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2) = 0.073 for 330 parameters and 5291 independent reflections. Crystallographic data for 1 have been deposited with the Cambridge Crystallographic Data Center as supplementary publication no. CCDC 192014. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ, UK [fax: (+44) 1223-336-033; e-mail: deposit@ccdc.cam.ac.uk].
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