Unsaturated hetero chains, IX([≠]) 1:1- and 2:1-copper(II) complexes from primary N-acylamidines

European Journal of Inorganic Chemistry

Volumn , Issue 8, 2000, Pages 1739-1743

  Eberhardt, Jan K ^a   Fröhlich, Roland ^a   Venne Dunker, Sabine ^a   Würthwein, Ernst Ulrich ^a  

^a UNIVERSITY OF MÜNSTER   (Germany)

Author keywords

Copper(II) complexes; N ligands; N acylamidines; O ligands

Indexed keywords

COPPER COMPOUNDS; LIGANDS; SYNTHESIS (CHEMICAL); X RAY DIFFRACTION ANALYSIS;

APPROXIMATE SQUARE; CHARGED COMPLEXES; COPPER(II) COMPLEX; COUNTERIONS; N LIGANDS; N-ACYLAMIDINE; N-LIGANDS; O LIGANDS; POSITIVELY CHARGED; SYNTHESISED;

IONS;

BENZAMIDINE DERIVATIVE; COPPER COMPLEX; LIGAND; METAL COMPLEX;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; CHEMICAL REACTION; CHEMICAL STRUCTURE; COMPLEX FORMATION; PROTON NUCLEAR MAGNETIC RESONANCE; SYNTHESIS; X RAY DIFFRACTION;

EID: 0038700406     PISSN: 14341948     EISSN: None     Source Type: Journal    
DOI: 10.1002/1099-0682(200008)2000:8<1739::aid-ejic1739>3.3.co;2-d     Document Type: Article

References (18)

1. The results described in this paper are part from the Diploma Thesis of J. K. Eberhardt, University of Münster, 1999.
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11. Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publications no. CCDC-137212 (2), CCDC-137213 (3), CCDC-137114 (4), and CCDC-137215 (5). Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge, CB2 1EZ, UK [Fax: (internat.) + 44-1223/336-033; E-mail: deposit@ccdc.cam.ac.uk].
12. Programs used: Data collection: Collect: Nonius B. V., 1994. - Data reduction: Denzo-SMN: Z. Otwinowski, W. Minor, Methods in Enzymology 1997, 276, 307-326. - Absorption correction: SORTAN: R. H. Blessing, Acta Cryst. 1995, A51, 33-37; J. Appl. Cryst. 1997, 30, 421-426. - Structure solution: SHELXS-86 and SHELXS-97: G. M. Sheldrick, Acta. Cryst. 1990, A46, 467-473. - Structure refinement: SHELXL- 97: G. M. Sheldrick, Universität Göttingen, 1997. - Graphics: SCHAKAL: E. Keller, Universität Freiburg, 1997.
13. Programs used: Data collection: Collect: Nonius B. V., 1994. - Data reduction: Denzo-SMN: Z. Otwinowski, W. Minor, Methods in Enzymology 1997, 276, 307-326. - Absorption correction: SORTAN: R. H. Blessing, Acta Cryst. 1995, A51, 33-37; J. Appl. Cryst. 1997, 30, 421-426. - Structure solution: SHELXS-86 and SHELXS-97: G. M. Sheldrick, Acta. Cryst. 1990, A46, 467-473. - Structure refinement: SHELXL- 97: G. M. Sheldrick, Universität Göttingen, 1997. - Graphics: SCHAKAL: E. Keller, Universität Freiburg, 1997.
14. Programs used: Data collection: Collect: Nonius B. V., 1994. - Data reduction: Denzo-SMN: Z. Otwinowski, W. Minor, Methods in Enzymology 1997, 276, 307-326. - Absorption correction: SORTAN: R. H. Blessing, Acta Cryst. 1995, A51, 33-37; J. Appl. Cryst. 1997, 30, 421-426. - Structure solution: SHELXS-86 and SHELXS-97: G. M. Sheldrick, Acta. Cryst. 1990, A46, 467-473. - Structure refinement: SHELXL- 97: G. M. Sheldrick, Universität Göttingen, 1997. - Graphics: SCHAKAL: E. Keller, Universität Freiburg, 1997.
15. Programs used: Data collection: Collect: Nonius B. V., 1994. - Data reduction: Denzo-SMN: Z. Otwinowski, W. Minor, Methods in Enzymology 1997, 276, 307-326. - Absorption correction: SORTAN: R. H. Blessing, Acta Cryst. 1995, A51, 33-37; J. Appl. Cryst. 1997, 30, 421-426. - Structure solution: SHELXS-86 and SHELXS-97: G. M. Sheldrick, Acta. Cryst. 1990, A46, 467-473. - Structure refinement: SHELXL- 97: G. M. Sheldrick, Universität Göttingen, 1997. - Graphics: SCHAKAL: E. Keller, Universität Freiburg, 1997.
16. Programs used: Data collection: Collect: Nonius B. V., 1994. - Data reduction: Denzo-SMN: Z. Otwinowski, W. Minor, Methods in Enzymology 1997, 276, 307-326. - Absorption correction: SORTAN: R. H. Blessing, Acta Cryst. 1995, A51, 33-37; J. Appl. Cryst. 1997, 30, 421-426. - Structure solution: SHELXS-86 and SHELXS-97: G. M. Sheldrick, Acta. Cryst. 1990, A46, 467-473. - Structure refinement: SHELXL- 97: G. M. Sheldrick, Universität Göttingen, 1997. - Graphics: SCHAKAL: E. Keller, Universität Freiburg, 1997.
17. Programs used: Data collection: Collect: Nonius B. V., 1994. - Data reduction: Denzo-SMN: Z. Otwinowski, W. Minor, Methods in Enzymology 1997, 276, 307-326. - Absorption correction: SORTAN: R. H. Blessing, Acta Cryst. 1995, A51, 33-37; J. Appl. Cryst. 1997, 30, 421-426. - Structure solution: SHELXS-86 and SHELXS-97: G. M. Sheldrick, Acta. Cryst. 1990, A46, 467-473. - Structure refinement: SHELXL-97: G. M. Sheldrick, Universität Göttingen, 1997. - Graphics: SCHAKAL: E. Keller, Universität Freiburg, 1997.
18. Programs used: Data collection: Collect: Nonius B. V., 1994. - Data reduction: Denzo-SMN: Z. Otwinowski, W. Minor, Methods in Enzymology 1997, 276, 307-326. - Absorption correction: SORTAN: R. H. Blessing, Acta Cryst. 1995, A51, 33-37; J. Appl. Cryst. 1997, 30, 421-426. - Structure solution: SHELXS-86 and SHELXS-97: G. M. Sheldrick, Acta. Cryst. 1990, A46, 467-473. - Structure refinement: SHELXL- 97: G. M. Sheldrick, Universität Göttingen, 1997. - Graphics: SCHAKAL: E. Keller, Universität Freiburg, 1997.