Reactivity of cyclometallated semicarbazone complexes of Pd(II): Crystal and molecular structures of [Pd{C6H4C(Et)=NN(H)C(=O)NH2}(PPh 3)][ClO4] and [Pd{C6H4C(Et)=NN(H)C(=O)NH2}{(Ph 2PCH2CH2)2PPh-P,P,P}][Cl]

Journal of Organometallic Chemistry

Volumn 598, Issue 1, 2000, Pages 1-12

  Fernández, Alberto ^a   López Torres, Margarita ^a   Suárez, Antonio ^a   Ortigueira, Juan M ^b   Pereira, Teresa ^b   Fernández, Jesús J ^a   Vila, José M ^b   Adams, Harry ^c  

^a UNIVERSITY OF A CORUÑA   (Spain)

^b UNIVERSITY OF SANTIAGO DE COMPOSTELA   (Spain)

^c UNIVERSITY OF SHEFFIELD   (United Kingdom)

Author keywords

Cyclometallated; Palladium; Semicarbazone

Indexed keywords

EID: 0038528853     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-328X(99)00629-4     Document Type: Article

References (30)

1. Omae I. Organometallic Intramolecular-Coordination Compounds. 1986;Elsevier Science, Amsterdam.
2. Dunina V.V., Zalevskaya O.A., Potapov V.M. Russ. Chem. Rev. 571:1984;250.
3. Newkome G.R., Puckett W.E., Gupta W.K., Kiefer G.E. Chem. Rev. 86:1986;451.
4. Ryabov A.D. Chem. Rev. 90:1990;403.
5. Pfeffer M. Recl. Trav. Chim. Pays-Bas. 109:1990;567.
6. Pfeffer M., Sutter J.P., Rottevel M.A., de Cian A., Fischer J. Tetrahedron. 48:1992;2440.
7. Ryabov A.D., van Eldik R., Le Borgne G., Pfeffer M. Organometallics. 12:1993;1386.
8. Espinet P., Esteruelas M.A., Oro L.A., Serrano J.L., Sola E. Coord. Chem. Rev. 17:1992;215.
9. Bose A., Saha C.H. J. Mol. Catal. 49:1989;271.
10. Vila J.M., Gayoso M., Pereira M.T., López-Torres M., Fernández J.J., Fernández A., Ortigueira J.M. J. Organomet. Chem. 532:1997;171.
11. Vila J.M., Pereira M.T., Ortigueira J.M., Lata D., López-Torres M., Fernández J.J., Fernández A., Adams H. J. Organomet. Chem. 566:1998;93.
12. Vila J.M., Pereira T., Ortigueira J.M., López-Torres M., Castiñeiras A., Lata D., Fernández J.J., Fernández A. J. Organomet. Chem. 556:1998;21.
13. J.M. Vila, M.T. Pereira, J.M. Ortigueira, M. López-Torres, D. Lata, M. Graña, A. Suárez, J.J. Fernández, A. Fernández, Unpublished results.
14. Nonoyama M. Inorg. Chim. Acta. 145:1988;53.
15. Vila J.M., Gayoso M., Fernández A., Bailey N.A., Adams H. J. Organomet. Chem. 448:1993;233.
16. Vila J.M., Gayoso M., Pereira M.T., López-Torres M., Fernández J.J., Fernández A., Ortigueira J.M. Z. Anorg. Allg. Chem. 623:1997;844.
17. 13C-NMR of Transition Metal Phosphine Complexes in NMR. 1979;52 Springer, Berlin.
18. Pauling L. The Nature of the Chemical Bond. 3rd ed. 1960;Cornell University, New York.
19. Tollari S., Palmisano G., Demartin F., Grassi M., Magnaghi S., Cenini S. J. Organomet. Chem. 488:1995;79.
20. Abboud K.A., Summers S.P., Palenik G.J. Acta Crystallogr., Sect. C. 51:1995;1709.
21. F. Cecconi, C.A. Ghilardi, S. Midollini, S. Moneti, A. Orlandini, G. Scapacci, J. Chem. Soc. Dalton Trans. (1989) 211.
22. (a) D. Granell, J. Sainz, X. Solans, M. Font-Altaba, J. Chem. Soc. Dalton Trans. (1986) 1785.
23. (b) I.R. Butler, M. Kalaji, L. Nehrlich, M. Hurthouse, A.I. Karaulov, K.M.A. Malik, J. Chem. Soc. Chem. Commun. (1995) 459.
24. (c) J. Vicente, A. Arcas, D. Bautista, P.G. Jones, Organometallics 16 (1987) 2127.
25. (d) J.M. Vila, M.T. Pereira, J.M. Ortigueira, M. López-Torres, J.J. Fernández, A. Fernández, M. López-Torres, H. Adams, Organometallics (in press).
26. (a) C.E. Housecroft, B.A.M. Shaykh, A.L. Rheingold, B.S. Haggerty, Acta Crystallogr., Sect. C. 46 (1990) 1549.
27. (b) B.L. DuBois, A. Miedaner, R.C. Haltiwanger, J. Am. Chem. Soc. 119 (1991) 8753.
28. Vila J.M., Gayoso M., López-Torres M., Fernández J.J., Fernández A., Ortigueira J.M., Bailey N.A., Adams H. J. Organomet. Chem. 511:1996;129.
29. Perrin D.D., Armarego W.L.F. Purification of Laboratory Chemicals. 4th ed. 1996;Butterwort-Heinemann, London.
30. G.M. Sheldrick, SHELX-97, An integrated system for solving and refining crystal structures from diffraction data, University of Göttingen, Germany, 1997.