Synthesis of trans-disubstituted cyclam ligands appended with two 6-hydroxymethylpyridin-2-ylmethyl sidearms: Crystal structures of the 1,8-dimethyl-4,11-di(6-hydroxymethylpyridin-2-ylmethyl)cylam ligand and its Co(II) and Ni(II) complexes

Journal of Heterocyclic Chemistry

Volumn 40, Issue 2, 2003, Pages 383-387

  Xue, Guoping ^a   Bradshaw, Jerald S ^a   Dalley, N Kent ^a   Savage, Paul B ^a   Izatt, Reed M ^a  

^a Brigham Young University   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

1,8 BIS(6 HYDROXYMETHYLPYRIDIN 2 YLMETHYL) 1,4,8,11 TETRAAZACYCLOTETRADECANE; 1,8 DIMETHYL 4,11 BIS(6 HYDROXYMETHYLPYRIDIN 2 YLMETHYL) 1,4,8,11 TETRAAZACYCLOTETRADECANE; COBALT DERIVATIVE; CYCLAM DERIVATIVE; LIGAND; NICKEL COMPLEX; UNCLASSIFIED DRUG;

ANISOTROPY; ARTICLE; ATOM; CARBON NUCLEAR MAGNETIC RESONANCE; CRYSTAL STRUCTURE; DRUG CONFORMATION; DRUG HYDROLYSIS; DRUG STRUCTURE; DRUG SYNTHESIS; PROTON NUCLEAR MAGNETIC RESONANCE;

EID: 0038710846     PISSN: 0022152X     EISSN: None     Source Type: Journal    
DOI: 10.1002/jhet.5570400232     Document Type: Article

References (26)

1. J. S. Bradshaw, K. E. Krakowiak and R. M. Izatt, Aza-crown Macrocycles in The Chemistry of Heterocyclic Compounds Vol 51; E. C. Taylor Ed.; John Wiley & Sons, Inc.: New York, 1993 pp. 1-885.
2. R. M. Izatt, R. L. Burening and M. B. Borup, Water Sci. Technol., 23, 301 (1991).
3. R. M. Izatt, K. Pawlak, J. S. Bradshaw and R. L. Bruening, Chem Rev., 95, 2529 (1995).
4. A. E. Martell, R. D. Hancock and R. J. Motekaitis, Coord. Chem. Rev., 133, 39 (1994).
5. F. Denat, S. Lacour, S. Brandès and R. Guilard, Tetrahedron Lett., 38, 4417 (1997).
6. I. Alfonso, C. Astorga, F. Rebolledo and V. Gotor, Tetrahedron: Asymmetry, 10, 2515 (1999).
7. B. M. Kim and S. M. So, Tetrahedron Lett., 40, 7687 (1999).
8. B. Gaudinet-Hamann, J. Zhu, H. Fensterbank and C. Larpent, Tetrahedron Lett., 40, 287 (1999).
9. A. K. Bazak and T. A. Kaden, Helv. Chim. Acta, 66, 2086 (1983).
10. W. Schibler and T. A. Kaden, J. Chem. Soc., Chem. Commun., 603 (1981).
11. M. Ciampolini, L. Fabbrizzi, M. Licchelli, A. Perotti, F. Pezzini and A. Poggi, Inorg. Chem., 25, 4131 (1986).
12. D. Tschudin, A. K. Bazak and T. A. Kaden, Helv. Chim. Acta, 71, 100 (1988).
13. E. Asato, H. Shinji, N. Matsumoto and S. Kida, J. Chem. Soc., Dalton Trans., 1741 (1990).
14. E. K. Barefield, K. A. Foster, G. M. Freeman and K. D. Hodges, Inorg. Chem., 25, 4663 (1986).
15. H. Häfliger and T. A. Kaden, Helv. Chim. Acta, 62, 683 (1979).
16. K. P. Wainwright, J. Chem. Soc., Dalton Trans., 2117 (1980).
17. C. M. Madeyski, J. P. Michael and R. D. Hancock, Inorg. Chem., 23, 1487 (1984).
18. P. J. Davies, M. R. Taylor, K. P. Wainwright, P. Harriott and P. A. Duckworth, Inorg. Chim. Acta, 246, 1 (1996).
19. M. Hediger and T. A. Kaden, Helv. Chim. Acta., 66, 861 (1983).
20. T. A. Kaden, Top. Curr. Chem., 121, 157 (1984).
21. M. Ciampolini, M. Micheloni, N. Nardi and P. Paoletti, J. Chem. Soc., Dalton Trans., 1357 (1984).
22. E. Kimura, J. Coord. Chem., 15 (1986).
23. M. Ciampolini, L. Fabbrizzi, A. Perotti, A. Poggi, B. Seghi and F. Zanobini, Inorg. Chem., 26, 3527 (1987).
24. G. Royal, V. Dahasui-Gindrey, S. Dahasui, A. Tabard, R. Guilard, P. Pullumbi and C. Lecomte, Eur. J. Org. Chem., 1971 (1998).
25. M. Newcomb, J. M. Timko, D. M. Walba and D. J. Cram, J. Am. Chem. Soc., 99, 6392 (1997).
26. G. M. Sheldrick, SHELXTL PC version 5.03, Bruker Analytical X-ray Systems, Madison, WI, 1994.