Trifluoromethylselenate(0), [SeCF3]-, and trifluoromethyltellurate(0), [TeCF3]- - Crystalline products of the reduction of the bis(trifluoromethyl)dichalkogen compounds, E2(CF3)2 (E = Se, Te), with tetrakis(dimethylamino)ethene (TDAE)

Zeitschrift fur Anorganische und Allgemeine Chemie

Volumn 629, Issue 6, 2003, Pages 1039-1043

  Tyrra, Wieland ^a   Naumann, Dieter ^a   Pohl, Herbert ^a   Pantenburg, Ingo ^a  

^a UNIVERSITY OF COLOGNE   (Germany)

Author keywords

Crystal structure; Selenium; Tellurium; Trifluoromethylchalcogenates(0)

Indexed keywords

ETHYLENE DERIVATIVE; METHYL GROUP; SELENIUM DERIVATIVE; TELLURIUM DERIVATIVE; TETRAKIS(DIMETHYLAMINO)ETHENE; TRIFLUOMETHYLTELLURATE; TRIFLUOROMETHYLSELENATE; UNCLASSIFIED DRUG;

ARTICLE; COLOR; CRYSTAL STRUCTURE; CRYSTALLIZATION; QUANTITATIVE ANALYSIS; REDUCTION; SOLID;

EID: 0038722674     PISSN: 00442313     EISSN: None     Source Type: Journal    
DOI: 10.1002/zaac.200300016     Document Type: Article

References (39)

1. W. B. Farnham, W. J. Middleton, US Patent 4 628 094 (1986).
2. W. Tyrra, D. Naumann, B. Hoge, Yu. L. Yagupolskii, J. Fluorine Chem. 2003, 109, 101-107 and references cited therein.
3. W. Tyrra, D. Naumann, Yu. L. Yagupolskii, J. Fluorine Chem. accepted.
4. A. Darmadi, A. Haas, B. Koch, Z. Naturforsch. 1980, 35b, 526-529.
5. H. Bock, K. Ruppert, K. Merzweiler, D. Fenske, H. Goesmann, Angew. Chem. 1989, 101, 1715-1717; Angew. Chem. Int. Ed. Engl. 1989, 28, 1684-1685.
6. H. Bock, K. Ruppert, K. Merzweiler, D. Fenske, H. Goesmann, Angew. Chem. 1989, 101, 1715-1717; Angew. Chem. Int. Ed. Engl. 1989, 28, 1684-1685.
7. G. Pawelke, J. Fluorine Chem. 1989, 42, 429-433.
8. N. Wiberg, Angew. Chem. 1968, 80, 809-822; Angew. Chem. Int. Ed. Engl. 1968, 7, 776-779.
9. N. Wiberg, Angew. Chem. 1968, 80, 809-822; Angew. Chem. Int. Ed. Engl. 1968, 7, 776-779.
10. R. D. Chambers, W. K. Gray, G. Sandford, J. F. S. Vaughan, J. Fluorine Chem. 1999, 94, 213-215.
11. A. Kolomeitsev, M. Médebielle, P. Kirsch, E. Lork, G.-V. Röschenthaler, J. Chem. Soc., Perkin Trans. I 2000, 2183-2185.
12. N. G. Payne, M. E. Peach, K. J. Schmidt, J. Fluorine Chem. 1993, 64, 255-258.
13. J. Kischkewitz, D. Naumann, Z. Anorg. Allg. Chem. 1987, 547, 167-172.
14. R. A. DeMarco, W. B. Fox, W. B. Moniz, S. A. Sojka, J. Magn. Reson. 1975, 18, 522-526.
15. W. Gombler, Angew. Chem. 1977, 89, 740; Angew. Chem. Int. Ed. Engl. 1977, 16, 723.
16. W. Gombler, Angew. Chem. 1977, 89, 740; Angew. Chem. Int. Ed. Engl. 1977, 16, 723.
17. W. Gombler, Z. Naturforsch. 1981, 36b, 535-543.
18. W. Gombler, Habilitationsschrift, Bochum, 1982.
19. H. Pohl, Diplomarbeit, Univ. Köln, 1997.
20. S. Herberg, D. Naumann, Z. Anorg. Allg. Chem. 1982, 492, 95-102.
21. S. Boye, Dissertation, Univ. Köln, 1996.
22. K. Elbl-Weiser, C. Krieger, H. A. Staab, Angew. Chem. 1990, 102, 183-185; Angew. Chem. Int. Ed. Engl. 1990, 29. 211-212.
23. K. Elbl-Weiser, C. Krieger, H. A. Staab, Angew. Chem. 1990, 102, 183-185; Angew. Chem. Int. Ed. Engl. 1990, 29. 211-212.
24. K. J. Wiberg, J. Am. Chem. Soc. 1990, 112, 3379-3385.
25. W. Gombler, Phosphorus, Sulfur Silicon Rel. Elem. 1988, 38, 231-243.
26. D. Christen, H. Oberhammer, W. Zeil, A. Haas, A. Darmadi, J. Mol. Struct. 1980, 66, 2203-210.
27. B. Solouki, H. Bock, A. Haas, M. Baum, C. Monse, Z. Havlas, Z. Anorg. Allg. Chem. 1999, 625, 1726-1731.
28. C. Meyer, D. Mootz, B. Bäck, R. Minkwitz, Z. Naturforsch. 1997, 53b, 69-71.
29. C. J. Marsden, G. M. Sheldrick, J. Mol. Struct. 1971, 10, 419-425.
30. W. Dukat, F. Gall, C. Meyer, D. Mootz, D. Naumann, G. Nowicki, K. Schulz, Z. Anorg. Allg. Chem. 1996, 622, 617-621.
31. H. Oberhammer, W. Gombler, H. Willner, J. Mol. Struct. 1981, 70, 273-281.
32. C. J. Marsden, G. M. Sheldrick, J. Mol. Struct. 1971, 10, 405-412.
33. K.-J. Ramme, Dissertation, Univ. Tübingen, 1984.
34. P. Jutzi, Chem. Unserer Zeit 1981, 15, 149-154.
35. X-RED 1.22, Stoe Data Reduction Program (C) 2001 Stoe & Cie GmbH Darmstadt.
36. X-Shape 1.06, Crystal Optimisation for Numerical Absorption Correction (C) 1999 STOE & Cie GmbH Darmstadt.
37. Crystallographic data for the structures have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication nos. CCDC 199672 for I and CCDC 199673 for II. Copies of the data can be obtained, free of charge, on application to CHGC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: +44 1223 336033 or e-mail: deposit@ccdc.cam.ac.uk).
38. G. M. Sheldrick, SHELXS-97-Program for Structure Analysis, Göttingen, (1998).
39. G. M. Sheldrick, SHELXL-93-Program for Crystal Structure Refinement, Göttingen (1993).