of Karlsruhe and Gieβen, Germany, 1993/1997.
19. Bruker AXS, SHELXTL, Version 5.1, Madison, WI, USA, 1998.
20. Flack H.D. Acta Crystallogr. A. 39:1983;876.
21. A.K. Spek, PLATON, a multipurpose crystallographic tool, Utrecht University, Utrecht, The Netherlands, 2001.
22. E. Dowty, ATOMS for Windows, Version 5.1, Shape Software, 521 Hidden Valley Road, Kingsport, TN USA, (2000).
23. Grdenić D. Q. Rev. Chem. Soc. 19:1965;303.
24. Brese N.E., O' Keeffe M. Acta Crystallogr. B. 47:1991;192.
25. Pervukhina N.V., Margarill S.A., Borisov S.V., Romanenko G.V., Pal'chik N.A. Russ. Chem. Rev. 68:1999;615.
26. Gospodinov G.G., Bogdanov B.G. Thermochim. Acta. 71:1983;391.
27. C.K. Johnson, ORTEPII., Report ORNL-5138, Oak Ridge National Laboratory, TN, USA, 1976.