9α-fluoro-16α-methyl-3,11-dioxoan-drosta-1,4-diene-17β- carboxylic acid: Catemeric hydrogen bonding and acetic acid solvation in a steroidal keto acid related to dexamethasone

Acta Crystallographica Section C: Crystal Structure Communications

Volumn 59, Issue 5, 2003, Pages

  Lalancette, Roger A ^a   Thompson, Hugh W ^a  

^a RUTGERS UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ACETIC ACID; CRYSTAL STRUCTURE; FLUORINE COMPOUNDS; HYDROGEN BONDS; KETONES; MOLECULAR ORIENTATION; MOLECULES;

FLUOROMETHYL DIOXOANDROSTADIENECARBOXYLIC ACID; KETO ACID; SOLVATION; STEROIDS;

CARBOXYLIC ACIDS;

EID: 0038722639     PISSN: 01082701     EISSN: None     Source Type: Journal    
DOI: 10.1107/S0108270103007121     Document Type: Article

References (12)

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3. Dupont, L., Dideberg, O. & Campsteyn, H. (1974). Acta Cryst. B30, 514-516.
4. Joly, R., Warnant, J., Goffinet, B., Jelly, J. & Prost-Marechal, J. (1974). Arzneim. Forsch. 24, 1-3.
5. Leiserowitz, L. (1976). Acta Cryst. B32, 775-802.
6. Newman, J. M., Lalancette, R. A. & Thompson, H. W. (2002). Acta Cryst. C58, o402-o404.
7. Sheldrick, G. M. (1997a). SHELXL97 and SHELXS97. University of Göttingen, Germany.
8. Sheldrick, G. M. (1997b). SHELXTL. Version 5.10. Bruker AXS Inc., Madison, Wisconsin, USA.
9. Siemens (1996). XSCANS. Siemens Analytical X-ray Instruments Inc., Madison, Wisconsin, USA.
10. Steiner, T. (1997). Chem. Commun. pp. 727-734.
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12. Thompson, H. W., Lalancette, R. A. & Brunskill, A. P. J. (1999). Acta Cryst. C55, 1680-1682.